分光光度测定

It is that:(1) the related compounds in Metronidazole Buccal Tablets prepared by Chongqing Medical College can be tested by determining (321nm) the total peak area of the impurities;(2) The related compounds in Metronidazole Disodium Phosphate for Injection prepared by Chongqing Medical College can be test by determining (254nm) the total peak area of the impurities and the peak area of the largest impurity;(3) Ceftriaxone polymer in Ceftriaxone Sodium for Injection prepared by Chongqing Keru Pharmacy Co.

结果如下：①用HPLC一UV法，在321nm处检测，用归一化法计算，控制各杂质峰面积的和，可检查重庆医科大学的注射用甲硝吟磷酸二钠中的有关物质：②用HPLC一UV法，在254nm处检测，控制杂质峰面积的和及控制最大杂质峰面积，可对重庆科瑞制药股份有限公司的注射用头饱曲松钠中的有关物质实施控制；③用HPLC一Uv法，在254nm处检测，按外标法计算，可检查注射用头抱曲松钠中的聚合物；④用紫外分光光度法，在277nm波长处测定吸收度，按C6H9N303的吸收系数为377计算每片标示百分含量，可测定重庆医科大学的甲硝哇口颊片的含量均匀度；⑤用紫外分光光度法，在277run波长处分别测定释放溶液20min、50min和90min的吸收度，按甲硝哇(C6H剥303)的吸收系数为377计算释放度，可检查重庆医科大学的甲硝哇口颊片的释放度。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小，进行综合分析，确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量，测定条件：加入100ml浓度为8.0±0.1％的氢氧化钠，在恒温水浴中煮沸回流6h；采用溶剂萃取法测定JOB-1C中TATB的含量，选择TATB饱和的二甲基甲酰胺为萃取溶剂，用G4坩埚式过虑器进行萃取分离；采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量，通过实验确定了多波长组合：λ=267nm，275nm，283nm，291nm，299nm；朗波—比耳定律的适用范围为PNP浓度：0.005～0.025mg/ml，HMX浓度：0.06～0.30mg/ml；在测定波长下，对PNP、HMX标准溶液的吸光度—浓度进行线性回归，由回归曲线的斜率得出PNP、HMX的吸收系数；根据朗波—比耳定律和吸光度加和性原理，在测定波长下，对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归，回归曲线的斜率即为混合溶液中PNP的浓度。

The contents of Mn, Cu, Fe, Zn in the leave, flower, seed of Impatiens balsamina induced by space flight are determined by flame atomic absorption spectrometry. The measure parameters for FAAS are optimized.

采用火焰原子吸收分光光度法测定了航天诱变凤仙花的茎、叶、花、种子中Mn、Cu、Fe、Zn四种微量元素的含量，优化了原子吸收分光光度法测定参数。

Caesalpinia Sappan L. that had immunosuppressive function was investigated in this paper. On the basis of establishing the method of determining content of hydroxybenzene in Caesalpinia Sappan L., extractive technology was investigated by orthogonal design. Permeation, soxhlet and ultrasonic extraction were surveyed with water, thirty-five, sixty-five and ninety-five percent of ethanol as solvents.

本文以具有免疫抑制作用的中药苏木为研究对象，在建立苏木中总酚含量分光光度测定方法的基础上，以水、35%、65%、95%乙醇为溶剂，通过渗漉法、煎煮法、索氏法、超声波法对苏木的提取工艺进行了优选。

spectrophotometric method with phenol disulfonic acid ; ultraviolet spectrophotometer ; nitrate nitrogen ; comparison

本文通过对常用的酚二磺酸光度法和紫外分光光度法进行实验比对，同时调查云南省内两种分析方法考核的情况，从而找出两种方法的优缺点，供分析人员在实践中借鉴。l原理1.1酚二磺酸光度法测定的原理方法依据：GB7480一87《水质硝酸盐氮的测定酚二磺酸分光光度法》。用浓硫酸与苯酚作用生成酚二磺酸

Organelle and biological molecular;the method to show the nucleic acid、protein、enzyme、glucide and lipid;microspectrophotometry and flow cytometry.

胞内核酸、蛋白质、酶、糖类与脂质等的显示方法；显微分光光度测定技术和流式细胞仪

In 0.015 mol/L NaOH medium, AuCl4(superscript -)reacted with hexadecyl trimethyl ammonium bromide, forming water soluble CTMAB-AuCl4 complex that exhibited a weak absorption peak at 400 nm. In the presence of hydrazine, the reaction produced orange-red nanogold particle and exhibited a surface plasma resonance absorption peak at 520 nm.

在0.015mol/LNaOH介质中，氯金酸根离子AuCl(上标-下标 4与阳离子表面活性剂十六烷基三甲基溴化铵反应生成水溶性的CTMAB-AuCl4缔合物，在400nm处产生一个很弱的吸收峰，当有肼存在时，反应生成橙红色的金纳米粒子，在520nm处出现一个表面等离子体共振吸收峰，从而可实现废水中微量肼的分光光度测定。

The studies took a investigation into the main biochemical constituent of the plant, and a set of quantitative analysis method to Jasminum flavonoids was established. Further more, the studies developed a water extract process, and a method to isolate and purificate Jasminum flavonoids.

本实验较全面的分析了茉莉花干的生化成分，研究了以茉莉花干为原料的速溶产品提制工艺，探讨了茉莉黄酮提取纯化条件的优化，并初步探索了茉莉黄酮的检测技术，实验结果如下：本研究建立了茉莉黄酮的分光光度测定方法。

In this paper,the authors compared extraction spectrophotometric method with gravimetric method in the determination of naphthenic acid in oil refining sewage,and found that the former method is better than the latter both in precision and operation.

讨论了萃取分光光度法测定炼油污水中环烷酸含量的测定条件和干扰因素并与重量法进行了比较，萃取分光光度法的精确度比重量法高而操作比重量法简单。

A highly sensitive method for the spectrophotometric determination of microamounts of aluminum by salicylfluorone and cetyltrimethyl- ammonium bromide is proposed.

本文提出一种用水杨基萤光酮和溴化十六烷基三甲基铵分光光度测定微量铝的高灵敏方法。

Chrysanthemum of 10 thousand birthday is lax to edaphic requirement, with the arenaceous qualitative loam with fecund, good drainage had better.

万寿菊对土壤要求不严，以肥沃。排水良好的砂质壤土为好。

He unstepped the mast and furled the sail and tied it.

他拔下桅杆，把帆卷起，系住。