锑的

In the medium of 0.013 mol/L H2SO4, phosphate reacts with sodium molybdate and potassium antimonyl tartrate, forming a yellowish phosphorus-antimony-molybdenum heteropoly acid. The acid exhibited a strong resonance scattering peak at 710 nm after added with nanogold. The heteropoly acid was reduced by ascorbic acid to antimony phosphomolybdate blue, which caused the decrease of resonance scattering intensity.

在0.013mol/L H2SO4介质中，磷酸根与钼酸钠、酒石酸锑钾反应生成淡黄色的磷锑钼杂多酸，加入纳米金后在710nm处产生一个较强的共振散射峰，抗坏血酸可将磷锑钼杂多酸还原为磷锑钼蓝，导致710nm处共振光散射信号降低。

From the perfusion experiments with isolated rabbit heart and vessels were obtained the follow- ing results:(1)Potassium antimony tartrate produced depression of the isolated rabbit heart,and this depressant action became more marked when the pH of the solution was raised from the original value of 5.4 to that of 7.2;(2)At the same pH levels,the cardiac action of the potassium salt was slightly stronger than that of the corresponding sodium salt;(3)The slight vase-dilator effect of potass- ium anti...

从离体器官的灌注实验得到下列结果：(1)酒石酸锑钾对离体兎心有抑制作用，将其pH 从5.4调整到7.2时，作用亦随以增加。(2)在相同 pH 时，酒石酸锑钾的心臓抑制作用较酒石酸锑钠略强。(3)酒石酸锑钾对离体兎耳血管的轻微扩张作用，系由于该药溶液的微酸性反应，当将药液 pH 调整至7后即无作用。(4)对于离体兎肺血管则不问 pH 为4.8或7，均产生轻微的血管收缩作用。

To December 31, 1997 ended, the company has an annual production capacity 10,000 tons of production capacity of antimony series products, has developed a catalytic antimony trioxide, antimony sodium, five antimony oxide, antimony oxide dust and other 14 kinds of antimony new products, become the country's antimony industry the most complete variety of enterprises, is the second largest - producer of antimony products.

至1997年12月31日止，公司已形成年产10000吨锑系列产品的生产能力，先后开发出催化型三氧化二锑、锑酸钠、五氧化二锑、无尘氧化锑等十四种锑系新产品，成为全国锑行业品种最为齐备的企业，是全国第二大-锑品生产企业。

Grew on the normal temperature, it was shown that the deposits of calcium antimonate being the indicator for Ca(superscript 2+) localization mainly concentrated within the vacuoles and intercellular spaces and there was also some Ca(superscript 2+) deposits in cell walls. But when Garyota urens L. was treated by the temperature of 2℃ for 48 h, the level of Ca(superscript 2+) increased in cytoplasm and plasma membrane, but decreased in vacuoles and intercellular spaces considerably. At the same time, the ultrastructure of chloroplasts suffered from chilling: the membrane of chloroplasts had been damaged, the layer of thylakoids was exiguous and unclear, the photosynthetic rate decreased evidently. And when Garyota urens L. was treated by the temperature of 2℃ for 120 h, the deposits of Ca(superscript 2+) mainly concentrated within the cytoplasm, nucleus and plasma membrane and there was also some Ca(superscript 2+) deposits in vacuoles, and the ultrastructure of some cells was simultaneously damaged severely: Chloroplasts structure, vacuole membrane and nuclear membrane had been damaged fully, the structure within the cell had become unclear, and the cell only have respiration.

研究结果表明，未经低温处理的董棕幼苗叶肉细胞，焦锑酸钙沉淀颗粒大量出现在液泡和细胞间隙中，细胞壁中也可见少量沉淀，而细胞基质中则看不到焦锑酸钙沉淀；经2℃ 48 h低温处理后，细胞基质和细胞膜上焦锑酸钙沉淀增加，而液泡和细胞间隙中的焦锑酸钙沉淀则显著减少，并且超微结构已初步显示出寒害的特徵，叶绿体外膜部分破损，类囊体片层稀疏且排列不规则，光合速率明显下降等；经2℃ 120 h低温处理后，细胞间隙内的焦锑酸钙沉淀极少，有的也紧贴在细胞外壁上，而细胞基质和细胞膜上则分布有非常多的焦锑酸钙沉淀，在核基质和液泡中也可见到少量的焦锑酸钙沉淀，并且超微结构遭到了显著破坏，叶绿体结构完全被破坏，核膜与液泡膜严重破损，内部结构模糊，细胞只表现为呼吸作用，不进行光合作用。

