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In this paper,2,2-dimethylolbutyraldehyde was synthesized through the acetal reaction of formaldehyde and butyraldehyde,using phosphomolybstic acid as catalyst.

研究了磷钼酸对此缩醛反应的催化反应活性,以及催化剂的用量、反应物配比、反应时间等因素对反应产物收率的影响,确定了最佳催化条件。

Decided relatively the craft condition of beautiful: IA occupies total monomer rub Er mark is 22%, 6.67% what cross ammonium sulphate dosage to be total monomer quality, reaction temperature ℃ of 80 ℃~85, acrylic acid and the drop that cross ammonium sulphate add time to be 2.5 H, heat preservation time is 3.5 H, total reaction time is 6 H.

确定了较佳的工艺条件:IA占总单体的摩尔分数为22%,过硫酸铵用量为总单体质量的6.67%,反应温度80℃~85℃,丙烯酸和过硫酸铵的滴加时间为2.5 h,保温时间为3.5 h,总反应时间为6 h。

The effects of acidity, reaction temperature, feeding mode, and rotational speed of the stirrer on the particle size of AC blowing agent were studied. The optimal conditions were obtained as follows: the catalyst composed with m:m(V2O5)=1:1 equal to 1%-2% ratio of the reagent''s mass,reagent reacts at 50℃ under pH=3-4 for 25min with 350~360r/min of the stirrer speed, and the NaClO3 solution must be added from burette.

研究了酸度、反应温度、加料方式、搅拌器的转速对AC发泡剂粒径的影响,最佳工艺条件为:催化剂m:m(V2O5)=1:1的质量约为反应物质量的1%~2%,反应体系的pH值3~4,反应温度控制在50℃左右,氯酸钠溶液(质量分数20%)采用通管滴加的方法加入,整个反应时间约为25min,搅拌器的转速一般控制在350~360r/min。

The effect of the mole ratio reactant, reaction temperature, reaction time , catalyzer on the each reaction were studied.

研究反应物配比、反应温度、反应时间、催化剂用量对各步反应的影响,得到最佳反应条件。

The mechanism of modified Catalysts treating leachate through microwave catalytic oxidation showed that, for those rich in granular organic matters, microwave catalytic oxidation attains good pretreatment effect, while for those rich in dissolved organic matter, the effluent attained the municipal wastewater effluent standardsⅢafter treated; Molecular weigh cutting experiments showed that the removal efficiency of organic matter changes disproportionally with different molecular weight.

单目标物质催化剂的机理分析表明,以空气为氧化剂时,Ni-O/CeO_2催化剂的催化效能高于以Fe-O/CeO_2催化剂的催化效能;以H_2O_2为氧化剂以Fe-O/CeO_2催化剂的催化效能高于Ni-O/CeO_2催化剂的催化效能;微波催化氧化反应与常温常压催化氧化反应和水浴催化氧化反应相比大大缩短了反应时间、提高了反应效率。

Reaction temperature, reaction time and different distillate oil on the properties of petroleum sulfonate were studied.

本文以发烟硫酸和三氧化硫作为磺化剂,选用重烷基苯或石油馏分油,在不同的工艺条件下进行磺化反应,摸索了反应物配比、反应温度、反应时间和不同原料等条件对合成产物的性能影响,得出反应物配比是影响磺化收率的重要因素。

The reaction time, reaction temperature and catalyst influencing on esterification were investigated, and the acid value, flashing point and other properties were determined.

考察了反应时间、反应温度、催化剂等反应条件对酯化反应的影响,并对增塑剂的酸值、闪点及其他主要性能指标进行了测定,改进了酯化反应工艺条件,讨论了样品色泽、酸值及闪点的影响因素。

The components of the catalyst are sulfurated more completely with a longer reaction time. But the catalyst congregates into a large volume ball with a low BET surface area after a certain reaction. So the best range of reaction time is from 60 to 90 minutes.

研究发现,虽然硫化时间的延长可提高催化剂中金属组分的硫化物含量,但超过一定反应时间可导致硫化物过度结晶聚集,颗粒度增大,比表面下降,较佳的反应时间为60~90 min。

In this paper, aging time of alkali cellulose was confirmed by researching the effect of aging time of alkali cellulose to its ability of withstanding alkali; The effect of temperature, the mass ratio of intermediate to cellulose, time, NaOH concentration on the mass and capacity of product.

研究了碱纤维的老化时间对抗碱能力的影响,确定了碱纤维的老化时间;研究了氢氧化钠的用量、中间体与纤维素的质量比、反应温度和反应时间对产物质量和产物交换容量的影响,并用红外光谱对产物的结构进行了表征。

All subjects performed eight times of grand battement in Chinese dance and scored by professional dancer to define the esthetics score of this technique. Results: The dominant side exhibited shorter reaction time than non-dominant side in paraspinatus muscles and gluteus muscles, high level group showed longer muscular activity and shorter resting time than lower level group, which were observed by electromyography.

结果发现惯用侧竖脊肌、臀大肌反应时间大於非惯用侧;高表现群总肌电讯号作用时间及二分之一最大强度肌电作用期间皆显著大於低表现群;高表现群之无肌电讯号反应时间显著小於低表现群。

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Chrysanthemum of 10 thousand birthday is lax to edaphic requirement, with the arenaceous qualitative loam with fecund, good drainage had better.

万寿菊对土壤要求不严,以肥沃。排水良好的砂质壤土为好。

He unstepped the mast and furled the sail and tied it.

他拔下桅杆,把帆卷起,系住。

Therefore, positively advances the interest rate marketability reform is one of current our country finance reform important tasks.

因此,积极推进利率市场化改革是当前我国金融改革的重要任务之一。