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Methods:a solid-phase extraction and gas chromatography-mass spectrometry procedure for the simultaneous detection of tramadol and its main metabolite in urine has been developed.results:the linearity of the tramadol solution from 0.1 g/ml to 100 μg/ml is fine ,and correlation coefficient is 0.9957.the average recovery was 99.21%,and the relative sandard deviation was 2.83%.conclusion:it is a rapid,simple,accurate and sensitive method.it is also an effective method for rapid detection whether there is tramadol in urine of druggy.

采用c18固相萃取法对尿中曲马多原体及其主要代谢物进行提取,利用gc-ms对其进行检测。结果:线性范围为0.1~100μg/ml(r=0.9957,n=6),平均回收率为99.21%,相对标准偏差为2.83%,最低测量限为 0.1 g/ml 。结论:本实验研究建立了尿中曲马多及其代谢物的快速、简便、准确、灵敏的检测方法,可作为快速检测吸毒人员尿中是否含有曲马多的一种有效的方法。

Its universality: its democratic equality and constancy to its nature in seeking its own level: its vastness in the ocean of Mercator's projection: its unplumbed profundity in the Sundam trench of the Pacific exceeding 8000 fathoms: the restlessness of its waves and surface particles visiting in turn all points of its seaboard: the independence of its units: the variability of states of sea: its hydrostatic quiescence in calm: its hydrokinetic turgidity in neap and spring tides: its subsidence after devastation: its sterility in the circumpolar icecaps, arctic and antarctic: its climatic and commercial significance: its preponderance of 3 to 1 over the dry land of the globe: its indisputable hegemony extending in square leagues over all the region below the subequatorial tropic of Capricorn: the multisecular stability of its primeval basin: its luteofulvous bed: its capacity to dissolve and hold in solution all soluble substances including millions of tons of the most precious metals: its slow erosions of peninsulas and islands, its persistent formation of homothetic islands, peninsulas and downwardtending promontories: its alluvial deposits: its weight and volume and density: its imperturbability in lagoons and highland tarns: its gradation of colours in the torrid and temperate and frigid zones: its vehicular ramifications in continental lakecontained streams and confluent oceanflowing rivers with their tributaries and transoceanic currents, gulfstream, north and south equatorial courses: its violence in seaquakes, waterspouts, Artesian wells, eruptions, torrents, eddies, freshets, spates, groundswells, watersheds, waterpartings, geysers, cataracts, whirlpools, maelstroms, inundations, deluges, cloudbursts: its vast circumterrestrial ahorizontal curve: its secrecy in springs and latent humidity, revealed by rhabdomantic or hygrometric instruments and exemplified by the well by the hole in the wall at Ashtown gate, saturation of air, distillation of dew: the simplicity of its composition, two constituent parts of hydrogen with one constituent part of oxygen: its healing virtues: its buoyancy in the waters of the Dead Sea: its persevering penetrativeness in runnels, gullies, inadequate dams, leaks on shipboard: its properties for cleansing, quenching thirst and fire, nourishing vegetation: its infallibility as paradigm and paragon: its metamorphoses as vapour, mist, cloud, rain, sleet, snow, hail: its strength in rigid hydrants: its variety of forms in loughs and bays and gulfs and bights and guts and lagoons and atolls and archipelagos and sounds and fjords and minches and tidal estuaries and arms of sea: its solidity in glaciers, icebergs, icefloes: its docility in working hydraulic millwheels, turbines, dynamos, electric power stations, bleachworks, tanneries, scutchmills: its utility in canals, rivers, if navigable, floating and graving docks: its potentiality derivable from harnessed tides or watercourses falling from level to level: its submarine fauna and flora, numerically, if not literally, the inhabitants of the globe: its ubiquity as constituting 90 percent of the human body: the noxiousness of its effluvia in lacustrine marshes, pestilential fens, faded flowerwater, stagnant pools in the waning moon.

