丁酮

The quantity of catalyst was equal to 0.6% of feedstocks,the reaction temperature was 78～110 ℃,and the reaction time was 45 min. The test results have shown that H_4SiW_(12-O_(40)/MCM-48 is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal with its yield reaching over 91.9%.

实验表明：H4SiW12O40/MCM-48是合成丁酮-1，2-丙二醇缩酮的良好催化剂，在n∶n(1，2-丙二醇)=1∶1.6，催化剂用量为反应物料总质量的0.6%，环己烷为带水剂，反应时间45 min的优化条件下，丁酮-1，2-丙二醇缩酮的收率可达91.9%。

Sodium bisulfate is an excellent catalyst for synthesizing butanone 1,2-propan.

以一水合硫酸氢钠为多相催化剂，由丁酮和1，2-丙二醇反应合成了丁酮1，2-丙二醇缩酮。

The acetalization and ketalization of various aldehydes and ketones with catechol by using HY zeolite as catalyst were studied.

研究了 HY分子筛催化邻苯二酚与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正己醛、正辛醛、苯甲醛、二苯甲酮等十余种醛的缩合反应。

The acetalization and ketalization of various aldehydes and ketones with glycerol by using KHSO4 as catalyst were studied. Effect of reaction time, mole ratio of reactants and amount of catalyst on yield of acetals were investigated.

研究了在KHSO4催化下，丙三醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

The acetalization and ketalization of various aldehydes and ketones with glycols using FeCl3 as catalyst were studied. The effects of reaction time, mole ratio of reactants and amount of catalyst on the yield of acetals were investigated.

研究了在FeCl3催化下，乙二醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

A Product main business categories: chemical solvents white oil, toluene, xylene, durene, valitin water, acetate, D resin, acetone, butanone, cyclohexanone , anti-white water, dichloromethane, trichloroethane, trichlorethylene, loose water-saving washing network water, open water, wash water, and days that water, rust agent, to water-logging, washing machine water, decontamination water, n-butyl alcohol, isopropyl alcohol, ethanol, industrial alcohol, car-washing water, washing machine water, clean lines of water, cleaning machine water, fire water, paint remover, fungicides, antifreeze water, chloroform, grinding fluid , diluent, release agent, dehydration agent substantial industrial solvents.

主要经营产品 A类：化工溶剂白电油、甲苯、二甲苯、四甲苯、凡立水、乙脂、丁脂、丙酮、丁酮、环己酮、防白水、二氯甲烷、三氯乙烷、三氯乙烯、松节水、洗网水、开油水、洗面水、天那水、除锈剂、去渍水、洗枪水、去污水、正丁醇、异丙醇、乙醇、工业酒精、洗车水、洗机水、抹线水、抹机水、火水、脱漆剂、杀菌剂、防冻水、哥罗仿、研磨液、稀释剂、脱模剂、脱水剂等大量工业溶剂。

The quantity of catalyst was equal to 0.6% of feedstocks,the reaction temperature was 78～110 ℃,and the reaction time was 45 min. The test results have shown thatH_4SiW_(12-O_(40)/MCM-48 is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal with its yield reaching over 91.9%.

实验表明：H4SiW12O40/MCM-48是合成丁酮-1，2-丙二醇缩酮的良好催化剂，在n∶n(1，2-丙二醇)=1∶1.6，催化剂用量为反应物料总质量的0.6%，环己烷为带水剂，反应时间45 min的优化条件下，丁酮-1，2-丙二醇缩酮的收率可达91.9%。

