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We have developed new types of pesticide with broad spectrum,high efficiencyand low poison.At present,we have six TC including insecticide,weedicide,bactericide and four series intermediates used in medicine,pesticide and dyestuff.

大力发展广谱、高效、低毒的新型农药，目前已形成前后一体化产品体制，包括杀虫、除草、杀菌六大原药以及用于医药、农药和染料的四大系列的中间体产品。

Methoxystilbene and 2-methoxy-4'-nitrostilbene were synthesized from benzyl chloride and nitrobenzyl chloride by the Wittig reaction, and used as intermediates for the synthesis of the final product fluorescent whitener FP4,4'-bis(2-methoxystyrylbiphenyl via reduction and diazotisation of the latter followed by reaction with the former in the presence of NaOH.

以氯化苄和对硝基氯苄为原料，经Wittig反应合成中间体：2-甲氧基-二苯乙烯和2-甲氧基-4'-硝基-二苯乙烯。后者经还原反应、重氮化反应后，在氢氧化钠存在下与前者反应生成最终产品荧光增白剂FP4，4'-双-2-(甲氧基苯乙烯基联苯。为该类荧光增白剂的合成开辟了一条新路线

Therefore esterification crosslinked reactionbetween polyearboxylic acid and wood can be quantitatively determined.According toexperiment results of stereoscopic configuration choices by crosslinking agents,crosslinkingreaction between model of reaction intermediate and wood,and the intermediate characteristic incrosslinking reaction,crosslinking reaction intermediate was proofed.We can infercrosslinking reactions between polycarboxylicacid and wood want through a mechanism of twosteps reaction process,the first cyclic anhydrides were formed as intermediates by dehydratingbetween hydroxyls in polycarboxylic acids,second esters were occurred by substitution reactionbetween wood hydroxyls and cyclic anhydrides.

从而可全面定量表征木材与多元羧酸类化合物的酯化交联反应；依据交联剂立体构型选择性、反应中间体模型物与木材的交联反应和交联反应中间体的波谱特征实验结果，证实了交联反应中间体，因此可以推测：多元羧酸类化合物与木材化学组分的交联反应是经历两步反应的机理，首先多元羧酸中相邻羧基的羟基之间脱水形成五元环酸酐中间体，然后木材的羟基与酸酐发生亲核取代反应形成酯。

Furthermore, through molecular structural design, we have also synthesized stable dual functional diphenylether polymer intermediates of ABB' types possessing ortho-dicarboxylic at one aromatic ring and diamine groups at another beginning from Xylenol and 1-Chloro-3,4-dinitrobenzene as the raw materials.

中文摘要本研究应用自氧化法与氢化法两反应，成功而有劾地制备出芳香族含酸酐及二胺基之官能基单体，并进一步经由分子结构设计，从3，4-二甲苯酚及1-氯-3，4-二硝基苯为原料，转化合成出安定性高带有羧基与双胺基双官能基之堑新ABB'型二苯醚中间体，并成功地应用此中间体从事自聚合反应，而合成分歧状聚醚亚醯胺高分子。

Xylitol is a kind of nutritional value of sweet substances, but also the human metabolic intermediates.

木糖醇是一种具有营养价值的甜味物质，也是人体新陈代谢的中间体。

Lots of new production technologies to enhance the competitive power of products have worked out in China's companies such as technologies for producing vitamin C manufactured via two-step zymosis; synthesizing chemically vitamin E with the domestically produced key intermediates linalool, isophytol and trimethylphenol; preparing vitamin B2 gained by genetically engineered bacterium fermentation, and commercialized production of vitamin H, etc.

我国企业研究出许多维生素生产新工艺，提高了产品的竞争力，开发的新工艺有两步发酵法生产维生素C，化学合成维生素E的关键中间体芳樟醇、异植物醇和三甲基苯酚等原料国产化，基因工程菌发酵生产维生素B2，维生素H的工业合成等。

It manufactures heterocyclic, such as pyrazine, thiazole, furan, pyridine and sulf-compounds with their ramifications; and pharmaceutical intermediates such as veratraldehyde, isovanillin, sufurol, diacetyl, acetoin, and 2, 5-dimethyl pyrazine.

食用产品有吡嗪、噻唑、呋喃、吡啶等杂环系列及含硫系列的合成香料化合物。医药中间体产品有：藜芦醛、异香兰素、硫噻唑、丁二酮、乙偶姻、2，5-二甲基吡嗪等。

Yields from chiral bisoxazolines (5a) with diethyl oxalate using NaOCH〓 as base for the first time. The structures of chiral multioxazolines and their intermediates, multi (β-hydroxylamide) s, were characterized by 〓H NMR, IR, mass spectra and elemental analysis. The catalytic activities and enantioselectivities of chiral multi (β-hydroxylamide) s (4) and chiral multioxazolines (5～8) were investigated by using acetophenone and β-acetonaphthone as former chiral ketone, KBH〓 or NaBH〓 as reductive reagent in chapter three.

在此基础上，对合成方法作了创新，以羧酸或酯为原料，在无催化剂的条件下与手性α-氨基醇反应，通过回流分水或脱醇的方法，一步反应合成了手性多噁唑啉（5～8），产率为89.2%～98.4%；以手性双噁唑啉（5a）为原料，在NaOCH〓的作用下，与草酸二乙酯反应，首次合成了呋喃类双嗯唑啉（6a），产率为72.9%～75.6%。

These new ionic liquid-supported acetylacetone catalysts were used for the oxidation of the intermediates of Vitamin E (2,3,5-trimethylphenol and 3,5,5-trimethylcyclohex-3-en-l-one). It not only checked the rationality of the design, but also established the base for the green oxidation of corresponding reactions.

论文进一步将此类离子液体支载乙酰丙酮金属催化剂应用于维生素E中间体三甲基苯酚和β—异佛尔酮的氧化过程，一方面检验了催化剂设计过程及结果的可靠性，另一方面为相关氧化反应的绿色化改造提供相关的基础。

The E-TOF will also be feasible and practical to assist chemists in screening the optimal reaction condition or evaluating the overall efficiency of different catalytic systems for a specific asymmetric reaction.4.For the first time,we explored chiralγ-hydroxy-α,β-acetylenic esters,which were prepared via asymmetric alkynylation,as key intermediates to the synthesis of chiralγ-butyrolactones. This convergent and enantioselective approach to chiralγ-butyrolactones is practical and easily handled with protecting group free.

这一概念包括反应产率、对映选择性、配体用量以及反应时间四个重要反应参数，不仅适用同一反应不同催化体系的横向综合性评价，而且适用于某一特定反应催化体系的优化过程，有助于研究人员选择最佳的反应条件。4、我们发展了以手性γ-羟基-α，β-炔酸酯为关键中间体完成了手性γ-丁内酯类天然产物的对映立体选择性全合成，该关键中间体能够以我们的催化体系方便的对映选择性合成，之后的官能团转换方法成熟，易于操作，无需进行繁琐的官能团保护和脱保护过程，绿色经济。

Foods high in this vitamin include oily fish such as salmon, tuna and, and fish liver oils.

维生素D含量高的食物包括诸如大麻哈鱼、金枪鱼和鲭鱼之类的油鱼以及鱼肝油。

We need you to cosign our public letter demanding that press intimidation cease immediately, and that all charges be dropped.

我们需要您cosign我们的公共信，要求记者立即停止恐吓，并要求所有收费下降。