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The average recovery was 99.1%.ConclusionThere is difference in the content of flavonoids of the different decocting methods of Qingjinningqi decoction.

结论不同煎煮方法的清金宁气汤中黄酮类成分的含量具有差异。

The decocting condition has effect on the dissolution rate and stability of the ingredients in Huanglianjiedu decoction.

煎煮次数对水溶性成分溶出影响不大,而对脂溶性成分的溶出影响较大。

Objective To analysis the effective ingredients in Huanglianjiedu decoction under different decocting conditions.

目的 以黄连解毒汤为例说明不同煎煮条件对中药汤剂有效成分的影响。

This method has also been successfully applied to determine the optimum time of the steeping and decocting process of Glycyrrhiza uralensis Fisch root.

该方法被成功地运用于测定甘草根的最佳浸泡和煎煮时间。

ObjectiveTo study the correlation between decocting time,administration dosage and the toxicity of Radix Aconiti.

目的揭示川乌煎煮时间、给药剂量与毒性的相关性。

Methods The detecting method of HPLC was established and the ingredients in Huanglianjiedu decoction under different decocting time and times were analyzed.

首先建立黄连解毒汤中多种有效成分的分析方法,对不同煎煮条件下中药汤剂中有效成分进行动态分析。

The majority of the poisoning cases were associated with excessive and/or long-term dosage,and improper preparation methods,such as decocting,heating or fumigating.

多数中毒病例为内服剂量过大及用药时间过长所致,其次为用药方法不合理,包括采用煎煮、加热熏蒸等。

Theevaluation of the efficiency of different extraction and ingredient-ingredientinteractions in the preparation decoction process has been studied.

同时还进行了生物碱萃取方法优化实验研究,并探讨了复方煎煮过程中成分-成分之间的相互作用。

Results: The optimum conditions for shuanghuanglian oral liquid by orthogonal test optimized process were as follows:water for ten times the quantity of medicinal materials in the process of decoction, ethanol with 75% in the process of deposition,pH with 7.0,12 hours about laying aside time.

结果:正交试验优选双黄连口服液制备工艺的最佳条件,即煎煮时加水用量为中药材的8倍,乙醇沉淀所用浓度为75%,pH值为7.0,静置时间为12h。

RESULTS The optimum conditions for shuanghuanglian oral liquid by orthogonal test optimized process were as follows: water for ten times the quantity of medicinal materials in the process of decoction, ethanol with 75% in the process of deposition, pH with 7.0, 12 hours about laying aside time.

结果表明正交试验优选双黄连口服液制备工艺的最佳条件,即煎煮时加水用量为中药材的8倍,乙醇沉淀所用浓度为75%,pH7.0,静置时间为12h。

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