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大茴香

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Synthesis of anisonitrile was carried out from anisaldehyde in the laboratory. Anisaldehyde was tranfered into aldoxime in the presence of 95% ethanol,and then gave anisonitrile using toluene as dehydrant.

摘 要:以5mL(0.04mol)大茴香醛为原料,在95%乙醇中制备大茴香醛肟,进一步在相转移催化剂作用下以甲苯作带水剂使大茴香醛肟脱水生成大茴香腈。

For dill is not threshed with a sharp tool, Nor is the cart wheel turned upon the cummin; But dill is beaten out with a rod, And cummin with a stick.

28:27 原来打小茴香不用尖利的器具,轧大茴香也不用碾轮;但用杖打小茴香,用棍打大茴香

Caraway is not threshed with a sledge, nor is a cartwheel rolled over cummin; caraway is beaten out with a rod, and cummin with a stick.

原来打小茴香、不用尖利的器具、轧大茴香、也不用碌碡。〔原文作车轮下同〕但用杖打小茴香、用棍打大茴香

"For the fitches are not crushed with a sharp instrument, and a cart-wheel is not rolled over the cummin; but the grain of the fitches is hammered out with a stick, and of the cummin with a rod."

原来打小茴香,不用尖利的器具,轧大茴香,也不用碌碡。但用杖打小茴香,用棍打大茴香

For the fitches are not threshed with a threshing itrument, neither is a cart wheel turned about upon the cummi but the fitches are beaten out with a staff, and the cummin with a rod.

28:27 原来打小茴香,不用尖利的器具,轧大茴香,也不用碌碡。但用杖打小茴香,用棍打大茴香

Caraway is not threshed with a sled ge, nor is a cartwheel rolled over cummin; caraway is beaten out with a rod, and cummin with a stick.

27原来打小茴香,不用尖利的器具;轧大茴香,也不用碌碡(原文作"车轮"。下同。);但用杖打小茴香,用棍打大茴香

For the fitches are not threshed with a threshing instrument, neither is a cart wheel turned about upon the cummin; but the fitches are beaten out with a staff, and the cummin with a rod.

027 原来打小茴香,不用尖利的器具,轧大茴香,也不用碌碡;但用杖打小茴香,用棍打大茴香

Under these conditions,the highest yield of anisonitrile from aldoxime was up to 90.7%,and the product anisonitrile was characterized by IR.

在此条件下,从大茴香醛肟到大茴香腈的最高收率达90.7%,并用IR表征了产物的结构。

For gith shall not be thrashed with saws, neither shall the cart wheel turn about upon cummin: but gith shall be beaten out with a rod, and cummin with a staff.

打小茴香不须用钉耙,打大茴香不须用碾机,而是用木棒打小茴香,用棍子打大茴香

Gith is not threshed with a sledge, nor does a cartwheel roll over cumin. But gith is beaten out with a staff, and cumin crushed for food with a rod.

打小茴香不须用钉耙,打大茴香不须用碾机,而是用木棒打小茴香,用棍子打大茴香

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