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The fluorescence anisotropy using steady-state fluorescence polarization method was measured for the solution of β-CD and cinchonine mixed and sonicated for 1h. The anisotropy values for the solution increased with the increase of the concentrations of β-CD, which implied the existence of some complexes of large size or nanotube structure. Many type of large size complexes formed between β-CD and Cin under high concentrations in gas phase were characterized by ESI-MS in moderate experiment conditions.

将辛可宁与环糊精的混合溶液超声1个小时后,用稳态荧光偏振方法测定溶液的各向异性值,发现随着环糊精浓度的增大,溶液的荧光各向异性不断增强,这意味着溶液中形成了大尺寸即纳米级结构的环糊精与辛可宁复合物;用温和的质谱测定条件表征发现高浓度的β-CD与辛可宁在气相中可形成各种类型的大尺寸复合物。

Theobserved strain is 10~2 times as local point strain at the same observed stress.This indicates that macroscopical symmetrical rock is quasi-brittle materialwith microcosmic heterogeneousness and its macroscopical mechanicalbehavior is the results of reciprocity and magnification between microcosmiccharacteristic, not simple sum.(4) The degree of irregularity of strain increases with the number of cycle.But degree of irregularity of transverse strain fluctuates larger at the samecycle. Moreover degree of irregularity of transverse strain is larger than that ofaxial strain. This shows that deformation and failure of rock is process ofevolvement of small crack. Small crack evolves from even and out-of-orderstatus to heterogeneous and ordinal status.(5) Ultrasonic speed decreases with the number of cycle. The decreasecourse is such: Firstly, ultrasonic speed fluctuates in a steady scope in somecycles; And then ultrasonic speed quickly decreases to a certain more smallvalue; Afterwards in succedent cycles, ultrasonic speed fluctuates about thevalue. That is to say, ultrasonic speed fluctuates and decreases at intervals ofcycles. In deformation process of rock, quantitative change and qualitativechange of its small crack evolvement carry through crosswise.(6) Strength and modulus of rock decrease with exponential function asscale of specimens increases.

同一表观应力下,局部点应变与表观应变相差可达2个数量级,表明宏观上均匀的岩石是具有细观特征的准脆性材料,其宏观力学行为是细观特征相互作用、放大的综合结果,而不是简单的叠加;(4)岩样轴向应变不均匀程度和横向应变不均匀程度随循环次数的增加渐进增大,但是在同一个循环内,横向应变离散系数随应力的变化波动较大,且同一循环级别下,横向应变不均匀程度大于轴向应变不均匀程度,表明岩石内部微裂纹的演化是岩石变形破坏的本质特征,这一演化表现为微裂纹从均匀无序分布逐渐向非均匀有序发展;(5)随循环次数的增加,所有岩样内部超声波速会出现衰减,衰减过程表现为在某几次循环内超声波速在某一相对范围内波动,然后急剧减小到某一较小值,在随后的循环内,超声波速又会保持在这一较小值附近波动,即超声波速表现为波动和急剧减小间隔形式衰减,表明从宏观看来平稳的岩石变形过程,内部结构演化过程(微裂纹发展及其相互作用)却表现为均匀量变和突发质变不断交叉进行的现象;(6)岩石强度和弹性模量随尺度增大呈指数函数规律减小。

The conclusions can be drawn through numerical simulation: The hydrate-forming region becomes small with increasing circulation rate and inhibiter concentration, and it is possible to make the hydrate-forming region away from sea floor by increasing circulation rate and inhibiter concentration, thus preventing blowout preventer lines from hydrate plugging; the decrease in gas volume fraction in the annulus due to hydrate formation reduces pit gain, which can delay the detection of well kick; the possibility of hydrate presence at a relatively low gas production rate is much greater than that at a relatively higher production rate; the bottom hole pressure is affected little by hydrate phase transition, and it is allowable not to consider hydrate phase transition when the bottom hole pressure is calculated; shut-in casing pressure cann't truly reflect gas kick due to hydrate formation and the situation is getting worse with time

模拟计算结果表明:溢流期间,天然气水合物的生成区域会随着循环流量的增大或抑制剂浓度的提高而减小,可通过增大流量和抑制剂浓度使水合物的生成区域脱离海底,减小防喷器管线被堵塞的危险;水合物的生成使环空中气体体积分数降低,泥浆池增量减小,给溢流检测带来延迟;当检测到有气侵发生时,水合物藏分解速率比较小时,井筒中生成水合物的可能性要比分解速率大的情况下更为严重;水合物相变对井底压力的影响较小,在工程中计算井底压力时可以忽略;由于天然气水合物的生成使得关井套压值不能真实反应气侵情况,而且随着时间的增加情况会更加严重。

Experimental results show that the water velocity is that when the BV ammonia concentration of 50 mg, L - 1 simulation wastewater and 98 mg, L - 1 point of industrial wastewater, penetrate respectively C/C0 = 0.3 and 0.15, water column of natural zeolite could handle respectively; 126 BV, 43 BV Modified zeolite column can handle respectively 157 BV, water, and with 46 BV hydraulic load increases, zeolite column can reduce water treatment, The experiment was found to leak after 8 NaCl solution with zeolite desorption regeneration effect is good, low cost, regeneration of zeolite adsorption capacity decrescent, Test through dynamics analysis found that zeolite column of ammonia nitrogen adsorption fast.

