有射线的

Experimental study of high temperature phase transformation for pyrophyllite

利用场发射扫描电镜表征了Zr-Co粉体的形貌特征和烧结后的陶瓷薄膜结构，热重分析了Zr-Co粉体烧结过程的失重和相转变吸放热过程，X射线衍射分析跟踪了不同温度段烧结体系的组成变化趋势，在此基础上对粉体烧结后陶瓷薄膜的防氧化效果进行了分析，结果表明：温度对粉体的颗粒形貌和晶相结构有较大的影响，高温烧结的粉体性质稳定，经过1200℃烧结后的陶瓷膜层具有很好的致密性，具有很好的防氧化效果。

SBA-15 samples obtained from both silica sources were highly ordered p6mm symmetric pillar structure,as was evidenced by XRD patterns,with similar surface area and slightly larger pore volume for the samples prepared from TEOS than those from sodium metasilicate.

通过X射线粉末衍射对样品进行表征，发现两种硅源合成的SBA-15都具有高度有序的二维六方立柱形结构。它们的比表面积相近，用TEOS作为硅源的SBA-15的孔容比用硅酸钠作为硅源的SBA-15的略大；用硅酸钠作为硅源的SBA-15有更高的微孔率和更厚的孔壁。

Notably, compounds 12–14 can be described as a 3D open–framework with nano–channels, compound 15 can be described as a 3D open–framework with double helical channels, while compound 16 can be described as a 3D heterochiral coordination polymer with double helical channels, which can be obtained by spontaneous resolution from the racemic phosphonic acid.X–ray powder diffraction analysis shows that compound 16 is a pure phase. Surface photovoltage spectroscopy of compound 16 indicates that it possesses positive SPV response in the range of 300–600 nm and shows p–type semiconductor characteristic.

值得注意的是，化合物12-14为具有一维纳米孔道结构的三维开放骨架结构，化合物15是具有双螺旋孔道的三维开放骨架结构，而化合物16是外消旋的有机膦酸配体通过自发拆分而形成的具有双螺旋孔道的多手性三维开放骨架结构。X-射线粉末衍射分析表明化合物16为纯相；化合物16的表面光电压光谱分析中，在300-600nm范围内有3个正的光(来源：ABC论文12网www.abclunwen.com)伏响应带，表明它具有p型半导体的特征；化合物16的诱导表面光电压谱进一步确定它的p型半导体的特征；磁性研究表明，化合物16中两Mn原子之间存在弱的反铁磁相互作用。

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8％, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察，在微球内外未发现尼群地平的完整结晶，X-射线粉末衍射和差示扫描量热试验结果也显示，尼群地平已经被高度分散在微球中；微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制；制备温度和搅拌速度对微球的质量影响较大；溶出仪的搅拌速度，释放介质的浓度和pH对微球的释放有较大的影响；制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显；方程拟合的结果表明缓释微球的释药行为符合扩散机制；测定三批微球样品的包封率均在96.8％以上，表明该法适合于制备难溶性药物的缓释微球。

I normally use quite a lot of light sources; I place them so I can highlight details of the scene. In this image I have used 13 lights: 4 omni lights as ambient lighting, 2 to highlight the form of the engine, 3 spotlights to highlight the back of the engine, 3 highlight to stress the specular and the greasy effect on the shell, a spotlight behind the snail neck for the sub surface scattering, in addition to the sun with area shade and the sky with a HDRI with an atmosphere similar to the photograph of the road for the global lighting I have used a surface with an asphalt texture for the floor and the yellow lines only to be reflected on the engine and to add some radiosity to the snail body and shine.

