高酸

In this dissertation, the stable radical cation salts ofphenothiazine and 10 - alkylphenothiazine alky=〓(〓 hexachloroantimonate,perchlorate and iodide were prepared by one- electron oxidationwith 2,2,6,6-tetramethyl - 4 -acetyloxypiperidine oxoammoniumhexachloroantimonate, perchloric acid/hydrogen peroxide andmolecular iodine respectively, and they were characteried by UV -Vis spectroscopy and ESR spectroscopy.

本文的主要内容有：吩噻嗪和10-烃基吩噻嗪分别被碘、高氯酸／过氧化氢，2，2，6，6-四甲基-4-乙酰氧基哌啶氧铵六氯锑酸盐氧化为相应的正离子自由基碘盐、高氯酸盐、六氯锑酸盐，并用UV-Vis光谱和ESR波谱进行了鉴定和研究。

Products for all types of civilian ammonium perchlorate and potassium perchlorate, such as industry, the annual production capacity of perchlorate 2000 tons.

产品为各种类型的民用高氯酸铵和工业高氯酸钾等，年生产高氯酸盐能力为2000吨。

This article that focuses on the systematic and in-depth research in the current primal problem about abnormal burst pressure reservoir depress burst pressure has procured following main fruits:1 It forms the method which could obtain massive vertical static state mechanics parameters.2 In a foundation of acquisition of rock mechanics parameters,apply bent lamella that as mechanical model along with characteristic of actual geologic characteristics to analysis curvature for anticlinal strcture, get homologous tectonic stress value throug relation between the curvature and stress and different principal curvature in anticlinal structure,consequently set up laminational stress model for anticline reservoir. The block lamination for existed fracturing date has formed method of setting up mechanical model of lamination terrestrial stress by abtaining the block tectonic stress coefficients which are got by complex utilization test, laboratory test and fracturing date playback.3 Analysesing the main reason which lead to high burst pressure by considering the characteristic of reservoir geology,reservoir,and rock mechanics and reservoir damage,etc.Establishing burst pressure quantitative prediction model which provide gist for depressing construction risk and optimizing construction craft under the condition of open hole completion ,gun-perforated completion and damaged reservoir.4 Provding theoretical basis for interpreting acidification pretreatment which could depress busrt pressure by finding the relation between the influencing factors and rock machanics parameters and analysing the factors that have effect on rock mechanics parameters. Expounding the mechanism of reaction of mixed monomineral and acid from the angle of microcosmic element, evaluating quantitatively acid sensilility of different kinds of mineral effectively, and determing the first-order reaction dynamical equation of each mineral.5 Revealing rock mechanics property chage as a result of acid flooding in different condition by sandstone traumata experiment in different temperatures which combined with rock mechanics triaxial stress experiment.6 Associating damage mechanics with sandstone acidizing, established sandstone damage mechanics model in the foundation of the recognition on the rock mechanics parametric variation which is caused by acid-rock reaction in both macroscopic view and microscopic view ,also demonstrated those processes and quantitative estimated the acid busrt pressure to direct the site operation.

本文针对目前异常破裂压力储层降低破裂压力的主要问题展开较为系统和深入的研究，取得了以下主要成果：1形成了利用测井资料，结合室内岩芯测试结果，获取静动岩石力学参数的相关性特征，从而获得纵向上大量静态力学参数的方法。2在获取了岩石力学参数的此基础上，利用弯曲薄板作为力学模型，结合区块实际地质特征对背斜构造进行曲率分析，通过曲率与应力的关系，利用背斜构造不同部位的主曲率求得相应的构造应力值，从而建立起背斜储层的分层应力模型；对已有压裂资料的区块分层，形成了综合利用测试、室内实验、压裂资料反演获得该区块构造应力系数，建立起分层地应力的力学模型的方法。3综合考虑储层地质、油藏、岩石力学特性和储层伤害等因素，分析造成高破裂压力的主要原因，综合利用岩石力学、弹性力学等知识，建立了裸眼完井、射孔完井条件下以及储层受到伤害后的储层破裂压力定量预测模型，为降低施工风险和优化施工工艺提供了依据。4完成了物性、岩性影响岩石力学参数的因素分析，找出了各影响因素和岩石力学参数之间的关系，为从机理上解释酸化预处理降低破裂压力提供了理论基础；从微观元素的角度阐述了单矿物与酸反应的机理；并在此基础上，有效评价了各种矿物的酸敏感性，定量确定了岩石中各矿物的一级反应动力学方程。5完成了不同温度下的酸液类型、酸液浓度、注酸量等一系列砂岩损伤实验，结合岩石力学三轴应力实验，系统揭示了在不同条件下注酸而引起的岩石力学性质变化。6将损伤力学与砂岩酸化相结合，在宏观、微观两个方面认识酸岩反应引起岩石力学参数变化基础上，建立了砂岩损伤力学模型，并对其进行验证，在此基础上定量计算酸化后的破裂压力，有效指导现场施工

Then studied on several clays affect on the stability of ferrate solution. The results show the addition of clays retarded the decomposition of ferrate in alkaline solution. Through analysed the results of test, we found this due to the silicium or polysilicium of clays and its increasing stabilizing effect on ferrate when the concentration of silicium or polysilicium increases.

