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Chromatography peaks were obtained by GC-MS and 56 compounds were identified. The main components were linalyl butyrate (30.212%),(1α, 3α, 4β, 6α)-4,7,7-trimethyl-bicycloheptan-3-ol (10.940%),-4-carene (1.826%), 4-methylene-1-(1-methylethyl)-bicyclo [3.1.0] hexane (1.109%),β-myrcene (1.170%), limonene (5.784%), 3, 7-dimethyl-1, 6-octadien-3-ol (5.742%), n-hexadecanoic acid (0.914%) and-9, 12-octadecadienoic acid (2.952%), etc.

用GC-MS分离出69个峰,鉴定出56种物质,主要成分为:芳樟丁酸酯(30.212%)、(1α, 3α, 4β, 6α)-4,7,7-三甲基-双环[4.1.0]庚烷-3-醇(10.940%)、-4-蒈烯(1.826%)、4-亚甲基-1-(1-甲基乙基)-双环[3.1.0]环己烷(1.109%)、β-月桂烯(1.170%)、柠檬烯(5.784%)、3,7-二甲基-1,6-辛二烯-3-醇(5.742%)、n-棕榈酸(0.914%)、-9,12-十八碳烯酸(2.952%)等。

They were acetic acid, benzaldehyde, n caproic acid, methyl pentadecanoic methyl ester, glycerin, benzoic acid,,9 octadecadienoic methyl ester, squalane, stearic acid and oleic eicosyl ester.

它们是乙酸、苯甲醛、正葵酸、-甲基十五烷酸甲酯、丙三醇、苯甲酸、,9-十八碳二烯酸甲酯、角鲨烷、硬脂酸和二十烷基油酸酯。

The research on anti-fatigue and anti-hypoxia functions of octacosanol extractants and the relativity of which with the purities of octacosanol extractants were carried out in this paper, which depended on the target related to creatural action and biochemistry.

并且本文将这三个纯度的二十八烷醇产品作为受试物,从动物行为学和生化指标的变化,来研究其抗疲劳、耐缺氧作用和检验其功效与二十八烷醇产品纯度是否具有相关性。

This paper is studied on a new synthesis method of amino-modified organic silicone micro-emulsion of cationic style by one step with a silane-alkyl coupling,3-(2-aminoethyl)-aminopropyl methyl dimethoxy silane while opening-cyclo polymerization of the octa-methyl cyclo tetra siloxane,thus the optimal manufacturing conditions are determined by comparing test of their properties.

采用硅烷偶联剂氨乙基氨丙基甲基二甲氧基硅烷改性,八甲基环四硅氧烷开环聚合,探索一步合成阳离子型氨基改性有机硅微乳新方法,通过其性能测试得出其最佳工艺条件:反应温度:80℃,反应时间:3 h,十六烷基三甲基溴化铵用量:5%,脂肪醇聚氧乙烯醚用量:5%,预乳液滴加时间:2 h。

The main volatile chemical components were n-hexadecanoic acid (24.03%), dodecanoic acid (6.20%) tetradecanoic acid (6.44%), 6, 10, 14-trimethyl-2-pentadecanone (4.03%), nonanal (4.54%), anthracene (4.26%), benzeneacetaldehyde (4.25%).

主要成分有:正十六酸(24.03)%、十四酸(6.44%)、6,10,14-三甲基-2-十五烷酮(4.30%)、壬醛(4.54%)、蒽(4.26%)、苯乙醛(4.25%)。

Silver nanoparticles with average particle size ranging from 2 to 131nm were manipulatively synthesized starting from silver nitrate using 10 kinds of different functional group-containing organic modifiers, such as polyvinylpyrrolidone, tween-80, sodium dodecyl sulfate, sodium polyacrylate, polyethylene glycol, D-sorbitol, sodium dodecyl sulfonate, sodium dodecylbenzene sulfonate, polyvinyl alcohol, cetyltrimethylammonium bromide, at room temperature.

