反应时间

In this paper, 2,2-dimethylolbutyraldehyde was synthesized through the acetal reaction of formaldehyde and butyraldehyde, using silicotungstic acid as catalyst.

通过实验研究了硅钨酸对此羟醛缩合反应的催化效果，研究探讨了硅钨酸对此缩醛反应的催化反应活性，以及催化剂的的用量，反应物配比，反应时间等因素对反应产品收率的影响，确定了最佳催化条件。

In the part of producing TONALIDE, through single-factor-experiments , the highest yield of reaction condition was confirmed as: reaction time about 4 hours; reaction temperature about 20 ; the quantity of chlori-acytyl about 10g; the quantity of aluminum chloride 13-15g and the yield of reaction was as high as 90%.

在TONALIDE的合成部分，通过单因素试验，找到了反应收率最高的反应条件为：反应时间4小时左右；反应温度20℃左右；乙酰氯的用量10g左右；反应中的三氯化铝的用量13～15g，此时反应收率可达90％。

The effect of different reaction conditions,such as catalyst concentration,molar ratio of reactants,reaction temperature,reaction time,on the coupling reaction of trioxane and methyl formate synthesizing methyl glycolate and methyl methoxy acetate using sulfuric acid as catalyst has been studied.Through the analysis for the yield of products and system pressure,and comparison with other different acidity catalysts,we considered that the activation of formaldehyde was the control step of reaction rate to the...

以硫酸为催化剂，研究了三聚甲醛与甲酸甲酯偶联合成乙醇酸甲酯和甲氧基乙酸甲酯的反应中，催化剂浓度、原料配比、反应温度、反应时间等条件对反应过程的影响，通过对产物收率和系统压力变化的分析，并结合与其它不同酸强度催化剂的对比，得到甲醛的活化是偶联反应的速率控制步骤，催化剂的酸强度决定其对甲醛的活化能力，是影响偶联反应的主要因素。

The result shows that the best reaction conditions for synthesizing CMC with a high degree of substitution (1.68) are that the ratio of chitosan to sodium chloroacetate is 1:5, reaction temperature is 90℃, reaction time is 5h, and the amount of catalyst is 3%.

研究了投料比、反应温度、反应时间、催化剂等单因素对取代度的影响，合成高取代度的最佳反应条件为m：m=1：5、温度90℃、时间5h、催化剂量为3%，可制得取代度为1.68的羧甲基壳聚糖。

Synthesis of ethyl chloroacetate with chloroacetic acid and ethanol catalysed by GdCl2-EDTB-H3SiW12O40was investigated.

研究了反应时间、醇酸比、带水剂用量及催化剂用量对杂多酸化合物GdCl2-EDTB-H3SiW12O40催化合成氯乙酸乙酯的影响，确定了最佳反应条件，醇酸摩尔比1.5∶1，带水剂量10mL，催化剂使用量为酸的1.0%，反应时间2.5h

Fumaric acid-containing wastewater was pre-treated by a method of microelectrolysis of iron and carbon , with the reaction time, pH value, temperature and ratio of iron to carbon studied.

采用铁炭微电解法预处理富马酸废水，研究了反应时间、pH值、温度、铁与炭的比例对预处理的影响，试验结果表明：当反应时间180min，铁炭比3∶1，反应温度313K时，CODCr去除率35。

The influence factors such as n/ n,n(H_2O_2)/n,the concentration of hydrogen peroxide,reaction temperature and time were studied to find how they affected the synthesizing of accelerant NOBS adopting hydrogen peroxide oxidation method.

研究了n/n、n(H2O2)/n、双氧水浓度、反应温度和时间对双氧水氧化法合成促进剂 NOBS的影响，通过L16(45)正交实验确定出的最佳合成配方及工艺条件：n/n为7；n(H2O2)/n为1.6；双氧水浓度为12%；反应温度为40℃；反应时间为3h。

The results showed that the addition leading to -2-phenyl-2-(2-vinylpiperidin-1-yl) ethanol 7 could proceed with good diastereoselectivity and excellent yield (95%).(3) The selective N-deprotection of -2-phenyl-2-(2-vinylpiperidin-1-yl) ethanol 2 without affecting the vinyl group in the substrate were untaken.(4) The Zip reaction for the transformation of -1-(3-aminopropyl)-3-methylazecan-2-one 8 to -7-Methyl-1, Sdiaza-cyclotetradecan-6-one 9 were undertaken. The results showed that, under controlled conditions, acceptable yields (43%) could be achieved and racemization can be minimized during the ring expansion reaction.

该合成路线与文献方法相比，反应条件较温和，也缩短了反应时间；(2)哌啶衍生物2与乙烯基格氏试剂进行加成反应的条件和立体选择性，取得了较好的结果（差向异构体比为80：20，产率95％左右）；(3)不饱和哌啶衍生物7在不影响碳碳双键的情况下去除苯基甘氨醇手性辅助基的条件；(4)具有羰基α位手性的氨基酰胺8在不同条件下经Zip重排反应转变为9的反应，控制反应条件，可使反应中消旋化减小到最小的程度。

The results showed that by using ethanol-alkali method to prepare cold-water-soluble starch, the impact of ethanol concentration and reaction time on the solubility of wheat granular cold-water-soluble starch was significant; the appropriate preparation conditions for wheat cold-water-soluble starch was on the reaction temperature of 65℃, ethanol concentration of 80 mL/l00 ml, reaction time of 80 min, alkali concentration of 10 g/100 ml, under this condition the solubility of the product was up to 81.44%.

结果表明：采用乙醇－碱法制备小麦颗粒状冷水可溶淀粉，乙醇体积分数和反应时间对产物溶解度的影响显著；小麦颗粒状冷水可溶淀粉的适宜制备条件为反应温度65℃，乙醇体积分数80%，反应时间为80min，碱浓度10g/100 ml，其溶解度可达81.44%。

CTX ip 0.06 mg/kg, 0.12mg/kg significantly reduced the errors of the mice in Y-Maze test, decreased the mices training times, shorten the escape latency in Shuttle box test. In Step-down test, CTX ip 0.06mg/kg, 0.12mg/kg increased the escape latency and reduced the number of errors, CTX also reduced the searching platform latency and swim path-length in Morris water maze test with mice.

实验发现，CTX能明显增加热刺激引起的疼痛闭值，明显减少醋酸引起的扭体次数，并能显著增加小鼠在Y型迷宫实验中的正确反应次数，减少在穿梭箱实验中小鼠重新训练至学会标准的训练次数及小鼠的反应时间，能增加小鼠在跳台法中的潜伏期，减少错误反应次数，减少小鼠在Morris水迷宫实验中的寻台时间和游泳路程，以上效果均表现出明显的剂量依赖性。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。