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The base-catalyzed rapid polymerization of caprolactam applied to the spinning of synthetic fiber was investigated. Acetanilide was used as molecular weight stabilizer, which could efficiently control the course of polymerization and to obtain the polymer with stable viscosity. The scale-up experiments on continuous polymerization and direct spinning were run smoothly.

对碱性催化的己内酰胺快速聚合应用于纺丝进行了研究,采用了合适的分子量稳定剂,控制了聚合进程,得到粘度稳定的聚合体,并且进行了连续聚合直接纺丝的扩大试验,取得了持续稳定运转的结果,纺出产品复丝,其抗张强度为5—6克/,延伸为19—25%,与水解聚合方法同类产品丝相仿。

This study evaluated the effect of SDS-PAGE with the low C separating alkalescence peptides under the different conditions.

本试验初步研究了低交联度的SDS-PAGE分析蜂毒碱性多肽的方法及有关条件的优化。

Analyzing the change of DH, PCL and active calcium, and selecting each of best method. The results:(1) Dealing with the bone under high pressure ①High content of protein in sheep bone or bone soup:0.05MPa, 2h, 1:2;②Low amino acids in bone powder:0.13MPa, 4h, 1:3; Low amino acids in bone soup: 0.10MPa, 3h, 1:4;(2) Hydrolysis the bone soup with enzymes ①High content of calcium: neutral enzyme, 1500u/L, 6h;②High DH: pancreatic enzyme, 1:100, 6h;③ Low PCL: Pancreatic enzyme, 1:125, 6h; High PCL: alkalescency enzyme,

结果表明:A、高压①骨粉及骨汤蛋白质含量最高:压力为0.05MPa,高压2.0h,骨水比为1:2;②骨粉中氨态氮最低:压力0.13MPa,高压4.0h,骨水比为1:3;骨汤中氨态氮最低:0.10MPa,3.0h,骨水比1:4;B、酶解①游离钙含量最高:中性蛋白酶,酶浓度1500u/L,酶解6h;②水解度最高:胰蛋白酶,酶浓度1:100,酶解6h;③PCL值最低:胰蛋白酶,酶浓度1:125,酶解6h;PCL值最高:碱性蛋白酶,酶浓度1500u/L,酶解8h。

The results:(1) Dealing with the bone under high pressure ① High content of protein in sheep bone or bone soup:0.05MPa, 2h, 1:2;② Low amino acids in bone powder:0.13MPa, 4h, 1:3; Low amino acids in bone soup: 0.10MPa, 3h, 1:4;(2) Hydrolysis the bone soup with enzymes ① High content of calcium: neutral enzyme, 1500u/L, 6h;② High DH: pancreatic enzyme, 1:100, 6h;③ Low PCL: Pancreatic enzyme, 1:125, 6h; High PCL: alkalescency enzyme,

结果表明: A 、高压①骨粉及骨汤蛋白质含量最高:压力为0.05MPa ,高压2.0h ,骨水比为1:2;②骨粉中氨态氮最低:压力0.13MPa ,高压4.0h ,骨水比为1:3;骨汤中氨态氮最低:0.10MPa ,3.0h ,骨水比1:4; B 、酶解①游离钙含量最高:中性蛋白酶,酶浓度1500u/L ,酶解6h ;②水解度最高:胰蛋白酶,酶浓度1:100,酶解6h ;③ PCL 值最低:胰蛋白酶,酶浓度1:125,酶解6h ; PCL 值最高:碱性蛋白酶,酶浓度1500u/L ,酶解8h 。

Wastewater containing titanium pigment was treated by microfiltration membrane, Nanometer titanium can be purified and concentrated by use of microfiltration. Operational conditions were optimized and the model was built. Finally, the amount of wash water was reduced. Based on the above research, the whole set equipment was designed, which can meet the needs in a titanium industry with a capability of 500 ton per year. Backflush and automatic control were used in the equipment, which has been steadily run two years, has been widely adopted in titanium industry. The technology has been widely adopted in titanium industry.In the recent years, whole set equipment of ceramic membrane was increasingly used in the recovery of desired production from fermentation broth in China. A new membrane process integrated with pretreatment of flocculation or coagulation was exploited to recover Inosine. ZrO2 ceramic membrane was used in the work, and the average permeation flux could reach 150L/m2.h under pH value of 3, transmembrane pressure 0.1MPa, CFV 3m/s, and temperature higher than 70C. The recovery ratio of inosine is higher than traditional recovery method, although inosine degraded under acidic and high temperature condition.