摘 要:选择10种含有不同官能团的有机物为表面修饰剂,如聚乙烯吡咯烷酮、吐温-80、十二烷基硫酸钠、聚丙烯酸钠、聚乙二醇、山梨醇、十二烷基磺酸钠、聚乙烯醇、十二烷基苯磺酸钠和十六烷基三甲基溴化铵等,在室温下进行了平均粒径在2~131nm范围内纳米银颗粒的控制合成研究。

Finally the application of the homemade ODS for MSPD and the economical availability of the product was evaluated. Results show as the following: 1. It is a simple method for the preparation of a bonded octadecyl phase which has large particle and high extent of coverage of the bonded phase.

研究结果表明:①采用大粒径无定形硅胶为基质,选择十八烷基三氯硅烷为硅烷化试剂,完整地合成了一种大颗粒、高表面积的ODS键合相,合成的ODS可作为基质固相分散MSPD的固相分散剂,用于样品的前处理。

Fine chemicals to add auxiliary Series: lubricating oil pour point depressant, calcium zinc magnesium methacrylate, methyl acrylic acid lauryl ester, tetradecane methacrylate ester, methacrylic acid octadecyl ester, a acid ethylene glycol, diethylene glycol methacrylic acid ester, glycidyl methacrylate, the second reduction of three ethylene glycol dimethyl acrylate, acrylic acid lauryl ester, tetradecyl acrylate, octadecyl acrylate, acrylic acid ethylene glycol, diethylene glycol acrylate esters, glycidyl, two shrink three acrylate such as ethylene glycol.

精细化工添加助剂系列:润滑油降凝剂,甲基丙烯酸钙锌镁,甲基丙烯酸月桂酯,甲基丙烯酸十四烷酯,甲基丙烯酸十八烷基酯,甲基丙烯酸乙二醇,甲基丙烯酸二乙二醇酯,甲基丙烯酸缩水甘油酯,二缩三乙二醇二甲基丙烯酸酯,丙烯酸月桂酯,丙烯酸十四酯,丙烯酸十八酯,丙烯酸乙二醇,丙烯酸二乙二醇酯,丙烯酸缩水甘油酯,二缩三乙二醇丙烯酸酯等。

Results Eleven compounds were obtained and identified as sarcodonin A, scabronine B, 3β-hydroxy-5α, 8a-epidioxyergosta-6, 22-dien,(22E, 24R)-ergosta-7, 22-diene-3β, 5α, 6β-triol,(22E, 24R)-ergosta-7, 22-diene-3β-ol, benzoic acid, 4-hydroxylben-zaldehyde, 4-monopropanoylbenzenediol, ethy1-β-D-glucopyranoside, thioacetic anhydride,(2S, 2'R, 3S, 4R)-2-(2-hydroxyoctadecanoylamino) docosane-1, 3, 4-triol.

结果共分离鉴定了11个化合物,分别是:sarcodonin A、scabronine B、3β羟-5α,5α-过氧麦角甾-6,22-二烯-3β-醇、(22E,24R)-麦角甾-7,22-二烯-3β,5α,6β三醇、(22E,24R)-麦角甾-7,22-二烯-3β-醇、苯甲酸、对羟基苯甲醛、对羟基苯甲酸乙酯、乙基-β-D-吡喃葡萄糖苷、硫代乙酸酐、(25,2'R,3S,4R)-2-(2-羟基-十八碳酰胺)二十二碳烷-l,3,4-三醇。

ASpheric FeNi nanoparticles with average diameter of about 70 nm were obtained in the system of cetyltrimethyl ammonium bromide/H_2O,while most of the products were nanofilms/rods with the addition of cyclohexane; nearly monodisperse FeNi nanoparticles with average diameter of about 25 nm were prepared in the system of PEG/cyclohexane/H_2O.With the assistance of ultrasonic,a no-surfactant method to 8.5 nm FeCo nanocrystals with high Ms(>200.5 emu/g)has been developed with economical FeCl_3·6H_2O as iron sources.

a以水合肼为还原剂在十六烷基三甲基溴化铵/H_2O体系中得到了平均粒径约70 nm的FeNi合金球形颗粒,当在此体系中加入环己烷时样品主要形态为纳米膜/棒;于PEG/环己烷/H_2O体系中制备了单分散性较好的平均粒径约25 nm的FeNi合金纳米颗粒,合金纳米颗粒粒径随金属离子浓度减小而减小。

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