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Methods A mixture of 10 mol/L potassium dihydrogen phosphate solution and acetonitrile(60 ∶ 40) was used as the mobile phase.

方法以乙腈-10mmol/L磷酸二氢钾(40∶60)为流动相，炔雌醇为内标，血浆样品经乙酸乙酯萃取。

Methods Using orthogonal experimental design L16(4^5, two factorial experiments were designed to explore the influence of four dosage levels of vitamin D30, 10^(-4,10^(-7),10^(-10)mol/L and four different stages (proestrous, estmus, postestrous, dioestrous)of estrous cycle on steroidogenesis in the ovary.

采用正交表L16(4^5)设计实验，研究VD3（10^(-4)， 10^(-7)， 10^(-10)mol/L在动情周期的4个阶段（动情前期、动情期、动情后期、动情间期）对卵巢切碎组织分泌E2和P4的影响。

By experiment we found that the reaction of aldehydes and nitromethane can proceed smoothly in the presence of a catalytic amount of Disodium Binaphtholate (3 mol %),and obtain a corresponding rate of product up to 100%.

通过筛选，我们发现在催化剂量的联二萘酚双钠盐(3 mol%)存在下，henry反应能够快速的进行，产率高达100%。

Based on the development of homogeneous gold complex catalyst, the polymer immobilized nano-gold catalyst was also prepared and used for oxidative carbonylation of amines or activation of carbon dioxide to carbamates and disubstituted ureas without addition of any co-catalyst and dehydration agents with greatly enhanced catalytic activity (TOF≈3000mol/mol/h).

同时，纳米金可以催化活化二氧化碳与脂肪族胺反应制备二取代脲，避免了传统上二氧化碳活化所大量使用的脱水剂，是当前文献报道最高效的胺与二氧化碳反应的催化剂体系（TOF≈3000mol/mol/h）。

The results showed that 1,5-naphthalene disulfonic acid could be degradated effectively by the catalytic supercritical water oxidation process,the removal rate of COD reached 98% or even above;the removal rate of COD increased with the increasing of temperature and residence time,the orders of catalytic oxidation degradation reaction of 1,5-naphthalene disulfonic acid to COD and oxygen in supereritieal water were 0.89 and 0.28 respectively,and the activation energy was 56.8 kJ/mol.

Ding等[3]研究了NH3在MnO2/CeO2催化剂作用下在超临界水中的降解情况；Savage[4]简述了在超临界水中以CARULIFE 150、TiO2、MnO2、CuO为催化剂，对苯酚进行了超临界水氧化机理研究情况，但迄今为止涉及催化超临界水氧化的反应动力学的研究还不多。萘系有机污染物是印染

The research results obtained showed that, sulphonating extent of synthetic starch xanthate was high, under room temperature, time 120 minutes, mol ratio of starch, sodium hydroxide and disulphide being 10 : 4 : 3, It was to say that sulphur content and supplent extent were high.

研究结果表明，原料配比为：淀粉：NaOH：CS_2为10：4：3，反应温度为室温，黄化反应时间为120min，合成DX的黄原酸化程度高，即产品含硫量和取代度高。

The influences of the composition of the catalysts, reaction temperature, space velocity and mol ratio of benzene and dodecylene on the conversion of dodecylene and the selectivity were researched.

在微型液相固定床反应器上考察了反应漫度，空速，磷钨酸负载量以及苯烯摩尔比等反应条件对催化剂性能的影响。

The plasmid DNA bands were detected clearly by agarose-EtBr gel electrophore sis.Two forms of plasmid DNA molecules,namely covalently closed circular DNA mol e-cules and open circular DNA molecules,were observed under electron microscope.

用琼脂糖-溴化乙锭凝胶电泳分析在两株菌的DNA中鉴别出明显的质粒带，用电镜方法在两株菌的DNA制剂中均观察到共价闭合超螺旋和开放型环状两种构型的DNA分子。

Take Pb〓 as an example, its detection limit is 8×10〓mol/L. The research on mechanism of this method shows that these achievements was caused by the characteristics of silver disc electroxidation and electroreduction and ACOC.

对该法的机理做了较深入的探讨，表明该方法灵敏度高、稳定性重现性好的原因是银盘电极的氧化还原性质和交流示波计时电位法的特点共同所致。

Cm^2 of nitromethane electroreduction appeared at -0.89 V and the reaction activation energy was 12.3 kJ/mol.

SCE时，硝基甲烷还原为甲基羟胺的电流达14.9mA/平方公分，其反应表观活化能为12.3kJ/mol。

This paper designs the communication system of radio telescope FAST.

针对500m口径球面射电望远镜FAST分布式控制系统的特点完成了其通信系统的设计。

Political sheep's step-by-step a large number of fossils unearthed in the county soil Ma Ali after rural village in the middle of sallow pelitic siltstone.

步氏和政羊化石大量出土于广河县阿力麻土乡后山村，产于灰黄色泥质粉砂岩中。