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Result: Eight compounds were isolated and they were identified as β-sitosterol (1), succinic acid (2), luteolin-7-O-β-D-glucoside (3), uracil (4), apigenin (5), chrysoeriol (6), chrysoeriol-7-O-β-D-glucoside (7), and apigenin-7-O-β-D-glucoside (8). Conclusion: Compound 4-8 were isolated from L.

结果：从藏药短管兔耳草醋酸乙酯提取物中分离得到8个化合物，经鉴定分别为β-谷甾醇（1），琥珀酸（2），木樨草素-7-O-β-D-葡萄糖苷（3），尿嘧啶（4），芹菜素（5），柯伊利素（6），柯伊利素-7-O-β-D-葡萄糖苷（7）和芹菜素-7-O-β-D-葡萄糖苷（8）。

In the passivated REBAR electrode surface formed by ORCs the grain observed from AFM examination is composed of γ-Fe〓O〓 and Fe〓O〓 0 At+0.7V, the passive film on REBAR electrode formed by single-step polarization is composed of Fe (Ⅲ oxide highly doped by Fe〓. In some areas, small γ-Fe〓O〓 particals or some polymeric structure which contains dioxy and dihydroxy bridging bonds between the iron atoms may also exist in the other region.

通过AFM实验观察到的钢筋电极经循环电位扫描至+0.7V形成的钝化膜中具有的结晶颗粒主要由γ-Fe〓O〓和Fe〓O〓·yH〓O0 阶跃电位形成的钢筋钝化膜在+0.7V下主要是由掺杂了大量Fe〓的三价铁氧化物构成，在某些微小的区域可能存在γ-Fe〓O〓微晶，而在另外一些区域则具有聚合物膜的结构。

National Day Golden Week holidays, Mid-Levels Yong Jing Yuan will launch 200 sets of fine grand ex gratia units will also be introduced flatly price concessionary units, including 183 foreign and pursued the age-in-O sky gardens, 270 degrees, 102 master of the Housing Great Piaochuang O 3 and 85-O of the Housing tight Xiao San Housing units.

国庆黄金周期间，半山雍景苑将隆重推出200套精品特惠单位，此外，还将推出一口价特惠单位，包括倍受追捧的183？O空中花园老少居、270度主人房大飘窗的102？O三房和85？O布局紧凑的小三房单元。

Research results of phase equilibrium for the KOH—K〓CrO〓—H〓O system, the KOH—KAlO〓—H〓O system and the KOH—K〓CrO〓—KAlO〓—H〓O system revealed that lower concentration of KOH was beneficial for the crystallization of KAlO〓, and within a certain range, higher concentration of KOH was favorable for the crystallization of K〓CrO〓.

KOH—K〓CrO〓—H〓O体系，KOH—KAlO〓—H〓O体系和KOH—K〓CrO〓—KAlO〓—H〓O体系相平衡研究结果表明，较低的氢氧化钾浓度有利于铝酸钾结晶析出，一定范围内，较高的氢氧化钾浓度有利于铬酸钾结晶析出，因此，通过控制氢氧化钾浓度可以使铬酸钾—铝酸钾—氢氧化钾得以分离。

These compounds were identified as follows:chrysophanol (FP-1),physcion(FP-2),eriosematin(FP-3),scoparone(FP-4),lupeol(FP-5),betulinic acid(FP-6),3\',4\'-Dihydroxy-trans-cinamic acid octacosyl ester(FP-7),β-sitosterol (FP-8),flemiphilippinone A(FP-9),monopalmitin(FP-10),emodin(FP-11),islandicin (FP-12),salicylic acid(FP-13),p-methoxyphenylpropionic acid(FP-14),trideca-1, 3-diene(FP-15),lupinifolin(FP-16),flemichin D(FP-17),flemiphilippinin A(FP-18), auriculasin(FP-19),erythrinin B(FP-20),6-C-prenylluteolin(FP-21), 8-(1,1-dimethylallyl) genistein(FP-22),flemiphilippinin E(FP-23),flemiphilippinin F (FP-24),5,7,3\',4\'-tetrahydroxy-6,8-diprenylisoflavone(FP-25),flemiphilippinin D (FP-26),dorsmaninsⅠ(FP-27),osajin(FP-28),6,8-diprenyleriodictyol(FP-29), lupinalbin A(FP-30),genistein(FP-31),3\'-O-methylorobol(FP-32),orobol(FP-33), 5,7,2\',3\',4\'-pentahrdroxyflavone(FP-34),the mixture of biochanin A and prunetin (FP-35 and 36),genistin(FP-37),sophororicoside(FP-38),3\'-O-methylorobol-7-glucoside(FP-39),the mixture of sissotrin and prunetin 4\'-O-β-D-glucoside(FP-40 and 41),adenosine(FP-42) and luteoloside(FP-43,mixture).

