试剂

Results The appearance of negative value was due to insufficient reagent purity, finding out in original absorption curve. The reagent contained chemicals besides response theory.

结果 从原始吸光度值的曲线上找到出现负值的原因是试剂纯度不够，试剂中含量有反应原理以外的化学物质。

The optimum reaction conditions are as follows: diphenylmethanethiol : methyl chloroacetate is 1:1.5, and the reaction carried out at 100℃ for 4 h, 2- acetamide can be carried out in the room temperature for 20 h, the yield of 2- acetamide was 76%, hydrogen dioxide: 2- acetamide is 1:1, and the reaction carried out at 60℃ for 3 h, the yield of modafinil was 79%, the total yield of reaction can be reached 48%.

研究表明，采用氯乙酸甲酯作为醚化试剂，反应时间4h，反应温度100℃，二苯甲硫醇：氯乙酸甲酯=1：1.5，室温下氨解反应20h，二苯甲硫乙酰胺收率76%；采用过氧化氢作为氧化试剂，反应时间3h，反应温度60℃，过氧化氢：二苯甲硫乙酰胺=1：l，莫达非尼收率79%，反应总收率可达48%。

Than between the rN-ELISA and IDEXX ELISA kit (90.8%), therefore the rNM-ELISA was selected as a optimal method to prepare kit for determine antibodies to PRRSV. The storage life of the rNM-ELISA kit at 4℃ and -20℃ was 12 months at least by adding protein stabilizer to reagents in the kit, this provided pig industry for our country with a serodiagnostic method which had advantages of high sensibility、strong specificity、long period of validity、safety and no shedding PRRSV.

将建立的rN-ELISA和rNM-ELISA分别与IDEXX ELISA试剂盒进行比较检测327份猪血清，结果rN-ELISA和rNM-ELISA的特异性差异不大，rNM-ELISA与IDEXX ELISA试剂盒的阳性符合率相对较高（92.3％），选择rNM-ELISA作为制备PRRSV抗体检测试剂盒的方法。

In the second chapter, p-hydrazino-benzenesulfonic acid was prepared by diazotizing sulfanili acid with sodium nitrite. The diazanium salt was then reduced with sodium hydrogen sulfite and acidified with sulfuric acid to give 83.4% product. After several repeated experiments, the reactant and reaction condition are determined.

由于Cy系列试剂的特殊结构使其在荧光标记方面与其他试剂相比有着显著的优点，在生物芯片和蛋白质组学方面得到了广泛的应用，因此文章综述了Cy系列试剂在DNA芯片和蛋白质组学研究中的标记方式以及应用。

In this project, we have prepared conveniently Si-Mg 1,1-difunctional group reagents-α-silylvinyl Grignard reagents by hydromagnesiation of alkynylsilanes; Se-Br 1,1-difunctional group reagents-α-bromovinylselenides by hydrobromination of alkynylselenides; Sn-Br and Sn-I 1,1-difunctional group reagents by hydrozirconation of alkynylstannanes followed by halogenating reaction.

本项目通过炔基硅烷的镁氢化反应，方便地制得了Si-Mg 1，1-双官能团试剂-α-硅基烯基镁化物；通过炔基硒醚的溴氢化反应，方便地制得了Se-Br 1，1-双官能试剂-α-溴代烯基硒醚；通过炔基锡烷的锆氢化反应，继而卤代方便地制得了Sn-Br和Sn-I 1，1-双官能试剂。

In the orthogonal designable experiment ,the analysis results of zirconium source, precipitation , the sulfating agent is 1.54%, 2.27%, 5.11%,respectively. This result show that the influence of sulfating agent to the catalytic activity is the biggest. Under the same density of the sulfuric acid soaks, the effect of sulfuric acid is well compared to ammonium sulfate .The second is the precipitation, but the influence of the zirconia source is the smallest.

正交设计实验中锆源、沉淀剂、硫酸化试剂的极差分析结果分别为1.54%，2.27%，5.11%，此结果说明硫酸化试剂对催化剂的影响最大，其次是沉淀剂，锆源的影响最小，同时表明以Zr(NO3)4·5H2O为锆源、乙胺为沉淀剂、硫酸为硫酸化试剂是催化剂的最佳制备方案。

There are three different nucleophilic reagent respectively reaction with m-dinitrobenzene ramification at distint alkaline term:With the nitrobenzene 、 m-nirtobenzenesulfone sodium salt 、 2.4-dinitro chlorobenzene 、 m-dinitrobenzene for bottom thing, benzyl cyanide、 benzyl chloride、 benzyl chloropyridine、is a nucleophilic reagent reaction for under the different term proceeds a series reaction. At the same time ,discuss about the impact factor to nucleophilicity such as the number of attract electron group、 ability of attract electron and the nucleophilic substitution reaction part.

设计了三类不同的亲核试剂分别与活化芳环在不同的碱性条件下发生反应：以苄基氰、苄基氯化吡啶为亲核试剂，以硝基苯、间二硝基苯、间硝基苯磺酸钠、2，4-二硝基苄基氯为底物进行亲核取代反应；并且对亲核试剂的体积效应、溶剂效应对亲核性影响，底物上吸电子基团的数目、吸电子能力对亲电性的影响，以及亲核取代反应的发生部位受哪些因素影响进行探讨。

Methods According to the drinking water legislation in Europe threshold: 0.10mg/L NO2(superscript -, a rapid spot test method for nitrite in water was established by using an optimized composition of reagent mixture and a binary positive/negative response, conducted as follows: a tablet of a mixture of solid reagents containing sulfanilamide, N-(1-naphthyl) ethylene diamine dihydrochloride and sodium chloride was put on a spot test plate of Teflon mould, then, a drop of 30% HCl and a drop of water sample were added on the reagent material.

根据欧洲饮水法规亚硝酸盐限值(0.10mg/L)，使用一种优化的试剂混合物和二元的阳性－阴性反应，建立一种水中亚硝酸盐快速点滴检验法。结果将1片含磺胺、N-（1-萘）乙二胺二盐酸盐和氯化钠的固体试剂混合物放在聚四氟乙烯模的点滴检验板上。加1滴30%盐酸和1滴水样于试剂片上。

Each test kit contains sufficient materials for 30 tests, including control and test latex reagents, positive and negative controls, mixing sticks, and pipettes.

每一个检测试剂盒包含供30次检测的试剂，包括包括对照和检测乳胶试剂、阳性和阴性对照、搅拌小棍和吸液管。

The effecting factors of the treatment of soil polluted by pentachlorophenol by Fenton reagent are determined by reading a large number of documentations.

通过查阅相关文献确定了Fenton试剂处理五氯酚的影响因子，并对各因子进行单因子分析，探讨了Fenton试剂的作用规律，确定了Fenton试剂法处理五氯酚的最佳处理条件。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。