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A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3,3'-偶氮双(6-氨基-1,2,4,5-四嗪)新合成路线、采用3,5-双(3,5-二甲基吡唑-1-基)-1,2,4,5-四嗪为原料,由文献报道的4步反应缩减为2步,经高压氨解、高锰酸钾氧化合成了DAAT,总收率大幅提高,达到58.1%,并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

On the basis of the analysis of the scores, the author makes conclusions about the characteristics of Schubert"s last three piano sonatas as followings: 1 The device of universal development in the movements composed in sonata form and rondo-sonata form is the most distinctive feature in the last three sonatas, which is also decisive in the trend of the whole movement and makes the developments relatively "still". 2 In the device of themes, the method of irregularity is preferred. However, By using extension, abbreviation, repetition and further repetition of periods, Schubert brings those themes to ingenious balance in both architectonics and aesthetics. 3 Chain method is applied in the connection of themes, in which the previous material is taken as basis and then modified together with the variations of new materials. By this way, the theme is continuously developed. 4 The principle of the dominant-subordinate is followed in Schubert"s three-key exposition, and the process of each key is extended.

本文在详尽分析乐谱的基础上,对最后三首奏鸣曲的主要创作特点进行了以下总结: 1、奏鸣曲式和奏鸣回旋曲式乐章中展开的普遍化是最后三首奏鸣曲最为显著的特点,它决定了整个乐章的走向,并使展开部具有相对"静止"的特点; 2、舒伯特的主题写作中更喜欢运用非方整性写法,并通过自身材料的延长、缩减和重复或者更高一级的段落重复使其达到了结构上和审美上的巧妙平衡; 3、舒伯特喜欢用链式的主题贯穿方式,音乐以之前的材料为依据,经过变化后再加入新的材料,用这种方式不间断地发展; 4、舒伯特的三调呈示部遵循从主到属的总体原则,并扩展了调性历程。

Advent of a bear market, for small fund companies, not the original number of management fee income by asset size has shrunk to speed up the grim challenges.

一个熊市的到来,小基金公司,而不是资产规模管理费收入原来的数量已经缩减加快的严峻挑战。

As long as you live austerely and stand it, the price will back again.

你只要勒紧腰带,将开支缩减些,忍得够久,股价大都会再回头的。

There would be growing enthusiasm when in the sekond year, it was anounsed that the troublesome 'ph' would henseforth be written 'f'. This would make words like fotograf twenty persent shorter to print.

在第二年,英语改造的热情会高涨起来,这时我们该宣布那个讨厌的"ph"从此改写为"f",这样就使fotograf这样的单词缩减20%拼写量。

Love is the highest value in life: It should not be reduced to stupid rituals.

爱是生命中的最高价值:它不应该缩减为那些愚蠢的仪式。

Military in the Asia region control of the sea will be reduced to 20%.

那么美军在亚洲地区的海面控制能力将被缩减到20%。

During the economic downturn, even Microsoft had to do some belt-tightening.

在经济不景气的时候,甚至连微软都在缩减开支。

Will the government cut back on the big-ticket programs?

政府会缩减那些耗资巨大的计划吗?

You also had a great growth in bilateralism, that instead of trading on a multilateral basis - that is trading with anyone and buying from the cheapest source - you had a whole series of trade agreements where preferences were being given to particular countries.

因此一共有三个方面的因素:一是货币动荡;二是贸易壁垒大量增加,再加上大萧条,贸易大幅度缩减;第三是大量通过优惠国渠道进行贸易。下面我们把斯纳普教授对国际货币基金组织成立时的历史背景的介绍再听一遍。

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Methods: Five patients with parkinsonism or dystonia were assigned to general anesthesia using an modified endotracheal tube.

本实验依照人体实验之相关规定进行,五位患有帕金森氏症或肌张力异常的病人接受神经立体定位手术。

If you can benefit from this book, it is our honour.

如果您能从本书获益,这将是我们的荣幸。

The report also shows that the proportion of unmarried men and women living together has doubled between 1986 and 2006, with 13 per cent of those aged 16 to 59 now cohabiting.

报告还指出,从1986年至2006年,英国未婚男女同居的比例增长了一倍,在16岁至59岁的人群中,有13%的人同居。