查询词典 for the first time

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法：利用正交设计试验L9(3~4)确定原料药提取工艺为：10倍量90％乙醇提取两次，第一次40分钟，第二次30分钟；醇提液用10倍量水沉；沉淀加6倍量石油醚40℃脱脂；用1mol／L的NaOH溶液碱洗，除去酸性杂质；以碱性氧化铝柱，以环己烷／丙酮为洗脱溶剂，在环己烷-丙酮(6：4)段富集到所需活性部位，洗脱剂用量为3VB。

For the first time, in [3] the authors discussed the inequalities of B-B and by using them the authors give a proof of the existence and uniqueness of the generalized solution for magnetostatic field problem with zero boundary value. By using the inequalities of B--H in, in[-5,6] the authors give a proof of the existence and uniqueness of the generalized solutions for 3-D magnetostatic field Neumann problem and 2-D magnetic field first boundary value initial problem.

前人已讨论了B—H间的几个基本不式，并由之证明了三维静磁场带零边值问题广义解的存在与唯一性，作者也曾利用给出的B—H间的不式证明了三维静磁场Neumann问题和二维时变场第一边值初值问题广义解的存在与唯一性。

Today, as she munched meditatively, she was telling herself, not for the first time, that there was a time and place for everything – and that the office was definitely not the place for imitations of the boss's wife.

今天当她一边沉思一边用力咬动下颚时，她告诫自己：做事要看时间地点－办公室绝不是模仿老板娘的地方。

The security of PKI system itself is especially emphasized during the system design and implementation process, which is in accordance with the pervasive characteristic of PKI. Second, the concept of a Trusted Key Management Center is introduced for the first time. This technology greatly strengthens key management practices and allows for smooth transition from PKI to Key Management Infrastructure. Third, certificate status mechanisms are investigated in depth, and a certificate revocation performance simulation system is devised. All these work will provide guides to practice and employment of PKI applications. Based on time constraints, a new taxonomy for authenticated dictionaries is proposed. Fourth, formal analysis ofOCSP protocol is carried out; then an efficient and scalable OCSP system is developed. Fifth, the special requirements caused by the working environments of Wireless PKI are analyzed. Based on communicative hashing and dynamic Merkle hash tree, an efficient certificate status validation method suitable for WPKI is presented. Sixth, one important kind of fair exchange protocols is studied, and a new CEMBS based on RSA cryptosystem is proposed. Afterwards, a novel fair exchange protocol totally based on RSA signature scheme is devised.

在系统设计和实现的过程中，考虑到PKI作为普适性安全基础平台的特点，特别强调PKI系统自身的安全性；第二，首次在PKI系统的设计中提出了"可信密钥管理中心"的概念，这一独特设计大大地强化了密钥管理功能的实施，为PKI向密钥管理基础设施的平滑过渡提供了良好的技术准备；第三，对证书状态验证机制进行了深入研究，设计了证书状态模拟系统，以指导PKI系统和应用的部署和实施；在此基础上，基于时间约束首次给出了认证字典的一种新的分类方法；第四，对OCSP协议进行了形式化分析，设计和实现了一种高效、可扩展的OCSP系统；第五，分析了WPKI工作环境对设计安全基础平台提出的特殊要求，结合无线移动设备的具体特点，基于可交换杂凑函数和动态Merkle杂凑树设计出了一种适用于WPKI环境的高效证书状态查询机制；第六，对一类公平交换协议进行了深入的研究，从设计公平交换协议的密码基础结构出发，提出了一种新型的基于RSA密码体制的高效CEMBS；在此工作的基础上，设计了一种基于RSA密码体制的最优化公平交换协议。

The security of PKI system itself is especially emphasized during the system design and implementation process, which is in accordance with the pervasive characteristic of PKI. Second, the concept of a Trusted Key Management Center is introduced for the first time. This technology greatly strengthens key management practices and allows for smooth transition from PKI to Key Management Infrastructure . Third, certificate status mechanisms are investigated in depth, and a certificate revocation performance simulation system is devised. All these work will provide guides to practice and employment of PKI applications. Based on time constraints, a new taxonomy for authenticated dictionaries is proposed. Fourth, formal analysis of OCSP protocol is carried out; then an efficient and scalable OCSP system is developed. Fifth, the special requirements caused by the working environments of Wireless PKI are analyzed. Based on communicative hashing and dynamic Merkle hash tree, an efficient certificate status validation method suitable for WPKI is presented. Sixth, one important kind of fair exchange protocols is studied, and a new CEMBS based on RSA cryptosystem is proposed. Afterwards, a novel fair exchange protocol totally based on RSA signature scheme is devised.

