再聚合

The copperas, a raw material, was oxidized by the oxidant under certain temperature, and then the sulfuric acid and the catalyst were added to the mixture. After the hydrolisis polymerization curing, the polymeric ferric sulfate was prepared.

采用钛白生产中的副产品绿矾(FeSO47H2O)为原料，在一定的温度下经氧化剂氧化，再加入硫酸和一定量的催化剂经水解聚合、静置熟化制备固体聚合硫酸铁。

In this study, Chitosan-Poly complex nanoparticles were prepared by template polymerization of acrylic acid in the chitosan solution. The preparation and characterization of CS-PAA nanoparticles including the yields of the nanoparticles, FT-IR spectrum analysis, dynamic light scattering, zeta potential, and morphology of nanoparticles were concentrated in this study. The effects of temperature, weight ratio of CS and PAA, and pH value on the physicochemical properties of nanoparticles were studied.

本研究中，我们以模板聚合法在几丁聚醣（Chitosan， CS）溶液中聚合丙烯酸（Acrylicacid， AA）以制备几丁聚醣－聚丙烯酸复合奈米颗粒并计算其产率，再以傅利叶红外线光谱仪、动态光散射粒径分析仪（Dynamic light scattering， DLS）、表面电位测定仪及穿透式电子显微镜等仪器分析CS－PAA 复合奈米颗粒之性质，以探讨聚合时温度、聚合反应时间、CS 与AA 之重量比，以及介质pH 值对CS－PAA 复合奈米颗粒结构的影响。

Electropolymerized pyrrole to polypyrrole was fabricated on gold electrodes and used as sensors. Cyclic voltammeter was applied to the characterization of the sensing material Ppy.

本文以电聚合方式，将吡咯聚合成的感测材料聚吡咯(polypyrrole， Ppy)薄膜镀制於金电极上，聚合完成的Ppy薄膜再经过循环伏安仪来作定性分析。

METHODS: MyoD cDNA fragments were extracted from plasmids pEMSV-MyoD with polymerase chain reaction, and PCR was used to clone the whole-length gene of MyoD. After adding CACC sequence at 5' end, MyoD gene was cloned by orient topology into transfer ventor, pENTR/D-TOPO. Objective gene was transferred into adenoviral expression vector DNA via pENTR/D-TOPO vector. The recombinant adenoviral vectors transfected into HEK293A cells by using lipofectamine were packaged and amplified.

从pEMSV-MyoD质粒上用聚合酶链反应法扩增出MyoD cDNA片段，再通过聚合酶链反应使MyoD基因加上CACC序列接头，经过定向拓扑克隆使目的基因连接到转移载体上，再通过LR酶促反应，将目的基因转移到腺病毒表达载体DNA上，获得MyoD基因重组的腺病毒DNA，用脂质体转染法转染HEK293A细胞，包装扩增出MyoD基因重组的腺病毒。

While all the phenyl groups in tetraphenylphenyl groups or benzophenanthrene groups are not coplanar. At the same time, by density function theory, the electronic energy gap between HOMO and LUMO frontier molecular orbitals of condensed aromatics are calculated and the Eg of acenaphthenyl groups in C_2 gum is the smallest, which explains the reason why C_2 gum has the best radiation protection effects.

利用甲基三氯硅烷和溴苯的格氏反应合成了甲基苯基二氯硅烷，用核磁分析证实了格氏反应中高沸点副产物为甲基二苯基氯硅烷；通过甲基苯基二氯硅烷和二甲基二氯硅烷的共水解，再裂解而制得含Me_2SiO链节的甲基苯基环硅氧烷混合物，进而利用碱胶开环聚合得到甲基苯基硅橡胶生胶；也可通过甲基苯基二氯硅烷水解所得甲基苯基环硅氧烷D_3~(3Ph、D_4~(4Ph_)与D_4开环聚合制得甲基苯基硅橡胶生胶。

The sperm whales in Odontoceti was closely related with baleen whales in Mysticeti, and then clustered with Delphinoidea and then with Ziphioidea.

其中抹香鲸总科与须鲸亚目聚合在一起，然后与海豚总科聚合再与喙鲸总科相聚。

Both star copolymer precursors are hydrolyzed in the acidic conditions, then the corresponding recovered star copolymers of EO and glycidol with multi pending hydroxylmethyls are esterified with 2-bromoisobutyryl bromide to produce the ATRP macroinitiators with multi pending bromoisobutyryl groups . Then the latters initiate the polymerization of styrene to form the corresponding amphiphilic three- and four-arm star PEO-g-PS.