这些化合物分别为大黄酚(FP-1)、大黄素甲醚(FP-2)、eriosematin(FP-3)、滨蒿内酯(FP-4)、羽扇豆醇(FP-5)、白桦酸(FP-6)、咖啡酸二十八烷酯(FP-7)、β-谷甾醇(FP-8)、蔓性千斤拔酮A(FP-9)、单棕榈酸甘油酯(FP-10)、大黄素(FP-11)、islandicin(FP-12)、水杨酸(FP-13)、对甲氧基苯丙酸(FP-14)、十三烷-1，4-二烯烃(FP-15)、lupinifolin(FP-16)、千斤拔素D(FP-17)、蔓性千斤拔素A(FP-18)、auriculasin(FP-19)、erythrinin B(FP-20)、6-C-异戊烯基木犀草素(FP-21)、8-(1，1-二甲烯丙基)-染料木黄酮(FP-22)、蔓性千斤拔素E(FP-23)、蔓性千斤拔素F(FP-24)、5，7，3′，4′-四羟基-6，8-双异戊烯基异黄酮(FP-25)、蔓性千斤拔素D(FP-26)、dorsmaninsⅠ(FP-27)、osajin(FP-28)、6，8-双异戊烯基圣草素(FP-29)、lupinalbin A(FP-30)、染料木黄酮(FP-31)、3\'-O-甲基香豌豆苷元(FP-32)、奥洛醇(FP-33)、5，7，2′，3′，4′-五羟基黄酮(FP-34)、鹰嘴豆素甲和樱黄素的混合物(FP-35和FP-36)、染料木苷(FP-37)、槐属苷(FP-38)、7-葡萄糖基-3\'-O-甲基香豌豆苷(FP-39)、印度黄檀苷和樱黄素4′-O-β-D-葡萄糖苷的混合物(FP-40和FP-41)、腺嘌呤核苷(FP-42)和木犀草苷(FP-43，混合物)。

A modified γ-Al〓O〓 was prepared by a special precipitation method with aluminum nitrate solution containing a certain amounts of orthosilicic acid and ammonia aqueous solution. Compared with commercial γ-Al〓O〓, the modified γ-Al〓O〓 was an effecient catalyst for dehydration of tetrahydrofurfuryl alcohol to dihydropyran. The results revealed that the strong acid sites on the surface of the catalyst may play a crucial role in this reaction.

并以硝酸铝和氨水为原料，用沉淀法制备出一种高比表面和拥有较多强酸中心的γ-Al〓O〓，它在四氢糠醇开环脱水制备二氢吡喃的反应中有优良的催化活性，通过比较此γ-Al〓O〓和普通商业γ-Al〓O〓的Py-TPD图，发现强酸中心在制备二氢吡喃的反应中可能具有关键的作用。

With this set of criteria, the literatures published 3—O—L—rhamnosyl—(1→2/1→4)—L— rhamnoside, 3—O -D—xylosyl—(1→2/1→4)-L-rhamnoside and 3-O-D — glucosyl-(1 →2/1→4)—L— rhamnoside structures of anhydroicaritin and desmethylanhydroicaritin were re-evaluated.