50它的普遍性,它的民主的平等性,以及保持着它自身求平的本质。用墨卡托投影法在地图上所标示出的浩淼的海洋;太平洋中巽他海沟那超过八千噚的不可测的深度;永不消停、后浪推前浪地冲刷着海岸线每一部位的波涛以及水面上的微粒子;水的单位粒子的独立性;海洋变幻莫测;根据液体静力学,风平浪静时它纹丝不动;根据液体动力学,小潮大潮时它便涨了起来。暴风雨后一片沉寂;北极圈与南极圈冰冠地带的不毛性以及对气候及贸易的影响;跟地球上的陆地相比占三对一优势;它在亚赤道带南回归线以南的整个区域延伸无数平方海里的绝对权威;其在原始海盆里数千万年以来所保持的稳定性;它那橙红色海床;它那把包括数百万吨贵金属在内的可溶解物质加以溶解,并使之保持在溶解状态的性能;它对半岛和有下陷趋势的岬角所产生的缓慢的浸蚀作用;其冲积层;其重量、容积与浓度;它在咸水湖、高山湖里的静谧;其色调因热带、温带和寒带而变为或浓或淡;与陆上的湖泊、溪流及支流汇合后注入海洋的河川,还有横跨大洋的潮流所构成的运输网。沿着赤道下面的水路自北向南的湾流;海震、水龙卷、自流井、喷泉、湍流、漩涡、河水暴涨、倾盆大雨、海啸、流域、分水岭、间歇泉、大瀑布、漩流、海漩、洪水、泛滥、暴雨等滥施淫威;环绕陆地的上层土壤那漫长的曲线;源泉的奥秘可用探矿杖来占卜或用湿度测定器来揭示;阿什汤大门的墙壁上的洞、空气的饱和与露水的蒸发能够证明那潜在的湿度;水的成分单纯,是氢二、氧一的化合物;水的疗效;水的死海里的浮力;它在小溪、涧谷、水坝的缝隙、船舷的裂口所显示的顽强的浸透性;它那清除污垢、解渴、灭火、滋养植物的性能;作为模范和典型,它的可靠性;它变化多端:雾、霭、云、雨、麦、雪、雹;并在坚固的消防龙头上发挥出压力;而且千姿百态:湖泊、湖岔、内海、海湾、海岬、环礁湖、环状珊瑚岛、多岛海、海峡、峡江、明奇、潮汐港湾、港湾;冰河、冰山、浮动冰原显示出它是何等坚硬;在运转水车、水轮机、发电机、发电厂、漂白作坊、鞣皮厂、打麻厂时,它又是那样驯顺;它在运河、可航行的河川、浮船坞和干船坞所起的作用;潮汐的动力化或利用水路的落差使它得以发挥潜力;海底那些成群的动物和植物虽然并非名副其实地栖息在地球上,论数目却占地球上生物的一大半;水无所不在,占人体的百分之九十;在沼泽地、闹瘟疫的湿地、馊了的花露水以及月亏期那淤积污浊的水塘子,水所散发的恶臭充满了毒气。

La Mer' reflected China classical aesthetic ideology, especially the aesthetic ideology consistency that China ancient scholars and painters reflected on the performance of natural landscape ,which was 'harmony between the heaven and human ','Sound outside what the string is making between the lines ' and 'approach determined by figure'. Its music reflected gamelan creative skills in many aspects,...更多 for example, the use of continuous tone and fixed voice type, the texture counterpoint imitation, the similarity of pitch and the harmony, etc. It could be seen that Debussy once studied Javanese gamelan music thoroughly on the analysis of 'La Mer' music ontology. Debussy choosed Japanese printer—Katsushika Hokusai's 'surfing in Kanagawa' as cover on the publication of 'La Mer', it was reflected that on the one hand he liked Japan Ukiyoe, on the other hand his work had painting factors.

大海》中体现了东方文化中的中国古典美学思想,尤其是与中国古代文人画家们在表现自然景观上所体现山的美学思想的一致性,即"天人和一"、"弦外之音"以及"以象立意"等;它在众多方面都体现山了加美兰的创作技巧,如持续音、固定音型的使用,织体对位的模仿,调式、和声的相似性等,在对《大海》音乐本体的分析中可以看出,德彪西对爪哇加美兰的音乐曾进行过深入的研究:作品出版时德彪西选择了日本版画家葛饰北斋的《神奈川冲浪里》作为封面,一是表现出他对日本浮世绘的浓厚兴趣,二是表达了他作品中具有的绘画性因素。

In a way bands like the smiths from the 80s were a breath of fresh air there was a lot of electronic rubbishy pop around at that time, but because of that the backlash was that things moved in a more positive direction .the London music seane is particularly good for prompting change people get bored quickly and with different multicultural musical influences it is constantly changing, it kind of boots you up the back side to stop you playing in same style, and look at new things.