Two series of polyurethane acrylate grafted acrylic resins (Acr-g-TPU-PETA and Acr-gPPU-PETA) self-emulsifying systems are obtained by grafting -NCO group modified polyurethane acrylates with acrylic copolymer prepared from n-butyl acrylate, styrene,βhydroxyethyl methacrylate and acrylic acid The self-emulsifying systems showed Newtonian fluidity with viscosity closed to that of water, the solid contents were around 30% The T〓 of 15～4℃ for dried film before photocuring favored film formation at room temperature DSC and DMA results showed that PU-PETA is compatible with acrylic resin in the grafted resin The TG and dTG curves for Acr-g-PU-PETA samples were substantially different from the corresponding blends, and the brodened dTG peaks for photocured grafted resin suggest that there might be multiple interactions among chain segments The photocued film of the grafted resins self-emulsifying system exhibited good overall properties with polyurethane acrylate grafts ranging from 30% to 50%, and Acr-g-TPU-PETA series showed better properties than Acr-gPPU-PETA series The adhesion of the photocured film was 1～2 grade, impact strength was 50kg-cm and flexibility was 1mm The Shore hardness and the adhesion of the film decreased markedly if PETA was replaced by HEMA as photoactive group due to the lower C=C double bond content in the grafted resin The polyhydroxy amine-linked thioxanthones photoinitiators can be evenly dispersed in self-emulsifying system without color spot appearing in the dried film The films photocured with IV〓～IV〓 generally exhibited higher Shore hardness, gloss and solventresistance than that cured with Irgacure 2959 and did not induce the rusting of the iron substrate Pigmenting with titanium oxide had no effect on the photocuring The polyhydroxy amine-linked thioxanthone IV〓 and IV〓 can be new candidates for the formulation of titanium oxide pigmented photocurable water-borne coatings for their pale-yellow appearance and slight interference with the color of the coatings WB 4759 with high water-solubility coalesced and separated from the dried resin film, and even induced the rusting of iron substrate.

以丙烯酸丁酯，甲基丙烯酸-β-羟乙酯，丙烯酸及苯乙烯合成厂丙烯酸共聚树脂，并与含-NCO端基的聚氨酯丙烯酸酯接枝反应，经水性化后，得到两个系列（Acr-g-TPU-PETA和Acr-g-PPU-PETA）各5个不同配比的丙烯酸树脂接枝聚氨酯丙烯酸酯自乳化体系，粘度与水相近，为牛顿流体，固含量30％左右。光固化前干燥涂膜的玻璃化转变温度在-15℃～4℃之间，有利于室温下成膜。DSC及DMA谱表明两种树脂基本相容。Acr-g-PU-PETA的热失重行为明显不同于共混材料，接枝样dTG峰明显宽化，表明接枝样中链段之间的相互作刚有多重性，丙烯酸树脂与聚氨酯之间有一定的相容性。接枝树脂自乳化体系光固化涂层的综合性能以聚氨酯丙烯酸酯成分为50％～30％者相对较好，且以Acr-g-TPU-PETA系列更理想。光固化膜的附着力为1～2级，冲击强度为50kg·cm，柔软性多为1mm。以HEMA代替PETA作为接枝树脂的活性基团，碳—碳双键密度太低，光固化膜交联点太少，硬度和附着力均较差。多羟基胺连硫杂蒽酮光引发剂能均匀分散于树脂自乳化体系和接枝树脂干膜中，不出现色斑，光固化膜肖氏硬度一般高于以Irgacure 2959为光引发剂的光固化膜，光泽度及耐丁酮溶剂性能均有所提高，不会诱导铁基生锈，钛白着色对光固化结果几乎没有影响。本论文所合成的多羟基胺连硫杂蒽酮光引发剂IV〓与IV〓为浅黄色，对光固化涂层的颜色干扰较小，为配制钛白着色光固化水性涂料提供了新的光引发剂。水溶性太强的WB 4759在干膜中易聚结析出，且对所附着的铁基有诱导锈蚀作用。

Determination of methyl ethyl ketone and sec-butanol by gas chromatography was reported.

丁酮在合成抗氧防胶剂N，N'-二仲丁基对苯二胺过程中是过量的，回收利用可以节省不少成本，但其可以加氢生成仲丁醇，有必要测定回收丁酮中仲丁醇的含量。

Alcohols, ketones, esters, alcohols, ethers common media are methanol, ethanol, ethylene glycol, propanol, etc., ketones medium with acetone, methyl ethyl ketone, etc., there are a variety of methyl esters of medium, ethyl ester, ether medium with ether, ethyl ether, butyl ether, etc., they basically did not corrosive materials can be used for the specific use of the property should also be under the media and related requirements to make reasonable choices.

醇类、酮类、酯类、醚类常见的醇类介质有甲醇、乙醇、乙二醇、丙醇等，酮类介质有丙酮、丁酮等，酯类介质有各种甲酯、乙酯等，醚类介质有甲醚、乙醚、丁醚等，它们基本没有腐蚀性，常用材料均可适用，具体选用时还应根据介质的属性和相关要求做出合理选择。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。