反应时间

The yield was 84%. With OP-10, NPE as the the catalyzer for the diazo reaction, the use of hydrolyzed propenenitrile instead of propenoic acid, and OP-10 as the catalyzers of the aminate reaction, these experiments showed the feasibility of industralization, due to the much reduced costs, shortened reaction time and a higher yield.

采用壬基酚聚氧乙烯醚（OP-10）、萘磺酸甲醛缩合物作重氮化反应催化剂，丙烯腈加成、水解替代丙烯酸，OP-10做氨化反应催化剂，通过四因子三水平正交试验法实验，得到较佳反应参数，反应时间、收率、成本都大大降低，适宜工业化生产。

The corresponding conditions were atmospherically react 3.5 h with heating up temperature 383 K, n/n=8 and n/n=0.08. The conversion of HDA was 100% with 91.24% yield of HDU-M.

Zr(NO3)4*5H2O可以有效抑制甲基化副反应，是活性最佳的金属含氧酸盐催化剂，对应工艺条件为：加热温度 383 K，反应时间 3.5 h，n/n=8，nCat。

N,N′-Disubstituted ureas,used as intermediates for synthesis of pesticides,resin precursors and carbamates,were synthesized from carbon dioxide and primary amines(namely n-propylamine,n-butylamine,n-amylamine,n-hexylamine,benzylamine and aniline) over organic base catalysts.

以有机碱为催化剂，CO2与伯胺反应合成了N，N′-二取代脲；考察了有机碱种类、伯胺碳链长度、反应温度、CO2压力、反应时间、催化剂用量对合成反应的影响。

For the purpose of research on relationship between liquid crystal phenomena and blood compatibility, the propionic, n-butyric esters of hydroxypropyl cellulose were prepared with hydroxypropyl cellulose and propionyl chloride/ butyryl chloride. The reaction conditions and phase behavior have been studied. The results show that the reaction time, temperature and amount of propionyl chloride have effect on content of propionyl, and the amount of proionyl chlorideis more obvious than the other factors.

液晶态的血液相容性是目前抗凝血材料研究的一个新领域，本文是在一系列液晶态材料血液相容性研究的基础上以羟丙基纤维素和丙酰氯为原料合成羟丙基纤维素丙酸酯和羟丙基纤维素丁酸酯两种液晶高分子化合物，并对其合成条件和相变行为进行了研究，结果表明：反应时间、反应温度和酰氯的用量均对产物中的酰基含量有影响，其中以酰氯用量影响最为明显。

The result shows that the best reaction conditions for synthesizing CMC with a high degree of substitution (1.68) are that the ratio of chitosan to sodium chloroacetate is 1:5, reaction temperature is 90℃, reaction time is 5h, and the amount of catalyst is 3%.

研究了投料比、反应温度、反应时间、催化剂等单因素对取代度的影响，合成高取代度的最佳反应条件为m：m=1：5、温度90℃、时间5h、催化剂量为3%，可制得取代度为1.68的羧甲基壳聚糖。

As concerning synthesis of 2-ethylhexyl chloroacetate, effects of catalyst dosage, molar ratio of 2-ethylhexanol to chloroacetic acid, reaction time, dosage of water entrainer on esterification rate were studied.

将此固体超强酸酯用于氯乙酸和异辛醇合成氯乙酸异辛酯的酯化反应，考察了异辛醇和氯乙酸的摩尔比、催化剂用量、反应时间、带水剂环己烷的用量对酯化反应的影响。

In acetic acid and using cobaltous acetate as catalyst m-chlorobenzoic acid was synthesized by the reaction of m-chlorotoluene with oxygen.

在醋酸溶液中，醋酸钴为催化剂，以间氯甲苯、氧气为原料合成间氯苯甲酸，分别研究了反应温度、反应时间、原料配比、催化剂的用量等条件对合成反应的影响，确定了最佳工艺条件。

The factors affect on the degree of substitution of product, yield and apparent viscosity, such as the mol rates of EPTAC with -NH2, reaction temperature, reaction time and the content of water in system have been discussed in detail. FTIR spectrometer and UV spectrometer are used to characterize the structure of the derivative and it is proved that substitution reaction mainly occurs on the -N element .The particle size and morphology of chitosan and quantemary ammonium salt of chitosan are analysised by comparing photos of their scanning electron microscope. The degree of substitution of HACC is determined by acid -base conductometric titration. An error in current formula of DS has pointed out and a correct formula has presented.On the base of experience of above experiment, the reaction conditions of HACC were systematically investigated through orthogonal design, and then the best conditions are found. Water-solubility and dependence of pH are studied.

壳聚糖和环氧丙基三甲基氯化铵在异相条件下发生反应，通过单因素实验，制备了一系列不同性能的壳聚糖季铵盐，本文首次详细讨论了反应条件(反应摩尔比、反应时间、反应温度、水含量)对产率及产物性能的影响；用红外光谱和核磁共振对结构进行表征分析时，发现季铵盐阳离子基以N位上取代为主；通过电镜图片对壳聚糖和季铵盐衍生物外观形貌进行对比，采用酸碱电导滴定法测定产物的取代度，并对常用取代度公式做了修正。

The effects of catalyst, deaquation reagent, reaction time and the ratio of raw materials on the reaction were examined.

考察了催化剂、带水剂、反应时间、物料比等因素对反应的影响。

This paper is studied on a new synthesis method of amino-modified organic silicone micro-emulsion of cationic style by one step with a silane-alkyl coupling,3-(2-aminoethyl)-aminopropyl methyl dimethoxy silane while opening-cyclo polymerization of the octa-methyl cyclo tetra siloxane,thus the optimal manufacturing conditions are determined by comparing test of their properties.

采用硅烷偶联剂氨乙基氨丙基甲基二甲氧基硅烷改性，八甲基环四硅氧烷开环聚合，探索一步合成阳离子型氨基改性有机硅微乳新方法，通过其性能测试得出其最佳工艺条件：反应温度：80℃，反应时间：3 h，十六烷基三甲基溴化铵用量：5%，脂肪醇聚氧乙烯醚用量：5%，预乳液滴加时间：2 h。

Some questions asked by the adjudicators in one English Speaking Contest still run upon me very often.

我参加了一场以"我心中的奥运会"为主题的英语演讲竞赛，其间评判提的几个问题时时萦绕我的心头。

He called InTERActive our most profitable release of the year.

他呼吁互动的我们的最有利可图的释放一年。