通常我使用很多的光源，我到处放置它们，这样我才能照到足够多的细节，在这幅图里我使用了13盏灯，4 盏点光源作为环境光，2盏来照亮引擎的形状，三盏聚光灯用来照亮引擎的背面，三盏来强调蜗牛壳的高光及油腻的感觉，有一盏蜗牛脖子背后的灯光来表现3S半透明效果，另外还有一盏太阳光来获得各个区域的阴影，以及一个赋予了HDRI贴图的sky，来作为全局光，我使用了一种沥青材质作为地面材质，并让引擎能反射地面上的黄色带子，并为蜗牛身体与光射线增加了一些radiosity，以取得得与背景类似的灯光环境。

Lighting灯光I normally use quite a lot of light sources; I place them so I can highlight details of the scene. In this image I have used 13 lights: 4 omni lights as ambient lighting, 2 to highlight the form of the engine, 3 spotlights to highlight the back of the engine, 3 highlight to stress the specular and the greasy effect on the shell, a spotlight behind the snail neck for the sub surface scattering, in addition to the sun with area shade and the sky with a HDRI with an atmosphere similar to the photograph of the road for the global lighting I have used a surface with an asphalt texture for the floor and the yellow lines only to be reflected on the engine and to add some radiosity to the snail body and shine.

通常我使用很多的光源，我到处放置它们，这样我才能照到足够多的细节，在这幅图里我使用了13盏灯，4 盏点光源作为环境光，2盏来照亮引擎的形状，三盏聚光灯用来照亮引擎的背面，三盏来强调蜗牛壳的高光及油腻的感觉，有一盏蜗牛脖子背后的灯光来表现3S半透明效果，另外还有一盏太阳光来获得各个区域的阴影，以及一个赋予了HDRI贴图的sky，来作为全局光，我使用了一种沥青材质作为地面材质，并让引擎能反射地面上的黄色带子，并为蜗牛身体与光射线增加了一些radiosity，以取得得与背景类似的灯光环境。

In the process of building and using the mass concrete structures, because of the effect of out-side condition and themselves, some faults will form in the structure, these faults will effect the bearing capability and endurance Using nondestructive testing method to test the concrete"s quality and diagnose its healthy, which has the significant sense in assessing the safety stability and research of the administering diseasesThis dissertation mostly researched the testing methods in the mass concrete structure, discussed the principles, methods, features, sphere of application of the ultrasonic testing in the mass concrete structure with faults, used dynamic FEM to simulate the testing process, discussed when the concrete structure with cracks is under the effect of the pulse, how the elastic waves propagate and what are their changing feature, Researched the principles of the first-arriving waves" phase when the cracks" depths are not same, obtained the relation between the inversion point and the cracks" depth, which has the direction sense in the application of projects,The second part of this dissertation is CT , which used the ultrasonic wave running through the tested-substance to get arriving-time of the ultrasonic wave, then inverse the image This dissertation drawed one CT program which can well present the different little cells ultrasonic wave velocity profiles of the substance, thereby to diagnose the quality of the part of the tested-substance, CT has the better using foreground..

在混凝土结构的施工及使用过程中，由于受其自身及外界各种因素的影响，常常会产生一些缺陷，对结构物的承载能力和耐久性造成严重影响，采用无损检测技术进行质量检测和健康诊断，这对混凝土结构开展安全、稳定性评估以及病害隐患治理研究具有重要意义。本论文主要针对大体积混凝土结构缺陷的检测方法展开研究工作，重点讨论了超声波法检测混凝土结构裂缝的基本原理和方法及其特点、适用范围，运用动力有限元数值模拟其检测过程，探讨了有裂缝缺陷的混凝土结构在脉冲荷载作用下弹性波的传播及其变化特征，研究了不同裂缝深度下首波相位变化规律，得出了反转临界点与裂缝深度之间的关系，这对实际工程应用具有指导意义。声波CT是一种新的无损检测技术，它是利用声波穿透被检测体获取声波接收时间，来进行计算机反演成像的技术。本文利用直射线法编制了层析成像程序，能较好地呈现被检测物体各微小单元的声波速度分布图像，从而对检测体的质量状况作出诊断评估，具有较好的应用发展前景。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。