查询词典 X-ray diffraction

Effects of hexamethylene tetramine surfactant on morphology of the products are studied by using X-ray diffraction pattern, scanning electron microscopy.

制得的样品利用X射线衍射仪、扫描电镜及紫外分光光度计进行表征。

These compounds are of substantial interest both inviewpoints of theory and practical applications, mainlyunder the stimulus to achieve synthetic models either foractive sites of iron-sulfur proteins or for transitionmetal catalysts. This thesis describes the synthesis, structures andconformations of 51 new iron-sulfur cluster complexes,which have been characterized by elemental analysis andstandard spectroscopic methods. In addition, single-crystalX-ray diffraction analyses were performed for 4 representa-tive new compounds. Reactivities of μ-〓 with mono- and di- Grig-nard reagents derived intermediates toward various organicelectrophilic substrates were studied, along with complexa-tion of arynyl-containing iron-sulfur clusters by 〓Thus, several bridged, non-bridged, monomeric, dimeric,homonuclear, heteronuclear iron-sullfur and iron-sulfur co-balt-carbon cluster complexes were synthesized. A novelreaction and convenient route for the synthesis in highyield of tetranuclear iron complexes 〓 containing atetracoordinated sulfur atom was discovered, whereas aplausible mechanism based on experimental results was propo-sed for the formation of the new cluster type.

鉴于有机铁硫原子簇化学在基础理论发展和应用方面的重要意义，因此我们开展了这一课题的研究，并取得以下主要成果： 1、本文共合成了51个新有机铁硫及含钴碳簇基的有机铁硫原子簇配合物，除用元素分析，NMR，IR，MS法表征其结构和构象外，还用X-光衍射技术测得四个代表性配合物的单晶结构和构象； 2、我们业已发现炔基Grignard试剂同〓可形成一种&开环&与&闭环&中间物的平衡混合物，研究该平衡混合物同各种亲电试剂的反应； 3、研究发现了一种可高产率地形成〓含〓四配位硫挛合簇的新化学反应并对此反应提出了—种有趣的反应机理； 4、首次由1，4-二溴丁烷双Grignard试剂与〓制得一种新型铁硫簇双硫阴离子活性中间体，并进而研究了它的亲核反应性能； 5、找到了通过〓的光化学反应来合成簇合物〓-〓的一条有实用价值的新路线。

The mechanisms of phosphate sorption on hydrotalcite and its calcined product are different, which has been confirmed by X-ray diffraction examination.

水滑石及其焙烧产物对磷的吸附具有不同的机理，并得到了X射线衍射的证实。

Using Gassian98 with LANL2DZ basis sets, the quantum chemistry calculation of the model was performed.4. A series of ligands which all include imidazolyl group were designed and synthesized. The crystal structure of one of them was determined by X-ray diffraction.

设计并合成了一系列含有咪唑基的配体，应用X-射线衍射方法测定了其中一种配体的晶体结构，并用Gaussian98程序包进行了量子化学计算。

The granular morphology and size, molecular weight distribution, crystal structure, thermodynamic properties, structural character, digestibility and glycaemic-index of starch from Kabuli and Desi chickpeas cultivars were investigated using scanning electron microscope, high performance liquid chromotagraphy, X-ray diffraction, differential scanning calorimetry,infrared spectrum and other modern analytical methods.

采用扫描电镜、高效液相色谱、X射线衍射、差示扫描量热仪、红外光谱等现代分析手段探讨了Kabuli与Desi品种鹰嘴豆淀粉的颗粒形貌与大小、分子量分布、结晶结构、热焓性质、结构特征、消化性能及血糖生成指数。

The total of 36 compounds were characterized by X-ray single crystal diffraction, EA, TG, IR, luminescence, adsorption, XPS, powder XRD, M〓ssbauer spectra, EPR, magnetical measurements.

本论文利用水热法，成功设计和合成出三个系列Ln-M(M=Mn〓，Fe〓，Ag〓)共23个未见文献报道的稀土—过渡混合金属配位聚合物，同时也得到了结构新颖的仅含稀土或两种不同过渡金属的从一维到三维的聚合物13个，并对它们进行了结构、元素分析、热重分析、红外光谱、荧光、吸附、磁性、光电子能谱、粉末衍射和M〓ssbauer谱等表征。

In this thesis several magnetic multilayers(Co/Pb,Fe/Si,and NiCo/Cu)were prepared by rf sputtering,the structure and magneticproperties were studied by using x-ray diffraction,vibrating samplemagnetometer,torquemeter,ferromagnetic resonance,magnetoresistanceand magnetooptical Kerr effect.

本文对用磁控射频溅射方法制备的Co/Pb，Fe/Si，NiCo/Cu等三个系列的磁性多层膜样品的结构和磁性，层间耦合与磁光效应的关联进行了系统的研究。研究中使用了X射线衍射仪，振动样品磁强计，转矩仪，铁磁共振，磁电阻和磁光等测量与实验方法。

Martensitic transformation in the binder of a WC-Co cemented carbide was investigated by means of X-ray diffraction and transmission electron microscope.

采用了X射线和透射电镜对WC-Co硬质合金中粘结相的相变进行了研究。

The metallograph, x-ray diffraction, TEM, EMPA and XPS technigues were used to research the microstructure, phase structure, microhardness, composition, Valence of composed elements, internal stress of coatings, and to measure the wear-resistance and resistance to high-temperature oxidation, too.

文中应用金相分析、X-射线衍射法、透射电镜、电子探针显微分析法和X-射线光电子谱法等手段研究了N膜的显微组织、相结构、显微硬度、膜层成分、组成元素的价态和膜层内应力等性能；还测定了铝合金表面的N膜的耐磨性和抗高温氧化性能。

Sulfidation kenetics of studied materials have been examined and compared. The structure and morphological features of sulfide scales have been investigated using metallographical, X-ray diffraction and EMPA techniques.

测定并比较了这些合金的硫化腐蚀失重，通过金相、X光衍射相分析和电子探针技术分析研究了硫化物锈层的形貌和结构特征。

Chinese traditional virtue is humility and wariness,the compliment and praise to the others should be declination

中国人的传统美德是谦虚谨慎，对别人的恭维和夸奖应是推辞。如

We bought this house on the never-never.

我们以分期付款的方式买下这座房子。