在阴离子共聚EPEE单体和环氧乙烷单体的过程中，通过变换引发剂体系中的醇的结构(由原来的二元醇变成多元醇，如三羟甲基丙烷和季戊四醇)，合成了星形结构的共聚物，通过水解反应脱去保护基团后，再与2-溴异丁酰溴反应，得到链的侧端挂有很多2-溴异丁酸酯基的星形大分子引发剂，通过ATRP聚合机理引发苯乙烯聚合得到PEO为主链，PS为侧链的星形一接枝共聚物。

According to the characteristic of silver nanoparticles, their uniform dispersion in reaction media was obtained by surface modification, ultrasonic radiation and the select of emulsion, and then emulsion polymerization system were formed by combination with reactive monomer and initiator. Nano-Ag/Polystyrene core-shell particles were prepared by emulsion polymerization and their microstructure were characterized by TEM, FTIR, XPS, AFM and TG/DTA. The experimental results showed that silver nanoparticles were coated by polymer and the composite particles had typical core/shell structure, and the microlevel combination was realized. Meantime, the form mechanism of nano-Ag/polystyrene core-shell particles was tentatively researched. The conclusion is that the perfect coating was able to obtained by the control of reaction condition.

根据纳米银粒子的特性，借助于表面处理、超声辐照以及乳化剂的选择，使其均匀分散在反应介质中，再与反应单体、引发剂等形成乳液聚合体系；采用乳液聚合方法、包裹聚合方式，制备出纳米银/聚苯乙烯核壳复合粒子，并借助于TEM、FTIR、 XPS、AFM、TG/DTA等分析手段对复合粒子微观结构进行了表征；结果表明：纳米银粒子表面被聚合物层包覆，复合粒子呈明显的核壳结构，实现了微观尺度上的复合；同时，初步探讨了纳米银/聚苯乙烯核壳复合粒子的形成机理，指出：通过控制反应条件，可以使形成纳米银/聚苯乙烯核壳复合粒子的聚合反应方式占主导地位，实现最大限度地包覆。

In this article, the factors that affect molecular weight and solubility of polyacrylamide are studied and suitable initiator system is selected. The optimum parameters of copolymerizing process are obtained as follows: the molar proportion of acrylamide and sodium acrylate is 7:3, the monomer concentration is 30%, pH value of solution is 12, the oxidizer (K2S2O8) concentration is 0.1%, the reducing agent (NH2CONH2) concentration is 1%, the chain-transfer agent concentration is 0.4%. The initial reaction temperature is 35℃.

讨论了影响聚丙烯酰胺分子量和溶解性能的因素，选取了合适的氧化-还原引发体系，确定了制备超高分子量速溶型部分水解聚丙烯酰胺的优化聚合工艺参数：起始共聚合反应温度为35℃，保持在密闭条件下的共聚合反应2.5h后，再将聚合反应温度升高到55℃，继续反应2h，反应结束；反应溶液单体总浓度：30％，共聚合反应溶液pH值：12，氧化剂K_2S_2O_8：0.1％，还原剂NH_2CONH_2：1％，共聚合反应中两种单体的投料比：丙烯酰胺：丙烯酸钠=7：3，异丙醇链转移剂：0.4％。

The humidity resistance and the sensitivity to chemical warfare agents simulants of the tuned films were also investigated.Self-assembled LBL polyaniline films were prepared from aniline monomers by in situ polymerization and the mechanism of film formation was discussed. It was proposed that the self-assembly of polyaniline occurred through the quick absorption of aniline monomer cations or aniline monomer cation radicals on the glass surfaces by electrostatic attractions to form homogeneous polymerization centers, then increased gradually by the way of upright to the glass supports for extensity, leading to the polyaniline chain growth. The polyaniline was doped under acidic condition to absorb anionic polyelectrolyte, such as sodium polystyrene sulfonate based on the electrostatic force, or to adsorb polymer based on hydrogen-bonding interactions, for example Polyvinyl Alcohol, and then recycled to fabricate_n or_n self-assembled multilayer films.

跟踪了原位聚合的具有纳米结构的聚苯胺多层自组装膜的成膜过程，提出了该自组装膜的成膜机理：聚合反应初始阶段的苯胺阳离子或苯胺阳离子自由基通过静电作用快速吸附到带负电荷的基片表面，形成均匀的聚合中心，然后以垂直于基片的方式进行链增长生成PANI；PANI在酸性条件下经现场掺杂后带正电荷，再通过静电作用吸附带负电荷的聚电解质如聚苯乙烯磺酸钠，或通过氢键作用吸附聚合物如聚乙烯醇，这样循环LBL-SA即得到_n或_n等原位聚合聚苯胺自组装膜。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。