实验表明,ZrO_2膜处理肌苷发酵液的合适条件为pH=3、操作压力为0.1MPa、膜面流速3m/s、温度大于70度,此时可以获得平均渗透通量150L/m~2h,但由于酸性条件、高温下肌苷降解,导致肌苷收率有所降低,但仍高于传统肌苷提取方法得到的收率;为进一步提高肌苷得率,缩短提取工序,实验研究了絮凝剂预处理发酵液,解决碱性条件下由于蛋白析出导致膜污染加重的问题,研究表明采用CaCl_2絮凝并调节pH=11,可以获得平均渗透通量为180L/m~2h,肌苷得率大于95%;比较了三种肌苷提取工艺得到的产品质量,采用预处理与陶瓷南京工业大学博士学位论文膜分离结合的除杂工艺得到的粗昔质量与陶瓷膜分离、离子交换及活性炭吸附工艺生产的粗普质量相当,均优于传统的提取工艺;设计了每小时处理12一巧吨肌普发酵液的陶瓷膜成套装置,采用部分内循环的方式降低设备的能耗,简化了肌昔提取方式,提高了产品的收率和得率,由于减少离子交换和活性炭吸附,使得工厂废水排放量降低30一40%,降低酸、碱用量,有利于环境保护。

Based on the principle of electronegativity equalization, a new method is developed which can be used to scale the basicity of binary oxides.

本文应用电负性均衡原理,建立了一种标度二元氧化物碱性强弱的新方法。

In borate solution, The order of effective mobilities of disaccharide-borate compolexes was saccharose<celloiose< maltose<lactose and that of polylol- borate complexes was ethylene glycol< propanetriol<erythritol<sorbitol<mannitol<dulcitol.

在碱性四硼酸钠溶液中二糖硼酸络合物淌度顺序为:乳糖>麦芽糖>纤维二糖>蔗糖,多元醇硼酸络合物的淌度顺序为:六羟基多元醇>四羟基多元醇>三羟基多元醇>二羟基多元醇。

Based on the comprehensive consideration of brilliance,colouring power,colour fastness to sunlight,cost of dyes and simplicity in operation,two methods are provided for solving the blue fade-in problem of the green cotton paper used in making the leaves of silk flower.

本文对碱性染料在棉纸上着色的坚牢度及迁移性作了研究,在对染色鲜艳度、着色力、日晒牢度及染料价格、使用简易等方面作了综合性考虑的基础上,对绢花生产中绿色棉纸变兰的问题提出了两种解决方法,取得了满意的结果。

The results showed that the solubility of lotus starch was low, the turgidity was closed to sweet potato starch, accordingly was a restrictive swelling starch. A lower transparency (10.4%) was researched in the lotus-seed starch pastes, condensation speed was faster, but it decreased at acidic or alkaline condition. Stronger freeze-thaw stability and lower gel strength was researched in it. It can be from the Brabender viscosity that the lotus-seed starch has a higher gelatinization temperature (77.1℃), better thermostability, stronger retrogradation, weaker cold viscosity stability.

试验结果表明:莲子淀粉的溶解度较低,膨润力接近甘薯淀粉,属限制型膨胀淀粉;莲子淀粉糊的透明度较低(10.4%),凝沉速度较快,在酸性或碱性条件下凝沉速度减缓;其凝胶具有较强的冻融稳定性和较低的凝胶强度;布拉班德粘度曲线显示,莲子淀粉的糊化温度较高达77.1℃,热稳定性好,凝沉性强,冷粘度稳定性差。

The invention provides a method when alkaline protease hydrolyses from big molecular collagen into minor polypeptides, free amino acids in enzymatic hydrolysate increase gradually, a positive correlation is shown between increased amount and hydrolysis degree, so the hydrolysis degree can be calculated by detecting total amino acids or a certain kind of amino acid content in enzymolysis liquid.

本方法是利用碱性蛋白酶水解大分子胶原蛋白生成小分子多肽的同时,酶解产物里游离氨基酸含量逐渐增加,其增加的量与水解度大小呈正相关,因此,通过检测酶解液中氨基酸总量或某一种氨基酸含量可计算出水解度的大小。

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我不赞成死刑——这是以牙还牙的报复行为。

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