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The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱，以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相，流速1ml/min，检测波长210nm，柱温40℃。结果阿奇霉素的线性范围为50.3～1006μg/ml，平均回收率100.1%，r=1.0000，RSD=0.8%(n=9)。

The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

采用C8柱，以0.045mol/L磷酸二氢胺溶液∶乙腈(2∶1)(用三乙胺调pH至7.35)为流动相，流速1ml/min，检测波长210nm，柱温40℃。结果阿奇霉素的线范围为50.3～1006μg/ml，平均回收率100.1%，r=1.0000，RSD=0.8%(n=9)。

ABSTRACT Objective To establish an HPLC method for the determination of azithromycin powder.Method The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

阿奇霉素为氮杂内酯类抗生素，日抗基和《中国药典》2005年版［1］均采用微生物检定法测定其含量，《欧洲药典》4.6版和USP26版中均采用HPLC法，专属性较强，试验周期短，但均使用的是聚合物极性柱，《欧洲药典》柱温为70℃，USP采用电化学检测器，其采用的设备在我国药检部门尚未普及［2］。

Anhui Institute for Drug Control, Hefei 230051ABSTRACT Objective To establish an HPLC method for the determination of azithromycin powder.Method The chromatographic conditions were as followed: C8 column, 0.045 mol/L ammonium phosphate monobasic solution∶acetonitrile (2∶1)(adjusted to pH7.35 with triethylamine) as mobile phase, temperature: 40℃, the flow rate: 1.0 ml/min, detection wavelength: 210nm.

阿奇霉素为氮杂内酯类抗生素，日抗基和《中国药典》2005年版［1］均采用微生物检定法测定其含量，《欧洲药典》4.6版和USP26版中均采用HPLC法，专属性较强，试验周期短，但均使用的是聚合物极性柱，《欧洲药典》柱温为70℃，USP采用电化学检测器，其采用的设备在我国药检部门尚未普及［2］。

A method for the determination of phenol and catechol in tobacco leaf by high performance liquid chromatography with methanol and 0.05 mol/L of monopotassium phosphate as mobile phase at a flow rate of 0.5 mL/min was described. Phenol and catechol were extracted from tobacco sample by distillation and solid phase extraction with Sep Park C 18 cartridge.

引 言挥发酚是烟草中一类重要的成分，它在烟草燃烧时直接进入烟气，大多有不好的气味，而且很难被掩盖；特别是苯酚和儿茶酚对呼吸系统有腐蚀作用和助癌作用，近年来逐渐引起了烟草化学工作者的注意〔1〕。

The HPLC condition consisted of C18 column(250 mm×4.6 mm,5 μm),mobile phase of 0.1 mol/L monopotassium phosphate-methanol(70 : 30,v/v) at the flow rate of 1.0 mL/min and at detection wavelength 280 nm.

本法采用C18色谱柱，流动相为0.1mol/L磷酸二氢钾溶液(用磷酸调节pH值至2.5)-甲醇的混合溶液(按v∶v=70∶30配制)，检测波长为280nm，流速为1.0mL/min。

Inosine -5'- monophosphate (5'-IMP) and guanosine-5'-monophosphate (5'-GMP) in samples were separated successfully using an Inertsil ODS-3 column (250 mm×4.6 mm, 5 μm) when 0.02 mol/L monopotassium phosphate (pH 4.5) was employed as the mobile phase with a flow rate of 1.0 ml/min at 250 nm and 25℃.

采用Inertsil ODS-3色谱柱(250 mm×4.6 mm， 5μm)；以0.02 moL/L磷酸二氢钾溶液(pH 4.5)为流动相，流速1.0 mL/min，柱温25℃，检测波长250 nm，同时分离了样品中5'-鸟苷酸二钠和5'-肌苷酸二钠。

(1-x)BiScO3-xPbTiO3 ceramics exhibits excellent dielectric and piezoelectric properties in the vicinity of the morphotropic phase boundary (x=64.0% mol fraction PbTiO3), which separates the rhombohedral phase from tetragonal phase.

(1-x)BiScO3-xPbTiO3陶瓷在x=64.0%附近存在一个从菱方晶系过渡到四方晶系的准同型相界，在此相界附近材料能获得优良的介电和压电性能。

BiScO3-xPbTiO3 ceramics exhibits excellent dielectric and piezoelectric properties in the vicinity of the morphotropic phase boundary (x=64.0% mol fraction PbTiO3), which separates the rhombohedral phase from tetragonal phase.

(1-x)BiScO3-xPbTiO3陶瓷在x=64.0％附近存在一个从菱方晶系过渡到四方晶系的准同型相界，在此相界附近材料能获得优良的介电和压电性能。

In the presence of an opioid analog,DAMA10(-13～10(-10)mol/L,human granulocytes and Mytilus edulis immunocytes were incubated with or without ligands at 37℃ for 10 minutes and at 23℃ for 20 minutes, respectively.

将人粒细胞和Mytilusedulis免疫细胞分别与不同浓度的类鸦片肽DAMA（10（－13）～10（－10）mol／L）或δ拮抗剂在37和23℃保温10～20min，用计算机显微图像分析法分析两种细胞的活化情况。

This paper designs the communication system of radio telescope FAST.

针对500m口径球面射电望远镜FAST分布式控制系统的特点完成了其通信系统的设计。

Political sheep's step-by-step a large number of fossils unearthed in the county soil Ma Ali after rural village in the middle of sallow pelitic siltstone.

步氏和政羊化石大量出土于广河县阿力麻土乡后山村，产于灰黄色泥质粉砂岩中。