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To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

The methodological 2 oxidation 75 μ Mol/L are cobaltic alone or jointly 30, the Rg3 action of 60 μ G/m L is mixed at 24 H of cell of esophagus cancer EC9706 48 H, part fluid of the Qing Dynasty on collection cell education, detect with ELISA law among them hemal endodermis grows factor level, in order to contain RPM I1640 of serum of 10% embryoes ox education radical does blank to contrast.

方法将75μmol/L的二氧化钴单独或联合30、60μg/m l的Rg3功能于食管癌EC9706细胞24 h和48 h，分别收取细胞培养上清液，用ELISA法检测其中血管内皮生长因子水平，以含10%胎牛血清RPM I1640培养基做空白对照。

In addition, there were 140 G + cocci, accounting for 28 %; and 31 mol...

下呼吸道感染仍以 G-杆菌感染为主，但要注意 G+球菌及霉菌感染

In this investigation,the composition of copolymer P(AM- co -NaAMPS) of acrylamide and 2-acrylamido-2-methyl-propanesulfonate sodium has been determined with the aqueous solution of cetyl trimethyl ammonium bromide as titrant at a concentration of 0.001 mol·L-1 by conductometric titration method.

与元素分析进行比较的结果表明，上述复合作用电导滴定法可作为测定水溶性大分子链中磺酸盐单体含量的方便而又准确的方法，而且预计还可用作为测定水溶性大分子链中其它离子性基团含量的简捷方法。

The factors affect on the degree of substitution of product, yield and apparent viscosity, such as the mol rates of EPTAC with -NH2, reaction temperature, reaction time and the content of water in system have been discussed in detail. FTIR spectrometer and UV spectrometer are used to characterize the structure of the derivative and it is proved that substitution reaction mainly occurs on the -N element .The particle size and morphology of chitosan and quantemary ammonium salt of chitosan are analysised by comparing photos of their scanning electron microscope. The degree of substitution of HACC is determined by acid -base conductometric titration. An error in current formula of DS has pointed out and a correct formula has presented.On the base of experience of above experiment, the reaction conditions of HACC were systematically investigated through orthogonal design, and then the best conditions are found. Water-solubility and dependence of pH are studied.

壳聚糖和环氧丙基三甲基氯化铵在异相条件下发生反应，通过单因素实验，制备了一系列不同性能的壳聚糖季铵盐，本文首次详细讨论了反应条件(反应摩尔比、反应时间、反应温度、水含量)对产率及产物性能的影响；用红外光谱和核磁共振对结构进行表征分析时，发现季铵盐阳离子基以N位上取代为主；通过电镜图片对壳聚糖和季铵盐衍生物外观形貌进行对比，采用酸碱电导滴定法测定产物的取代度，并对常用取代度公式做了修正。

Mol/L and calcinations temperature at 500?℃. The solid superacid can be used as catalyst two times in the alkylation of naphthalene, and the total composition of MIPN,DIPN, and TIPN in product is over 98%. When the consumpt...

在催化剂用量为 10 %、反应温度为 160℃、反应时间为 2 5h的条件下连续两次使用SO2 - 4 TiO2 超酸催化萘对丙烯的烷基化反应，产品中一异丙基萘、二异丙基萘、三异丙基萘的总含量大于 98%。

The overall activation energies of crotonic acid, undecylenic acid and oleic acid systems are 118, 122 and 134 kJ/mol, respectively.

反式丁烯酸、10-十一烯酸、油酸接枝ABS树脂的反应活化能分别为：118、122、134kJ／mol。

Grafting degree increased with increasing monomer concentration in acrylic acid and crotonic acid systems. In undecylenic acid and oleic acid systems, grafting degree increased with monomer concentration initially but decreased after monomer concentration reaching at 0.30 mol/L.

丙烯酸、反式丁烯酸体系的接枝率随单体浓度的增加而增大。10-十一烯酸、油酸体系的接枝率初始时随单体浓度的增加而增大，单体浓度超过0.30mol／L后，接枝率降低。

CVB-D+ verapamil group:verapamil of 0.1 μmol/L was added into the bath firstly,10 minues later AP was recorded,then CVB-D of different concentrations (3×10 -8,1×10 -7,3×10 -7,1×10 -6,3×10 -6,1×10 -5)mol/L was added into the bath cumulately and AP was recorded every five minutes.

环维黄杨星D(cyclovirobuxine D ，CVB D)是从黄杨科植物小叶黄杨中提取的甾体生物碱，具有良好的抗心律失常、抗心肌缺血和强心作用，临床上广泛用于治疗心律失常、心绞痛和冠心病[1，2 ] 。

Under the optimum conditions of a cyclopentene amount of 1.0 mol, a molar ratio of cyclopentene to water of 0.25, a reaction temperature of 120 ℃, a reaction time of 4.0 h, a main catalyst dosage of 4.0 g and a cocatalyst dosage of 0.8 g, the yield of cyclopentanol reached 68.6%.

确定适宜的反应条件为：环戊烯1.0 mol，n﹕n=1﹕4，反应温度120 ℃，反应时间4.0 h，硅胶负载铌酸主催化剂用量4.0 g，三（3，6-二氧杂庚基）胺助催化剂0.8 g。在此反应条件下，环戊醇收率68.6%。

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Tara appears in Buddhism, Jainism, and particularly, Tibetan Lamaism, as a complex array of manifestations: goddess of ascetism and mysticism, mother creator, protectress of all humans as they cross the sea of life.

度母出现在佛教，耆那教里面，尤其是西藏的喇嘛教，作为一系列的陈列阵容；神秘的女神，创世之母，人类横过生命之海洋的女性保护者。