本文以上述双糖1→2连接的光谱标准，对文献报道的脱水淫羊藿素和去甲脱水淫羊藿素3—O—L一鼠李糖—(1→2或1→4)—L—鼠李糖甙、3—O—D—木糖—(1→2或1→4)—L—鼠李糖甙及3—O—D—葡萄糖—(1→2或1→4)—L—鼠李糖甙类化合物的结构进行了重新评价。

The present invention concerns the compounds having the formula N-oxides, salts, stereoisomeric forms, racemic mixtures, prodrugs, esters and metabolites thereof, wherein R1 and R8 each are H, optionally substituted C1-6alkyl, C2-6alkenyl, C3-7cycloalkyl, aryl, Het1, Het2; R1 may also be a radical of formula (R11aR11b)NC(R10aR10b)CR9-; t is 0, 1 or 2; R2 is H or C1-6alkyl; L is -C-,-O-C-,-NR8-C-,-O-C1-6alkanediyl-C-,-NR8-C1-6alkanediyl-C-,-S2-,-O-S2-,-NR8-S2 ; R3 is C1-6alkyl, aryl, C3-7cycloalkyl, C3-7cycloalkylC1-4alkyl, or arylC1-4alkyl; R4 is H, C1-4alkylOC, carboxyl, aminoC, mono- or di(C1-4alkyl)aminoC, C3-7cycloalkyl, C2-6alkenyl, C2-6alkynyl or optionally substituted C1-6alkyl; R5 and R6 are H or C1-6alkyl.

本发明涉及右式化合物其N-氧化物、盐、立体异构形式、外消旋混合物、前药、酯及代谢物，其中R 1 及R 8 各是氢、C 1-6 烷基、C 2-6 烯基、C 3-7 环烷基、芳基、Het 1 、Het 2 ；R 1 也可以是式(R 11a R 11b )NC(R 10A R 10b )CR 9 -之基；t是0、1或2；R 2 是氢或C 1-6 烷基；L是-C-、-O-C-、-NR 8 -C-、-O-C 1-6 烷二基-C-、-NR 8 -C 1-6 烷二基-C-、-S 2 -，-O-S 2 -、-NR 8 -S 2 -；R 3 是C 1-6 烷基、芳基、C 3-7 环烷基、C 3-7 环烷基C 1-4 烷基或芳基C 1-4 烷基；R 4 是氢、C 1-4 烷基OC、羧基、氨基C、一-或二(C 1-4 烷基)氨基C、C 3-7 环烷基、C 2-6 烯基、C 2-6 炔基或任选被取代的C 1-6 烷基；R 5 及R 6 是氢或C 1-6 烷基。

By the nucleophilic substitution reaction of 6-O-tosyl-l,2:3,4-di-O- isopropylidene-a-Z-galactopyranose (3) with some substituted 1, 2,4- triazole-3-thiols (4a ~ 4c) or 1, 2, 3,4-tetrazole-5-thiols (5a~5f), nine 6-S-(substituted triazolyl or tetrazolyl)-l,2 : 3,4-di-O- isopropylidene-a-D-galactopyranoses (6a ~ 6i) were prepared in high yields. Their structures and configurations were analyzed and established by elemental analysis, IR, NMR, MS spectra.

报道了6－O－对甲苯磺酰基－1，2：3，4－二－O－异亚丙基－α-D吡喃型半乳糖（3）与取代的3－巯基三唑或5－巯基四唑4a-4c或5a-5f的亲核取代反应，合成了9个6－S－－1，2：3，4－二－O－异亚丙基－α- D吡喃型半乳糖（6a-6i），通过元素分析，IR，NMR和MS确证了上述化合物的结构，并经分子模型计算进行了其构象分析。

Meanwhile the defects are also studied by means of the methods of EPR, PSL, thermostimulated luminescence and absorption spectroscopy. These results indicate that the principal defects are F centers and O〓 in PSL. O〓 centers are formed by O〓 ions substituting for F ions with a trapped hole The trap depth of two kinds of F centers is obtained by using thermoluminescent spectra.

同时还利用电子顺磁共振谱，光激励发光，热释发光和吸收光谱的方法，研究了其材料中缺陷的性质，实验结果表明在光激励发光过程中主要的缺陷是F心和O〓心，其中，O〓心是O〓离子替代F〓离子并束缚一个空穴而形成的局域中心。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。