实验结果表明,进水速度为2.72 BV时,通入氨氮浓度为50 mg·L-1的模拟废水和98 mg·L-1的工业废水,此时穿透点分别为C/C0=0.3和0.15时,得到天然沸石柱可处理水量分别为126 BV、43 BV;改性后沸石柱可处理水量分别为157 BV、46 BV,且随水力负荷增大,沸石柱可处理水量减小;试验还发现对泄露后沸石用8%NaCl溶液解吸再生效果好,成本低,再生后的沸石吸附容量变小;试验通过动力学分析发现沸石柱吸附氨氮速度较快。

These spheres grew gradually as the culture time extended and the diameter reached to 1mm after 3 weeks of culture. These spheres could be continuously passaging in DMEM/F12 + bFGF + EGF.

随着培养时间延长,微球体直径逐渐增大,3周左右可达到1mm左右,在体外可连续传代,形成新的微球体。

Cylinder, the cylinder sets of radial a surplus deformation of the cylinder sets a great impact on the cylinder liner reduced radial a surplus amount to reduce the deformation of the cylinder sets, the top surface of the body decreases roughness, but it will increase the body on the plane cylinder only mouth the roughness ; Preload reduced cylinder head bolt deformation of the cylinder liner little effect, the body can reduce the top surface roughness and cylinder body on the plane I ended roughness; Shen appropriate reduced cylinder head bolt hole deep can reduce the deformation of the cylinder sets, but will cause the body and the top surface roughness on the cylinder body only I roughness increases Plane .

工作工况下,对于第2缸来说,气缸套径向过盈量对气缸套变形影响很大,减小气缸套径向过盈量,有利于减小气缸套的变形,减小机体顶面不平度,但会增大机体上缸套止口平面的不平度;减小缸盖螺栓预紧力对气缸套变形影响很小,可减小机体顶面不平度和机体上缸套止口平面的不平度;适当减小缸盖螺栓沉孔深可以减小气缸套的变形,但会造成机体顶面不平度和机体上缸套止口平面不平度的增大。

This research take late-maturing variety adzuki bean Jihong-4 as the experiment material, After the photoperiod inducement at different leaf ages treatment, the result showed that the activity of NR under LF treatment is higher than CK treatment on the whole, and is lower than SD treatment; The content of the dissociation amino acid under these three treatments show a descend trend along with the leaf ages accretion, but the inducement increasing the content of dissociation amino acid, different leaf ages leaves show some difference, and alternating rise with SD treatment; Inducement can reduce the content of soluble sugar, and continuous inducement shows a accumulation effect; 2LF is the most sensitivity stage for soluble protein under photoperiodic inducement, From this stage, each leaf indumenta can reducing the content soluble protein, but continuous inducement reducing rising it.

本研究通过光周期诱导的方法,对中晚熟品种冀红4号红小豆进行不同叶龄进行处理,结果表明:所有叶龄处理下硝酸还原酶活性基本高于自然光处理而低于连续短日照处理下的;随着叶龄增大,各处理游离氨基酸总量均呈下降趋势,但光周期诱导可提高游离氨基酸含量,不同叶龄表现有所差异,与连续诱导交替上升;诱导可降低可溶性糖的含量,并连续诱导出现累积效应;2LF是光周期诱对可溶性蛋变化最敏感的时期,这个时期起单个叶龄诱导可降低可溶性蛋白含量,但连续诱导却可提高;LF处理下的类胡萝素总体含量高于另两个处理,而LF处理下的叶绿素含量在仅3叶龄前高于CK处理下的,随后出现下降趋势。

The epoxidation can be performedwell when the concentration of quaternary ammoniumsaltand sodium tungstate is 0.06 mol/L and 0.03 mol/L, respectively.

结果表明,季铵盐和钨酸钠的浓度分别为0.06,0.03 mol/L时的催化效果最佳;α-和β-蒎烯的转化率随着H2O2与蒎烯的量比增大而增大,当H2O2与α-蒎烯和β-蒎烯的量比分别为2.0和1.8时,其转化率均可达到100%;较高的温度不利于环氧化反应的进行,因此,环氧化反应温度需控制在20℃以下。

As the loading increases count of hit and AE energy increases markedly. This proves that safety assessment of crane beam by AET is fully creditable. It can accurately evaluate the critical degree of crack and the safety reliability of the crane beam.

随着载荷的增大,撞击计数和声发射能量都明显增大,这证明用声发射技术进行起重机梁的安全评价是完全可靠的,它可准确地评价裂纹的危险级别和起重机梁的安全可靠性。

It was clear that the Cherenkov radiation is result of the coupling between the slow TM mode propagated along the waveguide and the negative-energy space-charge mode propagated along the beam, and the coupling strength is proportional to the beam density.

分析结果表明:切伦科夫辐射是由沿介质同轴波导传播的慢波与沿薄环形相对论电子注传播的负能空间电荷波耦合所致,且其耦合强度与电子注的密度成正比;输出频率和波增长率随着填充等离子体密度的增大而提高;保持一定的输出频率,增大电子注的束流可得到高的微波输出功率。

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Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克,果实色泽鲜艳,汁多味浓,甜酸适口,离核仁甜,清末时就驰名陕、甘两省,清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异:红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感,ED90值分别为47.65、71.67和29.17g/hm2;春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感,ED90值分别为96.91、114.20g/hm2;而番茄不敏感。

However, I have an idea.

不过,我有个主意。