A series of antimony mercaptide compounds which formula are Sb 〓 and Sb S (CH〓〓COOR 〓(R represents an alkyl or aryl, aralkyl, n=0～2) have been synthesized. A new synthetic method has been invented to solve the defect of abroad patent method which has complex technological conditions and singleness intermediate compounds. A new catalyst QL-1 and preactivated antimony trioxide and other means have been used to avoid neutralizing, washing, separating and other procedures of intermediate and simplifing process flow at the same time. According to this new technique, a series of antimony mercaptides and their intermediate products have been synthesized with high yield.

合成了结构为SbS(CH〓〓COOR〓及Sb〓（R为烃基或芳烷基，n=0～2）的一系列硫醇锑化合物，针对国外专利报道的合成工艺存在着工艺条件苛刻，同时需多步完成，操作复杂，而且中间体品种单一的缺陷，发明了一种一步法合成硫醇锑化合物的新工艺，采用QL-1催化剂，且将三氧化二锑预先活化，变固—液相反应为液—液相反应，同时可免除中间体的中和、洗涤、分离等工序，工艺流程简化，产品收率高，且能制得系列硫醇锑产品。

The basic reason for oxygen concentration reduction in heavily Sb-doped CZSi was that oxygen solubility decreased when element Sb with larger radius doped degenerately into silicon crystal.

为解释重掺锑硅单晶中氧含量较普通直拉硅低，且随着掺锑量增加，氧含量下降，而重掺硼硅单晶中氧含量并不降低这一实验事实，应用热力学计算，得到重掺锑硅单晶生长时，生成Sb〓O〓的反应不能自发进行，因此不会因Sb〓O〓的大量挥发而使重掺锑硅单晶中氧含量降低。

Commodities subject to export quota license are: corn, rice, wheat, cotton, wood products, live ox, live pig, live chicken, natural silk and its products, coal, coke, crude oil, finished oil, rare-earth metal, antimony oxide ore, antimony and antimony products, antimony oxide, tungsten ore, Ammonium Paratungstate, Ammonium metatungstate, Tungsten Trioxide and Blue Tungsten Oxide, Tungstic acid and salt, tungsten powder and its products, Zinc ores, Tin ores, tin and tin-base alloy, and white silver.

实行出口配额许可证管理的货物是：玉米、大米、小麦、棉花、锯材、活牛、活猪、活鸡、蚕丝类、煤炭、焦炭、原油、成品油、稀土、锑砂、锑及锑制品、氧化锑、钨砂、仲钨酸铵及偏钨酸铵、三氧化钨及蓝色氧化钨、钨酸及其盐类、钨粉及其制品、锌矿砂、锡矿砂、锡及锡基合金、白银。

A new technology preparation of pentachloride antimony from antimony-rich lead anode slime was developed, which is significant for the comprehensive use of antimony and improving the downstream processing of antimony products.

提出了处理铅阳极泥制备五氯化锑新工艺，并对五氯化锑水解过程进行了研究，这对锑资源的综合利用，提高锑品的深加工能力具有十分重要的意义。

The initial products of neutralization-conversion contain oxychloride, cubic and orthorhombic antimony white. The final products turned into single cubic antimony white.

在酒石酸根离子存在的情况下，氯氧锑中和转化初期产物物相含有氯氧锑、立方晶型和斜方晶型锑白，随着时间的延长，完全转化为单一的立方晶型锑白。

In the neutralization transforming process of antimony oxychloride, it will be more convement to form the metastable phase in theory, orth. Sb〓O〓, which stably exist all along in fact.

论文首先通过理论分析与实验研究，揭示了锑白湿法生产工艺中粉末结构形貌控制机理：(1)斜方晶型锑白的单位晶胞内所含分子数比立方晶型锑白少，结构与单斜晶型氯氧锑相似。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。