在系统设计和实现的过程中，考虑到PKI作为普适性安全基础平台的特点，特别强调PKI系统自身的安全性；第二，首次在PKI系统的设计中提出了"可信密钥管理中心"的概念，这一独特设计大大地强化了密钥管理功能的实施，为PKI向密钥管理基础设施的平滑过渡提供了良好的技术准备；第三，对证书状态验证机制进行了深入研究，设计了证书状态模拟系统，以指导PKI系统和应用的部署和实施；在此基础上，基于时间约束首次给出了认证字典的一种新的分类方法；第四，对OCSP协议进行了形式化分析，设计和实现了一种高效、可扩展的OCSP系统；第五，分析了WPKI工作环境对设计安全基础平台提出的特殊要求，结合无线移动设备的具体特点，基于可交换杂凑函数和动态Merkle杂凑树设计出了一种适用于WPKI环境的高效证书状态查询机制；第六，对一类公平交换协议进行了深入的研究，从设计公平交换协议的密码基础结构出发，提出了一种新型的基于RSA密码体制的高效CEMBS；在此工作的基础上，设计了一种基于RSA密码体制的最优化公平交换协议。

This dissertation involves the study of the growth dynamics of colloidal particles under unequilibrium and irreversibility condition. Firstly, it is of interest to investigate whether the ideal diffusion or reaction-limited aggregation universal behavior can be observed for the initially polydisperse practical system of basic yttrium carbonate as well. The fractal structure of basic yttrium carbonate aggregate cluster was observed using transmission eletron microscopy. The aggregation kinetics of basic yttrium carbonate colloids was studed using dynamic 1ight-scattering techniques. At 1.00mol/l NaCl solution the fast diffusion-limited aggregation behavior was observed with an increase in the aggregate size over time described by a power law. The aggregates are characterized by a fractal dimension D=1.82. The disordered and ramified cluster is consisted of primary colloidal particles and tenuous and more open. These are in good agreement with those observed for other colloidal system such as colloidal gold (1.86), silica (1.85) and polystyrene latex (1.82) in diffusion-limited aggregation from the static and dynamic light scattering by Lin. Therefore ideal diffusion-limited aggregation behavior can be observed in practical polydisperse system as well. Smoluchwski and fractal theories were used to obtain the aggregation rate constant for initially polydisperse system for the first time.

本论文研究胶粒的非平衡不可逆聚集动态学，分为两个部分，第一部分是通过实验研究一个新的初始多分散的碱式碳酸钇胶粒实际体系中，聚集标度性质的普适性，即使用透射电子显微技术观测聚集粒子簇的分形结构，使用动态激光光散射研究碱式碳酸钇胶粒的聚集动力学，胶粒带电而产生静电排斥作用使得碱式碳酸钇胶粒处于稳定状态，当加入电解质NaCl溶液时，碱式碳酸钇胶粒间的Debye-Hückel屏蔽距离缩短，从而降低静电排斥能垒，引起胶粒发生不可逆聚集，加入电解质NaCl的浓度为1.00mol/l时，碱式碳酸钇胶粒进行快速聚集，经历扩散控制聚集机理，形成结构疏松、更为开放的分形聚集粒子簇，其分形维数为1.82，碱式碳酸钇胶粒聚集增长动力学遵循幂函数增长规律，与Lin等使用静态激光光散射和动态激光光散射测量硅胶(1.85)、金胶(1.86)和聚苯乙烯胶乳(1.82)在扩散控制聚集状态形成聚集粒子簇的分形维数值以及粒子簇聚集增长的动力学规律相一致，表明胶粒聚集标度性质的普适性质在初始多分散的实际体系中也是存在的，首次由动态激光光散射的实验数据得到初始多分散胶粒分形粒子簇的聚集速率常数，并且其值与Smoluchowski聚集速率理论预期相符。

The NMR data of compound 6 were completely assigned by 2D-NMR techniques,including1H-1H COSY, HMQC and HMBC spectra.This was the first time to report isolation of the compound 6 from natural product.The compounds 1-5 was isolated from the genus Galium for the first time.

