查询词典 synthesis method

It is involved in the synthesis of triphenylcarbinol. In this pater, based on the principle of the ultrasonic wave radiation and its advantages, triphenylcarbinol was synthesized by ultrasonic irradiation. We have researched the influence on the synthesis of triphenylcarbinol for the solvent of different purity.

三苯甲醇的制备中就涉及到了格氏试剂的合成，本文根据超声波辐射作用的原理及其优点，利用超声波辐射法合成了三苯甲醇，考察了不同纯度的乙醚溶剂对产物合成的影响。

Results ET-1 increased the synthesis of soluble type I collagen in different periods besides the 24h group, and had no effects on the type III collagen; immunohistochemical staining revealed that ET-1 also increased the synthesis of unsoluble type I collagen.

结果 ET-1较对照组除24小时时相外，均有不同程度的促HDPC可溶性I型胶原合成作用，但对III型胶原作用不明显；经免疫组化染色证实：ET-1尚可同时促进细胞非溶解性I型胶原合成。

Bidentis were studied by adopting indoor bioassay. The results showed that the volatile matter of F. bidentis had not allelopathy to four receptor plants. The eluviated matter inhibited seedling growth of cotton obviously, the inhibition ratio of root and stem were 6.29% and 10.42% respectively. The aqueous extract of litterfall and root exudates had different inhibition to four receptor plants, The synthesis effectof all treatments was significantly greater than eluviated matter treatment except for B3 of the aqueous extract of root exudates, such as the synthesis effect of all treatments (A1, A2, A3, B1, B2, B3 and eluviation) were 44.74, 29.37, 14.5, 31.54, 16.52, 3.55, 1.48 respectively.

结果显示：黄顶菊自然挥发物对受体植物不表现化感作用；黄顶菊淋溶物对棉花幼苗生长表现出明显的抑制作用，对棉花幼苗高度和根长的抑制率分别为6.29%和10.42%；黄顶菊枯落物浸提液和根系分泌物浸提液对4种受体植物均表现出不同程度的抑制作用，除了黄顶菊根系分泌物浸提液 B3处理外，其它处理的综合效应均显著大于淋溶物处理，如黄顶菊枯落物浸提液（ A1、 A2、 A3）、根系分泌物浸提液（ B1、 B2、 B3）以及淋溶物等各处理对受体植物的综合效应分别为44.74、29.37、14.5、31.54、16.52、3.55、1.48。

Methods: 2ethyl aniline was used as starting material of the synthesis and was processed by acetic anhydride acylation, strong nitric acid nitraction at low temperature, and desacyl synthesis to produce 2ethyl5nitro aniline. The product was then synthesized to 3methyl6nitro1Hindazole by using ringclosing reaction in the presence of NaNO2, and then ethylated to obtain 2,3diethyl6 nitro2Hindazole. The latter compound was then reduced by SnCl2/Hcl to get target compound 2,3diethyl6nitro2Hindazole.

以2乙基苯胺为原料经醋酐酰化、浓硝酸低温硝化及去酰基保护合成2乙基5硝基苯胺，后用亚硝酸钠关环得3甲基6硝基1H吲唑，经硫酸二甲酯甲基化得2，3二甲基6硝基2H吲唑，最后用氯化亚锡将其还原得到目标产物，通过1H NMR确定结构与目标产物一致。

Methods: 2-ethyl aniline was used as starting material of the synthesis and was processed by acetic anhydride acylation, strong nitric acid nitraction at low temperature, and desacyl synthesis to produce 2-ethyl-5-nitro aniline. The product was then synthesized to 3-methyl-6-nitro-lH-indazole by using ring-closing reaction in the presence of NaNO2, and then ethylated to obtain 2, 3-diethyl-6- nitro-2H-indazole. The latter compound was then reduced by SnC12/Hcl to get target compound 2, 3-diethyl-6-nitro-2H-indazole.

