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The time for the reaction to go to completion depends on both the amount of catalyst and acetic anhydride used.

该酰化反应进行到完全所需的时间取决于催化剂用量和乙酐用量。

The acylation of 2,3-dimethyl-2-butene by acetic anhydride in the presence of H3PO4 was investigated.

在H3PO4存在下进行了2,3-二甲基-2-丁烯与乙酐的酰化反应。

The effects of the amount of catalyst, the amount of acetic anhydride, reaction time, and addition of solvents etc. on the acylation reaction were investigated.

考察了催化剂用量、乙酐用量、反应时间和溶剂的加入等因素对该酰化反应的影响。

It was found that H3PO4 is an effective catalyst for the acylation of 2,3-dimethyl-2-butene by acetic anhydride at room temperature.

结果表明,H3PO4是室温下催化2,3-二甲基-2-丁烯与乙酐酰化反应的有效催化剂。

Ferrocene will be acetylated by the action of phosphoric acid* and acetic anhydride*.

二茂铁可以与磷酸*和乙酐*作用而被乙醯化。

The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究,采用硫磺及乙酐复合催化剂,并且对氯化温度、氯化气氛、尾气回收等进行了过程优化,实现了乙酸氯化反应工艺条件的重大突破,使得氯乙酸的收率达到92.1%。

Kinetics of photo-chlorination of acetic acid to form monochloroacetic acid ;2. The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究,采用硫磺及乙酐复合催化剂,并且对氯化温度、氯化气氛、尾气回收等进行了过程优化,实现了乙酸氯化反应工艺条件的重大突破,使得氯乙酸的收率达到92。

The volume ratio of furaldehyde to acetic anhydride is 1∶2; the mole ratio of furaldehyde with anhydrous potassium carbonate is 1.00∶0.54. The best phase transfer catalyst is PEG1000, the mass ratio of PEG1000 with furaldehyde is 4.3%, the reaction time is 11 min, the reaction power of microwave is 260 W. The yield ofα-furanacrylicacid is up to 72.3% under these reaction conditions.

研究结果表明:在微波辐射功率为260 W、微波反应时间为11 min、以聚乙二醇1 000(PEG1000)为相转移催化剂,糠醛与乙酐的体积比为1∶2,糠醛与无水碳酸钾的量比为1.00∶0.55时,α-呋喃丙烯酸的产率为72.3%。

Ferrocene will be acetylated by the action of phosphoric acid* and acetic anhydride*.

二茂铁可以与磷酸*和乙酐*作用而被乙醯化。在反应混合物中,产物的数量可以通

Ferrocene will be acetylated by the action of phosphoric acid* and acetic anhydride*.

二茂铁可以与磷酸*和乙酐*作用而被乙醯化。在反应混合物中,产物的可以通

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