丁酮

Methods: Based on national standard, detected n-hexane, benzene, toluene, dimethylbenzene, ethyl acetate, butyl acetate and butanone in 450 factories.

根据中华人民共和国国家标准，对昆山市的450家接触正己烷、苯、甲苯、二甲苯、乙酸乙酯、乙酸丁酯、丁酮7种有机物的企业车间空气进行采样检测。

Results: The good linear range of method was 10 to 1000μg/ml (T=0.9999) with the correlation coeffivient of 0.9999, and the limit concentration in air was 0.2 mg/m^3 with the average relative standard deviation less than 5%(n=6). The average sampling rate ranged from 96.6 to 100%, and the breakthrough capacity of l00mg activated charcoal was 4.7mg. The average desorption rate was 97.6%, and mesityl oxide absorped in activated charcoal tube was stable for 7 days and can be detected accurately with other gas coexisting in the air of workplace.

结果：异亚丙基丙酮浓度在10~1000μg/ml内呈良好线性关系，相关系数0.9999，最低检出浓度为0.2mg/立方公尺，相对标准偏差＜5%(n=6)；气体采样效率≥96.6%，100mg活性炭对异亚丙基丙酮的穿透容量为4.7mg，平均解吸效率97.6%；活性炭样品室温下可保存7天；丙酮、丁酮、异佛尔酮、苯、甲苯、二甲苯等共存物不干扰测定。

There is a parallel shift of the dose-response curve of the ligand to left. Present study suggests that there may be an internal molecular/chemistry interaction between quinolones and BPAA, producing a new structure which has a high affinity on the GABAA receptor sites.

本研究直接反映了联苯丁酮酸和BPAA与喹诺酮类药物在体内与GABAA受体的相互作用，其作用机制可能是两种药物发生了化学/分子作用，形成一种与GABAA受体有着极高亲和力的新结构。

Major procurement of goods: a three-chlorosilanes, dichloromethane, AE activity ester, 3-iodine Silane, special acid, pentyl chloride, triethylamine, thiadiazole, tetrazolylazo acid, 2 - Acetamide, tetrahydrofuran, the four-guanidine, isopropanol, five phosphorus trichloride, sodium vary bitter, acid, sodium phenylacetate, 6-2 silicon n-amine, Ethylacetoacetate , Methyl isobutyl ketone, potassium dihydrogen phosphate, aluminium oxide, DL methionine, N, N-dimethylaniline, NN-diethyl aniline, 4 sodium EDTA, Anhydrous sodium sulfate, ammonium sulfate, potassium sulfate, sodium acetate, sodium carbonate, DMC, formic acid, sodium chloride medicinal, oxalate, protopine, acetone, alcohol, acetic acid, vinegar Ethyl, butyl acetate, methanol, ethanol (anhydrous, industrial, medicinal), formaldehyde, Ye Jian (30%), hydrochloride (industrial-grade, refined grade, reagent level), sulfate (98%), Ammonia, calcium carbonate, chlorine dioxide, 6 - APA ,7-ACA ,7-ADCA ,7-ANCA, sulbactam, ceftazidime activity ester, Deng salt (hydroxymethyl-K, acid precursors Potassium, sodium dihydrogen methyl), resin, the enzyme, water treatment agent, Xiao Mo agent, demulsifier, flocculants, activated carbon, all kinds of medicinal materials, All kinds of additives

三甲基一氯硅烷、二氯甲烷、AE活性酯、三甲基碘硅烷、特戊酸、特戊酰氯、三乙胺、噻二唑、四氮唑乙酸、二甲基乙酰胺、四氢呋喃、四甲基胍、异丙醇、五氯化磷、异辛酸钠、苯乙酸、苯乙酸钠、六甲基二硅胺烷、乙酰乙酸乙酯、甲基异丁酮、磷酸二氢钾、三氧化二铝、DL蛋氨酸、N，N-二甲基苯胺、NN-二乙基苯胺、乙二胺四乙酸四钠、无水硫酸钠、硫酸铵、硫酸钾、醋酸钠、碳酸钠、碳酸二甲酯、甲酸、药用氯化钠、草酸、片碱、丙酮、正丁醇、冰醋酸、醋酸乙酯、醋酸丁酯、甲醇、乙醇、甲醛、液碱（30％）、盐酸（工业级、精制级、试剂级）、硫酸（98％）、氨水、碳酸钙、二氧化氯、6－APA、7－ACA、7－ADCA 、7－ANCA、舒巴坦、头孢他啶活性酯、邓盐(羟甲基钾、前体酸钾、二氢甲基钠)、树脂、生物酶、水处理剂、消沫剂、破乳剂、絮凝剂、活性碳、各种药用辅料、各种添加剂

In this paper, the synthesis ways and applications of 4,5-dimethyl-l,3-dioxolen -2-one were introduced. An appropriate way synthesizing DMDO from acetoin via acylation, cyclization and dehydrochlorination was selected. The influences of various process conditions on the reaction were studied in detail, and the optimum process conditions were obtained by single factor experiments.