化合物6为首次从天然产物中得到，并运用二维核磁共振波谱技术(1H-1H COSY，HMQC和HMBC)首次对其碳谱和氢谱数据进行了全归属，化合物1～5均为首次从该属植物中得到。

March 8 at noon, his joy to go home early and his mother reported to the class teacher is also the first time to eat Siwan rice for the first time his mother found his inner thoughts of a child!

3月8日中午，他欢天喜地的早早回家向他母亲报告了老师还在上课，第一次吃了四碗饭，他母亲第一次发现他的孩子内心的想法！

The intensity ratio of TO and LO inMCT was observed to be different. Such difference was explained in terms of the different Ramangeometry arrangement.〓. The laser-induced micro-photoluminescence in the range of 1000～5000〓(1.34eV～1.83eV) was found for the first time in LPE MCT epilayer. The center of photoluminescence wasat 2750〓 or 1.62eV and the FWHM of luminescence was 2000〓 or 0.25eV. We assume thatthe photoluminescence is due to recombination of electron from an anion vacancy resonance levelto the top of valance. In addition, new Raman shift was observed at 750〓 in LPE MCTepitaxial film.〓. The laser-induced micro-photoluminescence with quasi-periodic structure was observed forthe first time at room temperature in one of MOVPE MCT epitaxial film samples. The range offluorescence was from 1.46eV to 2.21eV, i.e., 1.73eV above the conduction band edge.

2首次在LPE生长的碲镉汞外延薄膜的显微Raman谱中，在1000～5000〓范围发现了激光激发显微荧光，该荧光的发光范围换算为电子伏特标度为1.34eV～1.83eV，荧光的发光中心大约位于2750〓，即1.62eV，发光的半峰高宽约为2000〓或0.25eV；指出该显微荧光来源于碲镉汞薄膜中的阴性离子空位共振能级的激光激发发光；观察到了碲镉汞外延薄膜中一个新的Raman散射峰，位于750〓位置； 3首次在一块用MOVPE方法生长的〓Te外延薄膜的显微Raman谱中，发现了1.46eV至2.21eV范围并伴随有周期结构的显微荧光峰，该发光峰对应的能带中心位于〓Te材料导带底上方1.73eV，通过研究得出样品在1.46eV至2.21eV范围的显微荧光峰是由于改进 MOCVD 生长工艺，提高了碲镉汞外延薄膜的结构质量所致；通过分析指出该显微荧光来源于外延层中的阴性离子空位的共振能级发光。

In 1992, Peter Kinder won election in his first campaign for the 27 th district in the Missouri Senate, representing the counties of Bollinger, Cape Girardeau, Madison, Mississippi, Perry, and Scott· In 2001, the Republicans gained a majority in the Missouri Senate for the first time in 53 years· As a result, Kinder was elected President Pro Tem, the top elected official in the Missouri Senate, and led this body for four years through some of the toughest budget times in Missouri history· When Kinder successfully ran for Lt· Governor in 2004, he became the second sitting President Pro Tem to be elected Lieutenant Governor

1992年，金得尔先生代表伯林格，开普吉拉多，麦迪逊，密西西比，佩里和斯科特区首次赢得密苏里州第27次参议院选举的胜利。由于2001年共和党在53年中首次赢得了密苏里州参议院选举的多数席位，金得尔先生当选临时参议院主席，在四年任期中领导参议院度过了密苏里历史上几次预算最为紧张的时期。他是历史上第二位成功当选副州长的临时参议院主席。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。