研磨的

Chemiluminescent immunoassay is one of the advanced immunoassay ofnon-radioisotopic immunoassay because of its high sensitivity, wide dynamic range,high accuracy, stable labeled protein, full automation and extensive application field.CLIA using acridinium ester derivatives as chemiluminescent label has advantages oflow background, high signal-to-noise ratio, no need of catalyst and simpleluminescence system. Different aspects associating the DMAE·NHS-based CLIA were studied in thisthesis, including synthesis of acridinium ester, chemiluminescentcharacteristics of DMAE·NHS, labelling antibody or streptavidin with DMAE·NHS,two-site sandwich chemiluminescent immunoassay for TSH, two-sitesandwich chemiluminescent immunoassay involved biotin-streptavidinsystem for TSH, and competitive chemiluminescent immunoassay usingbiotin-streptavidin system for TT〓. The desired acridinium ester, DMAE·NHS, was synthesized according to thereference method with some modifications. The products were identified by IR, NMR,MS and elemental analysis. In our method, KOH was used in place of NaOH tosynthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate waspurified on a silica gel column with chloroform/ethylacetate(4:1, v/v) as eluent andfurther purified by triturating with hexane/acetone(2:1, v/v).

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-二甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿／乙酸乙酯(4∶1，V∶V)作溶剂和淋洗剂，第二次柱层析用己烷／丙酮(2∶1，V∶V)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷／丙酮(2∶1，V∶V)进行研磨，过滤，洗涤，除去溶于己烷／丙酮(2∶1，V∶V)的部分，得到所需要的产品。

TEM shows that drying by direct heating might result in hard aggregation of the tourmaline powder, while hard aggregation might be avoided by azeotropic distillation. Raman spectroscopy reveals that there are O_H and C_H on the surfaces of the tourmaline powder obtained by azeotropic distillation, which indicates that butoxy is chemically adsorbed on the surfaces of tourmaline particles, but not adsorbed on those formed by direct drying. X_ray powder diffraction shows that the intensity of diffraction peaks decreases after grinding. There is no damage to the tourmaline crystal lattice in the process of direct heating, azeotropic distillation, or ultrafine grinding.

透射电镜分析结果表明，直接加热脱去水或正丁醇会使电气石超细颗粒发生硬团聚，而共沸蒸馏法则可有效防止硬团聚的产生；拉曼光谱结果表明，共沸蒸馏法制备的电气石粉末表面存在O—H和C—H键，说明正丁醇在颗粒表面为化学吸附，而直接干燥法得到的电气石粉末表面则没有；X射线粉晶衍射结果表明，研磨过程降低了粉末衍射峰的强度，但直接加热干燥和共沸蒸馏干燥均未破坏电气石的晶格结构。

Any of various tropical African shrubs or trees of the genus Coffea, especially C. arabica, widely cultivated in the tropics for their seeds that are dried, roasted, and ground to prepare a stimulating, aromatic drink.

咖啡树一种咖啡属热带非洲地区的灌木或树，尤指因经干燥、烘烤和研磨以作为一种剌激性的、有香味的饮料的种子而广泛在热带地区栽培的小果咖啡

The permanent magnets of single-phase exchange coupling Nd 〓N〓 and Nd 〓N〓 with ThMn〓 structure have been prepared by MM and MA process and the following treatments of crystallization、nitrogenation. By means of XRD、SEM、TEM、DTA/DSC and magnetic measurements, the variations of microstructure in each corresponding stage and the related magnetic properties have been studied systematically.

本文采用机械合金化和机械研磨法及随后的晶化、氮化处理分别制备了具有ThMn〓结构的Nd〓N〓单相耦合及Nd〓N〓纳米永磁材料，借助于X射线衍射、扫描电镜、电子探针、透射电镜、差热分析以及磁测量等分析技术系统地研究了上述工艺各阶段对应的组织结构的变化以及它们与磁性能的相互关系。

Meguiar'Mirror Glaze/professional medium-cut cleaner 盒子背面 Removes tough paint defects resistant to less aggressive cleaners ·Works with a rotary buffer for FAST,EFFECTIVE removal of swirls,water spots,acid rain damage and bonded contaminants ·Buffered Abrasive Action lubricates the finish to prevent scouring ·Diminishing Abrasives cut quickly then break down and disappear as they polish the finish ·Safe and effective on all paints,including CLEAR COATS ·PAINTABLE:safe for use in a paint shop environment METHOD OF APPLICATION:for use with rotary buffer only.

