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分光光度测定

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Methods:the dispersible tablets was prepared by taking lose subsfrits hydroxypropyl cellulose and hydroxypropymethyl cellulose as excipient.the phenobarbital content in tablets was determined by uv spectrophotometry at 240 nm.results:the uniformity test of dispersion showed that the tablets could smoothly disperse and pass through a no.2 sieve within 1 min.

以低取代羟丙基纤维素、羟丙甲纤维素等为辅料研制该分散片,紫外分光光度法测定该片中苯巴比妥的含量,测定波长为240 nm。结果:分散均匀性试验表明该分散片在1 min内均匀分散并通过2号筛。

Content of trypsin inhibitors in extracts of cyanobacterium from Taihu lake was determined by UV spectrophotometry in this paper.

采用紫外分光光度法对太湖蓝藻提取液中的胰蛋白酶抑制剂进行了含量测定,测定的线性范围在 4~ 4 0 μg/mL 。

The optimum condition of spectrofluorimetric determination of uranyl ion in pyridine 2,6 dicarboxylic acid β cydodextrin system is studied.

研究了吡啶 2 ,6 二羧酸β环状糊精体系荧光分光光度法测定铀酰离子的最佳条件以及某些稀土共存离子对荧光体系的干扰,并应用于人工样品的测定。

Rats was cannulated for in situ recirculation. UV and HPLC methods were used to determine the concentrations of phenolsulfonphthalein and scopoletin, respectively.

采用大鼠在体胃、小肠吸收实验模型,以高效液相色谱法测定灌注液中药物的浓度,紫外分光光度法测定酚红的浓度。

Effect of different surfactants on the UV intensity of Al(superscript 3+)-MXFX have been studied. Is Cetyl Trimethy-lammonium Bromide can increase the UV intensity of Al(superscript 3+)-MXFX is discovered. Based on this reaction, the reaction conditions in detail and proposed a simple, rapid and sensitive new method for the determination of MXFX by UV method is inve stigated. This method has been applied for the determination of MXFX in tablet with satisfactory results.

通过研究不同表面活性剂对Al(上标 3+)-莫西沙星体系紫外特性的影响,发现十六烷基三甲基溴化铵对该体系有显著的增敏作用;系统研究了CTMAB-Al(上标 3+)-MXFX反应体系的紫外特性,利用这一反应体系,建立了简单、快速、灵敏的测定莫西沙星的紫外分光光度法,选择了最佳实验条件,并将此方法用于莫西沙星片剂的测定,结果满意。

A spectrophotometry method, which based on the reaction of diacetyl monoxime and urea in acidic solution, was established for determination urea in bovine milk.

根据二乙酰一肟与在酸性条件下尿素的反应,建立了一种分光光度法快速测定牛奶中尿素含量的方法,该方法可以定性和定量测定牛奶中尿素含量。

According to the yogurt's complex ingredients and the particular content of diacetyl , this article studied the determination of diacetyl in yogurt with ultraviolet spectrophotometer.

本文根据乳品中的成分的复杂性及双乙酰含量的特殊性,研究了以鲜奶为溶剂制作双乙酰标准曲线和紫外分光光度法测定乳品中双乙酰含量的测定方法。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂,甲醇为溶剂的回流提取法来提取植物多酚,用显色反应检识酚羟基;采用紫外分光光度法对多酚粗体物进行总多酚含量的测定;选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌,采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验,并测定其最低抑菌浓度;采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析,根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

In order to detect product\'s quality and to adjust the synthetic conditions, UV and RP- HPLC methods for the determination of the target product were established according to the components of products in the electrosynthesis course, by which target product were able to be simply, fast and accurately determined without separation in advance. And satisfactory results were obtained when they were applied to the determined of the product\'s content.

本研究为检验产品质量,调整合成工艺条件,根据电合成过程中生成物的组成情况,首先建立了无需进行分离就能够简单、快速、准确测定目标产物的紫外分光光度法和反相高效液相色谱法,并将其应用于产品含量的测定,获得令人满意的实验结果。

In this paper, the determination of trace elements including copper, manganese,cobalt, nikel and chromium in lead metasilicate by atomic absorption spectroscopyhas been investigated.

本文提出用火焰原子吸收分光光度法测定硅酸铅中的微量元素铜、锰、钴、镍和铬,并探索了样品中可能存在的干扰元素及溶剂介质酸度对测定的影响。

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