就像在80年代Smiths的出现如一股新鲜空气,因为当时有太多的电子垃圾音乐。但正是因为这个原因,人们对音乐的需求推动了其向前发展。伦敦音乐的背景对刺激音乐的改变起着特别的推动作用。人们对一种音乐会很快失去兴趣,受不同文化交流的影响,音乐背景也一定会随之改变。这一现实会促使你向新事物新方向发展而不能总是奏一成不变的音乐。

We have to completely change the previous order must be ready to move on the school field to break the conventional PK up 2 if not a direct one to eight locked him up and then directly to Yang Jian + YUE +欲擒故纵+ million一阳指+ static shadow Shen Xue-Yong Choi,+ blue Guan (Why should we put this last because the snow has a chance of sealing a hole shut you hole you made) on this almost four seconds if you are lucky the snow over the hole then sealed Congratulations you because you have already won the war 60 percent of the seal if there is no point you would present him with a hidden weapon and then let the points title, such as pieces of a scamper up in the coming months Sanyang kai tai closed at this time point almost did not state the business Jian Yang is also the state of almost 15 seconds to less then one Ze Jian-lun up on OK after you select what he skills on the line you up for the OK to this you have won 80% of you are not called Yang Jian He wasted (a little trick if you do not have confidence in their own operations should not be used when you stealth stealth opponent immediately hidden stealth so he did not you or punches you, you can how much you a few of his) if the two sides blood depends on many things on their own time for the operation of more than two minutes after you beat him you mean you are invincible Blue啦short or very important operation to operate a bad person it up!!

我们要彻底的改变以前的出招顺序要勇于打破常规关于校场PK 上去2话不说直接一个八门上去先锁住他然后就直接上商阳剑+欲擒故纵+万岳+一阳指+静影沉璧+雪拥蓝关(为什么要最后一个放呢因为雪拥有一定的几率封穴封住穴你就发啦)这时差不多就4秒啦要是运气好雪拥封住了穴那就恭喜你啦因为这场战争你已经赢了60%啦如果没有封住穴的话现在就用暗器封他的穴吧然后一个等衔枚疾走上去在来个三阳开泰这时封穴状态也差不多没了商阳剑的15秒状态也差不多到了这时一个少泽剑抡上去就OK啦以后就有啥技能往上抡就行啦进行到这这场OK你就已经赢了80%啦商阳剑也没叫他白白浪费掉(一个小计谋如果你对自己的操作没信心就不要用先用隐身对手隐身时候你马上就隐这样的话他隐身没啦你还是隐的你就可以多大他几下啦)如果双方血都多的话就要靠自己的操作多争取时间啦 2分钟后你一打他蓝你就等于无敌啦总之操作还是很重要操作不好的人努力吧!!

The study, an online poll of more than 1,000 people with investible assets of at least $1 million, excluding workplace retirement accounts and any real-estate holdings, found that 46% of millionaires didn't feel wealthy.

一份网上民调对一千多人进行调查,这一千多人可供投资的资产(包括工厂退休金和任何房产)不到1百万。

People could see some new features during this period such as images going with events.Part Three probes into the themes and philosophy in Historical Ode. The diversity of poets" ideologies has resulted in complicated themes and intricate philosophy in their works. Generally speaking, themes and philosophy among the poems were expressed in three forms: Chanting in the Wind, that is, the poets give voice to their ambitions and concerns among the words with optimistic attitudes; Bitter of Lofty Ideal Frustrated: poems of this kind usually take up pessimistic themes expressing poets" bitter suffering and their failed ambitions and among these poems signing for the misfortunes of some female has taken a large portion; Detached Stance toward Fame and Wealth: Secluding from the world and seeking political ambitions are two opposing elements in an antimony which have coined the peculiarity of ancient literati.