以2-乙基苯胺为原料经醋酐酰化、浓硝酸低温硝化及去酰基保护合成2-乙基－5-硝基苯胺，后用亚硝酸钠关环得3-甲基－6-硝基－1H-吲唑，经硫酸二甲酯甲基化得2，3-二甲基－6-硝基－2H-吲唑，最后用氯化亚锡将其还原得到目标产物，通过1HNMR确定结构与目标产物一致。

Along with the science and technology development, the networking popularization,the digitized technology will become now the science and technology development the front, the transformer substation digitization to further promotes the transformer substation synthesis automation level to get up to the limit the big promoter action, is the future transformer substation construction development direction.based on this kind of development demand, this transformer substation uses edcs-6200 the 110kv transformer substation synthesis automation.solves at present using the digitized technology to synthesize the automated transformer substation existence the question possibly to become.this transformer substation is causes the transformer substation using the digitized technology information gathering, the transmission, processing, the output process to digitize completely, and causes the correspondence network, the model and communication protocol unitizing, the equipment intellectualization, the movement management automation.

随着科学技术的发展，网络技术的普及，数字化技术成为当今科学技术发展的前沿，变电站数字化对进一步提升变电站综合自动化水平将起到极大促进作用，是未来变电站建设的发展方向。基于这种发展的需求，该变电站采用edcs-6200型110kv变电站综合自动化。利用数字化技术来解决目前综合自动化变电站存在的问题已成为可能。本变电站就是利用数字化技术使变电站的信息采集，传输，处理，输出过程全部数字化，并使通信网络化，模型和通信协议统一化，设备智能化，运行管理自动化。

The synthesis of alkylcyclohexylbenzoic acid: take the synthesis of ethylcyclohexylbenzoic acid as a typical example. With the AlCl3 as the catalyst, cis+trans acetylcyclohexylbenzene is synthesized from the reaction of acetyl chloride, cyclohexene and benzene.

烷基环己基苯甲酸的合成研究：主要研究了乙基环己基苯甲酸的合成，以乙酰氯、环己烯、苯为原料，三氯化铝为催化剂，合成乙酰基环己基苯，用水合肼、氢氧化钾、一缩二乙二醇经过高温加热还原羰基(Wolff-黄鸣龙还原)，将所得到的乙基环己基苯用乙酰氯进行傅克酰基化得到乙基环己基苯乙酮，所得中间体经过处理之后直接得到反式产物，将反式异构体的乙酰基氧化得到反式烷基环己基苯甲酸。

Through the comparison between methanol synthesis process and ammonia synthesis process, the specific features of chemical production process with different product and their effects on integration of the polygeneration system are discussed.

首先概述了多联产系统集成的原则思路，分析了生产醇醚燃料和合成氨的两类化工系统的流程特点，指出了其对化工和动力系统集成的影响。

At the same time, with reference to the conditions of synthesis of methyl ester of salicylic acid, we combined ethyl ester of salicylic acid, salicylic acid-n-butyl, isobutyl salicylate, amyl salicylate, isoamyl salicylate and salicylic acid benzyl ester,besides, experimented the possibility for series of ester synthesis catalyst with Sodium bisulfate as a catalyst .

同时参照水杨酸甲酯的合成条件合成了水杨酸乙酯、水杨酸丁酯、水杨酸异丁酯、水杨酸戊酯、水杨酸异戊酯和水杨酸苄酯，实验了以硫酸氢钠为催化剂合成系列酯的可能性。

On the basis of the total synthesis of-ypaoamide, the asymmetric synthesis ofthe key segment of marine natural product Microcolin B 97 was achieved.

在以上研究工作的基础上，完成了海洋天然产物Microcolin B关键片段97的不对称合成。

There had been a moment during the breakfast meeting, though, after the backslapping and the small talk and when all of us were seated, with Vice President Cheney eating his eggs Benedict impassively and Karl Rove at the far end of the table discreetly checking his BlackBerry, that I witnessed a different side of the man.

那次早餐会期间，在表示过关心和寒暄以后，我们所有人坐了下来，我注意观察了一下，副总统切尼面无表情地吃着班尼迪克蛋（Eggs benedict，源自美国，以英式松饼、火腿、水煮蛋以及荷兰酱组合而成），卡尔。罗夫在餐桌的远端谨慎地经常查看他的黑莓手机，我目睹了他所不为人知的一面。

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