毛细管

Chapter 4 Capillary Zone Electrophoresis with Amperometric Detection forComposition Analysis of LaminarinThe composition of laminarin was firstly determined by analyzing its hydrolysis monosaccharides with capillary zone electrophoresis - amperometric detection.

第四章毛细管电泳一安培检测法测定昆布中多糖成分本论文首次用毛细管电泳一安培检测法测定了昆布多糖水解单糖的成分，实现对(来源：Aa4BC9b2b论文网www.abclunwen.com)昆布多糖的测定。在选定的最佳条件下，昆布多糖水解产物岩藻糖、半乳糖、葡萄糖、甘露糖、木糖在20min内实现完全分离而且在铜电极上有着很好的电流响应。通过对昆布多糖中水解单糖成分含量的计算显示该多糖中岩藻糖、半乳糖、葡萄糖、甘露糖、木糖的摩尔比为

Methods: The cyclodextrin, concentration, pH, organic solvent were studied, and the results indicated that the enantiomer of ephedrin and ephedrine levorotatory were baseline separated under the following experimental conditions: uncoated fused silica capillary (75 μm× 68 cm), 25 mmol/L Tris, 2% HP-β-CD and 1% SBE-β-CD, pH was adjusted at 3.0 by phosphoric acid, and 15 kV separation voltage.

以SBE-β-CD和HP-β-CD二元环糊精为手性添加剂，探讨了环糊精种类及浓度、pH、有机溶剂种类等因素对麻黄碱及伪麻黄碱对映体拆分的影响，结果表明：毛细管：未涂渍熔融石英毛细管75μm×68 cm（有效长度60 cm）。分离用缓冲液为25 mmol/L的Tris缓冲液，含2.0% HP-β-CD和1.0% SBE-β-CD，用磷酸调节pH至3.0。

METHOD:Hemotocrit and fibrinogen were determinded by capillary micromethod and capillary heat microprecipitation method in mice models with repeated cerebral ischema-reperfusion.ηb,ηp,ηh,VAL,TEL and MST were also determined.

采用反复脑缺血再灌注模型鼠，应用毛细管微量热沉法和毛细管微量法分别检测血纤维蛋白原含量和红细胞压积数值，并将结果输入全自动血液流变仪得出血浆粘度、血液粘度、血液还原粘度、血细胞聚集系数、血栓形成系数及微循环滞留时间。

The characterization equations of primary normal stress difference of polymer melt were derived with or without the consideration of the inertia item respectively.

以振动场中流经毛细管的聚合物熔体为研究对象，针对忽略和不忽略惯性力项对熔体弹性行为的影响 2 种情况，分别推导出振动力场中毛细管壁处聚合物熔体第一法向应力差的计算公式。

It was found that well-defined separation of EP was achieved with decoupling devices containing on-line pretreated the working electrode, and the working electrode located very close to the capillary outlet (10-20 μm).

采用自行组装的毛细管电泳柱端安培检测系统，以肾上腺素为分离检测对象，系统考察了工作电极与毛细管末端对齐的距离、去耦器和工作电极的预处理等对分离检测的影响。

Capillary Electrophoresis as a Method for Determining Hydrolysis Rate Constant of Raffinose Capillary electrophoresis was first employed for the determination of hydrolysis rate constant of trisaccharide raffinose.

测定棉子糖水解速率常数的毛细管电泳方法毛细管电泳首次用于测定三糖的水解速率常数。

The background electrolyte was a 75 mmol/L sodium borate solution adjusted to pH 9.7 with 0.1 mmol/L NaOH solution. The detection wavelength was 228 nm and a voltage of 14 kV was applied. The Forsythia suspensa Vahl was extracted by water and a set of CEFP containing 29 peaks was obtained.

中文内容：摘要：采用毛细管区带电泳法，以75 mmol/L硼砂溶液(用0.1 mmol/L氢氧化钠溶液调pH 9.7)为背景电解质，运行电压14 kV，检测波长228 nm，重力进样15 s(高度9 cm)，建立了连翘药材的毛细管电泳指纹图谱。

The capillary electrophoresis fingerprints of Fructus Forsythiae was established to control its quality. The background electrolyte was a 75 mmol/L sodium borate solution adjusted to pH 9.7 with 0.1 mmol/L NaOH solution. The detection wavelength was 228 nm and a voltage of 14 kV was applied. The Forsythia suspensa Thunb.

采用毛细管区带电泳法，以75 mmol/L硼砂溶液(用0.1 mmol/L氢氧化钠溶液调pH 9.7)为背景电解质，运行电压14 kV，检测波长228 nm，重力进样15 s(高度9 cm)，建立了连翘药材的毛细管电泳指纹图谱。

Enantiomeric separation of promethazine and thioridazine, unstable at room temperature, was performed at temperatures down to 3℃ on a lab-built-up CE instrument.

研究了手性药物异丙嗪和硫利达嗪的低温手性毛细管电泳分离，利用实验室自制的低温毛细管电泳仪，成功拆分了它们的混合物。

By the interaction of ethyl acetate and water class solution, The nano silica was synthesized on fused silica capillary tubular inner surface, its morphology and change trend of surface area pore volume and pore size under different reaction condition were investigated.

第三章 原位溶胶-凝胶法制备纳米SiO〓型PLOT石英毛细管色谱柱及其应用建立了原位溶胶-凝胶法制备纳米SiO〓型PLOT色谱柱的方法，采用原位溶胶-凝胶法在毛细管内壁合成出均匀的纳米硅胶多孔层，对所合成的纳米硅胶颗粒进行了形貌表征，同时考察了不同反应条件下纳米硅胶的比表面积、孔体积和孔径的变化规律。

He and Nina moved to California and lived at 2005 Ivar Street, Apt.

他和Nina搬到加州，并在2005年伊瓦尔街，公寓生活。

Droperidol （ potently inhibits transfected HERGchannels and this is the probable mechanism for QT prolongation.

氟哌利多有效地抑制了转染的 HERG 钾通道，可能是 QT 间期延长的机制。