第三章:咏史诗的主题哲思诗人带着对历史的主观感悟进行咏史诗创作,使咏史诗的主题哲思呈现纷繁复杂的现象,汉魏六朝咏史诗的主题哲思主要有:长啸清风—英雄抱负的乐章:在传统儒学熏陶下形成的历史责任感和积极入世心态往往使文人将其对国家、民族的关怀和对自身建功立业的渴望流露在他们所寄托的文学作品中;世事迪遣—壮志难酬的苦闷:入世受阻后诗人往往从对英雄的追慕转向对不幸人物的同情,悲情主题是咏史诗中较多的一种,表现作者壮志难酬的苦闷和怀才不遇的伤感的形式是多样的,其中又以对不幸女性的吟咏居多,这主要是因为诗人和悲剧女性命运和情感上的类同使然;遗荣守真—无与外物的逸响:遗荣守真的隐逸思想和政治关怀的入世态度作为一组对立面共同构筑古代士人的理想情趣,&仕&与&隐&的抉择冲突作为文人生活中不断上演的主旋律,常常通过咏史诗体现出来。

Main results are listed as below: 1. In rapid solidification, when the cooling rate is over some critical value, the solidification system will become unstable in the sense of the nonequilibrium thermodynamics, a uncontinuous steady state jump phenomenon will occur, and this uncontinuous steady state jump can be understood as the glass transition.

主要得到了如下结果:(1)通过对快速凝固过程的动力学及热力学的分析,提出了非晶转变的分枝理论模型,结果表明,对一合金熔体,当冷却速度大于某一临界值时,凝固体系会出现非平衡热力学意义上的失稳而出现多定态分枝现象,这一多定态现象可以被理解为非晶转变。

When it is under certain perturbation, a quasi-elliptic response with transmission zeros to improve the transition can be obtained using the transmission zero technique given in the dissertation. Further, a multi-mode resonator composed of a half wavelength resonator loaded with two shunt series LC circuit is also investigated intensive.

本文提出了一种新型准集总元件谐振器,它既具有结构紧凑的优点,又能够引入传输零点构成准椭圆特性响应;本文也提出了一种由半波长传输线加入微扰构成的双模谐振器,并对它的传输零点技术做了全面系统的研究,这种双模谐振器相比传统的环形双模谐振器有更加紧凑的尺寸;本文提出了一种由半波长传输线加载并联串联LC电路构成的多模谐振器并对其在宽带滤波器的应用进行了研究;论文对一种复合谐振器及其在双通带滤波器设计中的应用进行了研究。

La Mer' reflected China classical aesthetic ideology, especially the aesthetic ideology consistency that China ancient scholars and painters reflected on the performance of natural landscape ,which was 'harmony between the heaven and human ','Sound outside what the string is making between the lines ' and 'approach determined by figure'. Its music reflected gamelan creative skills in many aspects,...更多 for example, the use of continuous tone and fixed voice type, the texture counterpoint imitation, the similarity of pitch and the harmony, etc. It could be seen that Debussy once studied Javanese gamelan music thoroughly on the analysis of 'La Mer' music ontology. Debussy choosed Japanese printer—Katsushika Hokusai's 'surfing in Kanagawa' as cover on the publication of 'La Mer', it was reflected that on the one hand he liked Japan Ukiyoe, on the other hand his work had painting factors.

大海》中体现了东方文化中的中国古典美学思想,尤其是与中国古代文人画家们在表现自然景观上所体现山的美学思想的一致性,即&天人和一&、&弦外之音&以及&以象立意&等;它在众多方面都体现山了加美兰的创作技巧,如持续音、固定音型的使用,织体对位的模仿,调式、和声的相似性等,在对《大海》音乐本体的分析中可以看出,德彪西对爪哇加美兰的音乐曾进行过深入的研究:作品出版时德彪西选择了日本版画家葛饰北斋的《神奈川冲浪里》作为封面,一是表现出他对日本浮世绘的浓厚兴趣,二是表达了他作品中具有的绘画性因素。

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Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来,英国,在此地早期居住的是凯尔特人,已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。

The almost sure central limit theorem is a pop topic of the probability research in recent years,because it has many actual applications in the random analogue.

中文摘要:几乎处处中心极限定理是近几十年概率论研究的一个热门话题。它之所以引起人们的注意是由于它在随机模拟方面的实际应用参见Fisher