本文介绍了医药中间体4，5-二甲基-1，3-二氧杂环戊烯-2-酮的应用情况和合成路线，选择了适于工业化生产的工艺路线，即采用羟基丁酮为原料，经酰化、环合和脱氯化氢等步骤合成DMDO，并采用单因素试验法详细研究了各项工艺条件对反应结果的影响规律，确定了优化工艺条件。

In the presence of ethanol- HCl solution, arylamine-HCl and w=37% aqueous formaldehyde solution or the condensation product of arylamine and formaldehyde are directly reacted with ethyl 3-oxo-2-phenylmethylenebutyrate to form l-aryl-2-phenyl-3-carbethoxy-4-piperidone.

2－苯亚甲基－3－丁酮酸乙酯与芳香胺和w＝37％甲醛水溶液或芳胺和甲醛的缩合物在氯化氢－无水乙醇存在下可直接发生的Mannich反应，得到1－对位取代芳基－2－苯基－3－羰乙氧基－哌啶－4－酮。

Amination reaction was carried out at temperature of 90℃ to 150℃ for 2h to 10h and then ashless dispersant of polyisobutylene succinimide would be obtained after dehydration with the operations of vacuum distillation and filtration.

结果发现，实验在N_2保护下进行，BPO／PIB质量比为0.035，MA／PIB摩尔比为1.3，反应温度为150℃，反应时间为12h，搅拌速率为250rpm，引发剂过氧化苯甲酰以丁酮为溶剂分六次，时间间隔为30分钟，均量地加入反应器时，烃化反应物聚异丁烯的转化率最高。

By using gas chromatography technique nine kinds of fragrance components(acetic aldehyde,ethyl acetate,ethanol,propyl acetate,3-hydroxy-2-butanone,acetic acid,furfural,metacetonic acid,2,3-butylene glycol)were measured quantitatively in different kinds of Shanxi overmature vinegar and the other kinds of vinegar.

应用气相色谱方法对山西老陈醋和其他种类醋的9种香气成分(乙醛、乙酸乙酯、乙醇、乙酸丙酯、3-羟基-2-丁酮、乙酸、糖醛、丙酸、2，3-丁二醇)进行了定性、定量测定，并用聚类分析、模糊综合评判、方差分析、回归分析的方法对实验结果进行了数理分析。

Administrative control: Carries on the appraisal to the entire factory clean water used, the control uses the water volume The formulation procedure guarantees the clean water used at will not to discharge The factory will have the latent risk after the appraisal the source of pollution to divide into two parts, after because the factory all cleans waste water content will have the harm matter all will be same:Methyl ethyl ketone, peroxidation armor second grade alkone, styrene, MMA, therefore will possess the washes with pool and washes the eye to treat as a source of pollution, and the suggestion will make the improvement with the identical plan.

行政控制：对全厂清洁用水进行评估，控制用水量。制定程序以确保清洁用水不被随意排放。工厂通过评估后将有潜在风险的污染源分为两个部分，因为工厂所有的清洗后的废水内含有的危害物质都是一样的：丁酮、过氧化甲乙酮、苯乙烯、MMA，所以将所有清洗池和洗眼器当作一个污染源，并建议用同一个方案去进行改进。

The relative contents of hexanal, heptaldehyde, 2-butanone, hexanoic acid, decrease in silkies on feeding stuff, The relative contents of acetaldehyde, 2-octanone decrease in silkies on feeding medlar, in primary volatile compounds.

经分析比较：枸杞园散养乌骨鸡肉中，醛类物质的相对含量最大，占48.82%，是饲料笼养的1.27倍。在主要挥发性物质中，己醛、庚醛、2-丁酮、己酸的相对含量饲料笼养乌骨鸡较枸杞园散养乌骨鸡减少，乙醛和2-辛酮的相对含量增加。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。