接着作了粘土对高铁酸盐溶液的稳定作用的研究，结果表明粘土对高铁酸盐溶液有良好的稳定作用，通过实验分析得到其稳定作用是由于粘土中溶出的硅酸根或多聚硅酸根所致，且随着其浓度的增加对高铁酸盐的稳定作用增强。

Alcaligenes eutrophus WSH3 was selected as the strain for the production of polyβ-hydroxybutyrate and copolymer of 3-hydroxybutyrate and 3hydroxyvalerate . This study is aimed at finding an operative way leading to high PHB and PHBV productivity, high yield coefficient and high content of PHB and PHBV. The main research results are as follows

本文以真养产碱杆菌(A.eutrophus)WSH3为聚-β-羟基丁酸和3-羟基丁酸与3-羟基戊酸的共聚物的生产菌株，以实现PHB和PHBV发酵过程的高的生产强度、高的产物对基质的产率系数和高的聚合物含量为目标，进行了PHB及PHBV发酵条件的研究，主要研究内容和结果如下

The results show that magnesium and aluminum theoretically can be thoroughly dissolved from the blast furnace slag by diluted sulfuric acid pretreatment on the blast furnace slag even if the ended concentration of sulfuric acid is 0.001mol/L, while the titanium basically could not be dissolved. Therefore it is theoretically indicated that the separation of the magnesium and aluminum from the slag with the least titanium loss by diluted sulfuric acid pretreatment is possible.

结果表明，采用稀硫酸对高炉渣进行预处理，当终酸浓度即使为0.001mol·l~(-1)时，镁、铝理论上也能全部被酸浸出，而钛在0.001 mol·l~(-1)的酸浓度条件下基本不被浸出，从而从理论上可以说明对高炉渣采用稀酸预处理可以很好的将炉渣中的镁、铝等杂质分离出来，而钛极少被浸出。

The new acid system can stabilize the ferric ions, furthermore it can prevent the acid sludge forming during acidizing treatment, also can eliminate sulphide scale.

实验表明螯合酸对于高含碳酸盐岩砂岩储层具有很好的酸化效果，对于高含酸敏性矿物而碳酸盐岩含量较低的砂岩储层酸化效果有限，但不会给储层带来二次伤害。

High-Al cement or calcium aluminate cement, soft clay, kyanite, Al2O3 and/or SiO2 powder, and naphthalenesulfonic acid-formaldehyde condensate.

铝硅质原料是焦宝石、莫来石或高铝矾土中的一种或几种以上，其中Al 2 O 3 ≥45％；结合剂为高铝水泥或纯铝酸钙水泥；高铝水泥占喷补料总量不少于5％，其中Al 2 O 3 ≥46％，CaO≤40％；纯铝酸钙水泥中Al 2 O 3 ≥69％，CaO≤25％；烧结剂和可塑剂为软质粘土，膨胀剂为蓝晶石；外加剂为萘磺酸甲醛缩合物。

Based on the judgement on the existing of whether leading functional group or unleading functional group,if unleading exists,what about its bond type,with these pre-classification information,a new classification methods and uint structure model which can reflect the name,composition,stucture and function was put forward in this paper.

前言 高性能混凝土外加剂分子只存在磺酸、羧酸两种主导官能团，以磺酸、羧酸、&磺酸-羧酸&三种方式存在，因而把高性能外加剂分成磺酸、羧酸、&磺酸-羧酸&三大系列 [1、2 ]。磺酸系列外加剂的一个重要性能是高减水率，故有时将它称之为高效减水剂。

A comparison of the degradation effectiveness of PVA by potassium ferrate, sodium hypo-chlorite and combination of them was studied. The effects of potassium ferrate and sodium hypochlorite dosage, oxidation time, initial concentration of PVA and pH on removal rate of PVA were explored.

文章比较了高铁酸钾、次氯酸钠、高铁酸钾与次氯酸钠联用对PVA的降解效果，考察了高铁酸钾和次氯酸钠的投加量、氧化时问、PVA溶液的pH值和初始质量浓度对PVA去除率的影响。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。