反应时间

Under the conditions of stir speeds 400 r·min~(-1) and distance between anode and cathode 1 mm, by using the orthogonal design, the optimum technological conditions were found that the current density was 0.3 A·cm~(-2), initial NaOH concentration in catholyte was 50 g·L~(-1), reaction times of two steps were all theoretical electrochemical reaction times. In the first electrosynthesis, initial Na_2CrO_4 concentration in anolyte was 650 g·L~(-1), and reaction temperature was 80℃. In the second electrosynthesis, initial Na_2Cr_2O_7 concentration in anolyte was 700 g·L~(-1), and reaction temperature was 85℃.

324全氟磺酸增强复合阳离子交换膜、阴阳极液中搅拌速度均为400r·min~(-1)条件下，通过正交实验得到优化工艺条件为：电流密度0.3A·cm~(-2)，阴极液氢氧化钠初始浓度50g·L~(-1)，两步反应时间均为理论电催化反应时间，第一步阳极液铬酸钠初始浓度650g·L~(-1)，反应温度80℃，第二步阳极液重铬酸钠初始浓度700g·L~(-1)，反应温度85℃。

Methods: The effects of the ratio of reactants, the amount of the catalyst used, the reaction time and the amount of an water-taking agent on synthesizing isoamyl cinnamate were investigated to obtain a suitable condition for synthesizing the ester.

考察了醇酸比、反应时间、带水剂用量等因素对合成肉桂酸异戊酯的影响，得到合成该酯的较适宜条件。结果：最佳反应条件为n：n=5：1，催化剂用量为肉桂酸用量的20%，反应时间2h，反应温度110～118℃，酯收率可达76.6%。

4The obtained solid alkali catalyst was applied to biodiesel preparation with colza oil and used oil as materials respectively and the technics was optimized by sigle-factor and orthogoral experiments with esterification rate as the index. The optimal technique conditions using colza oil were: the amount of solid catalyst 12%, the mol ratio of methanol to oil 9:1, reaction temperature 65℃, reaction time 3h, under which the esterification rate reached to 94.48%.

4以菜籽油和煎炸废油为原料，利用固体碱催化剂催化制备生物柴油，以转化率为考察指标，采用单因素和正交试验对工艺进行优化，得到以菜籽油为原料时制备的最佳工艺参数为固体催化剂投入量2.5％，醇油摩尔比9∶1，反应温度65℃，反应时间3h，转化率达到93.9％；以煎炸废油为原料时最佳工艺参数为反应温度65℃，反应时间3h，固体催化剂投入量4％，醇油摩尔比6∶1，转化率达到91.2％。

In the part of isobutylene producing HMT, through single-factor-experiments , the best reaction condition was found as : the quantity of aluminum chloride was about 4g; the drop-wise time was about 60 min; the keeping reaction time was about 3 hours and in such a condition , the yield of reaction was 86%.

由新己烯合成HMT反应中，通过单因素优化实验，确定较好的反应条件为：三氯化铝用量为4g左右，反应时间定为60分钟左右，滴加时间确定为3小时左右，此时反应收率为86％。

However, when reaction time is fixed, this system can follow Lambert-Beer Law within visible spectrum. Furthermore, it can not be affected by temperature. Based on these findings, CTAB Turbidness Method, a quick method to determine hyaluronic acid contents in fermentation broth is established.

研究表明，随着反应时间延长，反应体系的吸光度逐渐升高，但当反应时间固定后，在可见光区反应体系能较好的遵循朗伯－彼尔定律，并且不受温度的影响。

When the causticization time was longer than 120min and higher than 80℃ with 1.1:1 of stoichiometric ratio, and the precipitation was longer than 30min at 80℃ with n:n(Na2S) being 1.45:1, the NaOH concentration after reviving was denser than 8%, and the revived caustic approximately had the same physical property and adsorption of CO2 as the new caustic.

结果表明：苛化反应温度大于80℃，反应时间超过120 min，n：n(Na2CO3)为1.1：1， CuO沉淀反应温度为80℃，反应时间30 min，n：n(Na2S)为1.45：1等条件下，再生后的NaOH含量可在8%以上，并且再生碱液的物性以及再生碱液对CO2吸收速率上与新鲜碱基本相同。

Prolonging nitration time and increasing reaction temperature would promote the formation of dinitro products while shortening the nitration time and decreasing reaction temperature would promote the formation of mono-nitro products.

延长反应时间和提高反应温度有利于二硝化产物的形成，缩短反应时间和降低反应温度有利于单硝化产物的形成。

The optimum reaction condition was as follows: catalyst dosage=4.3% of the amount of ethanediol,reaction time 50 min.1,4-dioxane yield of 84.82% was obtained under the optimum condition.

考察了催化剂用量、反应时间和反应温度等因素对收率的影响，得出最佳反应条件：催化剂用量为乙二醇质量的4.3%，反应时间50 min，收率可达84.82%。

A new fullerene derivative containing energy-producing groups was prepared, and the reaction conditions affecting the yield were studied by the kroenecker method. The optimal reaction conditions with a 53.5% yield (based on consumed C60) are: 1:3:6 of molar ratio of C60 , o–nitrobenzaldehyde and sarcosine , 55℃ of reaction temperature, 12 h of reaction time, 40mL of toluene solvent.

利用N-甲基甘氨酸、邻-硝基苯甲醛和C60反应，合成分离出了含有硝基的新型富勒烯吡咯烷衍生物，通过正交试验对其工艺条件进行了研究，探讨了反应物剂量比、温度、时间和溶剂体积对产物产率的影响，得到了合成产物的最佳工艺条件：反应物剂量比为1：3：6、温度为55℃、反应时间为12h、溶剂甲苯体积为40mL，此时产物产率可达到53.5%（以消耗的C60计）。

The reaction temperature and reactants concentration have important influence on the morphologies of the products.

反应温度和反应物浓度对产物的形貌影响较大，反应时间对产物的形貌影响不大，但随着反应时间的延长，产物的粒径有增大的趋势。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。