正面：美光'Mirror釉面/专业medium-cut清洁反面：移除强硬的涂料缺陷抵抗清洁工与轨道式·快速、有效的去除螺旋纹、水体、酸雨的伤害和污染物研磨作用的缓冲·可完成预防冲刷很快就切·减少磨擦分解和消失，因为它们擦亮·安全、有效的一切，包括清洁的漆漆面：安全使用。

As flux used in light metal processing for metal surface treatment; as component in the production of aluminum-titanium-boron alloys and for the fabrication of grinding wheel and abrasive disc to reduce operating temperature; as flux used in welding; as fire retardent for cotton and artificial fibre; rodent for the removal of exposed lead in printed circuit board; chemical analytical reagent in electrochemistry; used to melt with silver, gold, stainless steel; as material to produce boron alloys.

作为熔剂用于轻金属加工对金属表面处理，制造铝钛硼合金和作砂轮研磨盘的成份，以降低操作温度；用于焊接上作助熔剂及制造其它氟盐的原料；用作棉花和人造纤维的阻燃剂，用来清除印刷电路中露出铅的侵蚀液；用于电化学合成的化学分析试剂，用于熔接和熔合银、金、不锈钢等金属，可做铝镁浇铸生产含硼合金的原料。

According to the invention, a mineral with layer structure is used as the inorganic component of the suspension, which is milled in delaminating in a liquid, after which the suspension containing the organic phase and the obtained plate-like mineral particles, which have become smaller in size, is brought onto the surface of the product particles.

根据本发明，使用具有层状结构的矿物作为悬浮液的无机成分，在液体中进行层分离研磨，然后，把含有有机相和所获得的尺寸已经变小的片状矿物颗粒的悬浮液涂敷到产品颗粒表面上。

The products were identified by IR,NMR,MS and elemental analysis. In our method,K.OH was used in place of NaOH to synthesize benzyl ester of 3,5-dimethyl-4-hydroxybenzoic acid,2',6'-dimethyl-4'-(n-succinimidyloxycarbonyl) phenyl-acridinium-9-carboxylate was purified on a silica gel column with chloroform/ethylacetate(4:l,v/v) as eluent and further purified by triturating with hexane/acetone(2:l,v/v).The luminescence produced by DMAE-NHS is a flash light with maximumemission at 0.4s and decay half-time of 0.9s. The luminescence intensity is 6.11x10 cps/mol,which is affected by the composition of trigger and surfactant.

DMAE·NHS的合成是本论文的关键和难点，我们对文献方法进行改进：文献方法用氢氧化钠与3，5-二甲基-4-羟基苯甲酸反应制得3，5-甲基-4-羟基苯甲酸钠，再用3，5-二甲基-4-羟基苯甲酸钠与苄氯作用制备3，5-二甲基-4-羟基苯甲酸苄酯，我们用氢氧化钾代替氢氧化钠，使合成取得成功；在合成2'，6'-二甲基-4'-苯基-吖啶-9-甲酸酯时，文献方法对粗产品进行两次硅胶柱层析纯化，第一次柱层析用氯仿/乙酸乙酯(4：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，第二次柱层析用己烷/丙酮(2：1，Ⅴ：Ⅴ)作溶剂和淋洗剂，按照文献方法得到的不是所需要的化合物，我们只进行第一次柱层析纯化，然后用己烷/丙酮(2：1，Ⅴ：Ⅴ)进行研磨，过滤，洗涤，除去溶于己烷/丙酮(2：1，Ⅴ：Ⅴ)的部分，得到所需要的产品。

So that the requirements of high precision and high efficiency of grinding tools and remember the people and customers think of the common development of the "Pearl of the diamond tool."

我们将适应时代的发展，追求技术的革新，满足客户的需求。让要求高精度、高效率的研磨工具的人们想起并记住与客户共同发展的&明珠钻石工具&。

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Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。