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The optimal conditions were found as follows: reaction temperature 90℃, reaction time 50 min, the molar ratio of catalyst to diethyl adipate 1.1:1, providing 99.5% yield.

结果表明,各试验因素的影响效能为反应温度(反应时间(催化剂用量;最佳合成条件为反应温度90℃,反应时间50 min,催化剂与原料的摩尔比为1.1:1,在此条件下,常压合成目标物的产率可以达到99.5%。

The results showed that the amount of artemisinin was 1.5 g, the use level of deionized water 300 mL, the amount of reductant 1.0 g, the reaction time 1.5 h and the carbinol amount of solvent 100 mL, the yield of the product was 74.25% and the purity was 99.13% respectively.

实验表明,最佳工艺条件为:青蒿素用量为1.5 g,去离子水用量为300 mL,还原剂硼氢化钠用量为1.0 g,反应时间为1.5 h,溶剂甲醇用量为100 mL。在此条件下,产物产率为74.25%,纯度高达99.13%。

The HPLC methods for analysis of N--ribitylxylidine and N-methyl glucamine were established. After optimizing the operation conditions, the principal product and main impurities were well separated. And they were determined by LC-MS. The operation condition of N--ribitylxylidine is, columniation temperature is 30℃, flow rate is 0.7mL/min, UV wave is 244nm, the mobile phase is methanol: water=40: 60 .

首次建立了对葡甲胺和核糖胺的高效液相色谱分析方法,通过对色谱操作条件的优化,成功分离了主产物和杂质,在此条件下,应用液相色谱-质谱联用仪对糖基胺及生成杂质进行了指派定性,并测定了两种糖基胺及其主要杂质的含量,获得了满意的结果。

In the function of the transaction costs being concave function and more general market friction conditions, giving a algorithm of mean-absolute deviation model and the mean-average absolute deviation model under conditions.

在一般摩擦市场下交易费用函数为凹函数时,给出了均值—绝对偏差模型和均值—平均绝对偏差模型在此条件下的求解算法。

With corn embryo being coproduct in corn starch production as material, glutathione was extracted through hot water extraction after supercritical CO2 fluid extraction and ultrasound wave treatment. The results showed that The optimum conditions of hot water extraction are solid; liquid 1:15, temperature 90 ℃, pH3.0, time is 15 min. On these conditions GSH yield is 97 mg/100 g corn embryo.

以淀粉加工副产物玉米胚为原料,经过超临界流体萃取脱脂及超声波破壁处理后,采用热水浸提法提取谷胱甘肽,最佳热水浸提工艺条件为固液比1:15 g/mL、浸提温度90℃、浸提液pH3.0、浸提时间15 min,在此条件下谷胱甘肽提取量为97 mg/100g玉米胚。

The decomposition of hydroxylamine hydrochloride under the reaction conditions was studied to understand its function during the amination process.

在此条件下,得到的苯胺收率为64 mol%,苯胺选择性为95.6%,转化数为48摩尔苯胺/摩尔V,此结果好于已有文献报道值。

The first chapter, main instead " duo-ring " condition of " every maximal left ideal is GW-ideal " condition,study strongly regularities of GP-V-ring on this condition.lt is shown that (1) R is strongly regular iff R is left GP-V-ring whose maximal left ideals are GW-ideal.(2)R is strongly regular iff R is left GP-V-ring whose maximal right ideals are GW-ideal. The second chapter, generalize some results of GP-V-ring to GP-V-ring, discuss regularity of GP-V-ring.It is shown that (1) R is left self-injective regular with non-zero socle iff R is left GP-V -ring with Soc = Soc and R contains an injective maximal left ideal.(2)R is regular ring and every maximal essential left ideal is ideal iff R is left GP-injective left GP-V -ring and every maximal essential left ideal is ideal.

第一章主要将"duo-环"条件替换成"每一极大左理想是GW-理想"条件,研究在此条件下,GP-V-环的强正则性,证明了:(1)R是强正则环当且仅当R是左GP-V-环且R的每一极大左理想是广义弱理想;(2)R是强正则环当且仅当R是左GP-V-环且R的每一极大右理想是广义弱理想,第二章,主要将GP-V-环上一些结果推广到GP-V′-环上,讨论GP-V′-环的正则性,证明了:(1)R是左自内射正则环且Soc≠0当且仅当R是包含内射极大左理想的GP-V′-环,且Soc=Soc;(2)R是正则环且每一极大本质左理想是理想当且仅当R是左GP-内射的左GP-V′-环且每一极大本质左理想是理想。

Recently, many coding experts have studied much of the Z_4-cyclic code(which is not necessarily linear) and its Gray map, and obtained a set of equivalent conditions in which a family of cyclic codes are linear, and the condition that this family codes are self-dual cyclic, and in this condition Nechaev-Gray image of the cyclic codes are self-dual cyclic.

近年来,已有编码学家对Z 4-循环码和Z 4上的映射作了深入研究,得到一类循环码是线性码的一系列等价条件,以及这类线性码是自对偶线性循环码的条件,在此条件下它的Nechaev-Gray像也是自对偶线性循环码。

A substrate concentration of 0.277 kg/L, enzyme/ substrate level of 1408 U/g, temperature of 39.2 ℃, and a hydrolysis time of 4.86 hour were found to be the optimum conditions for high antibacterial activity. Under this condition, the bacteria Escherichia coli, Micrococcus luteus and Bacillus subtilis in the hydrolysates had the inhibitory rate of 71.40%, 56.88%, and 64.54%, respectively.

经Design Expert 7.1.2软件优化,得出胃蛋白酶酶解鲶鱼骨蛋白的最优条件为:底物浓度0.277kg/L,加酶量1408 U/g,水解温度39.2℃,水解时间4.86 h,在此条件下获得的水解物,对大肠杆菌、藤黄微球菌及枯草芽孢杆菌的抑菌率分别为71.40%、56.88%和64.54%。

The type, initial feeding time and concentration of precursor for HV unit formation had great effects on PHBV production in shake flasks. Propionate was selected as the better precursor for HV fraction than valerate after comprehensive survey of these two precursors. The suitable PHBV shaking-flask culture conditions were obtained through the analysis of PHBV fermentation process, the investigation of several factors by using RSA method and the fed-batch experiments. Cell dry weight, PHBV content, PHBV concentration, HV fraction and yield coefficient of HV unit to propionate were 27. 7g/L, 80.7%, 22. 4g/L, 16. 1mol% and 0.50g/g, respectively.

在共聚物PHBV的摇瓶发酵过程中,PHBV中HV组分形成的前体物质的种类、初始加入时间以及加入量是影响PHBV发酵过程的重要因素;在综合比较丙酸和戊酸这两种前体的基础上,选择丙酸作为HV组分合成前体较适宜;通过对PHBV发酵过程曲线分析、影响PHBV发酵指标的各因素的响应面分析以及摇瓶发酵补料试验,得到了较适宜的PHBV摇瓶发酵补料条件,在此条件下,细胞干重、PHBV含量、PHBV浓度、HV组分含量和HV组分对丙酸的产率系数可分别达到27.7g/L、80.7%、22.4g/L、16.1mo1%和

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Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克,果实色泽鲜艳,汁多味浓,甜酸适口,离核仁甜,清末时就驰名陕、甘两省,清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异:红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感,ED90值分别为47.65、71.67和29.17g/hm2;春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感,ED90值分别为96.91、114.20g/hm2;而番茄不敏感。

However, I have an idea.

不过,我有个主意。