查询词典 synthesis method

The replacement of toxic and volatile organic solvents as reaction media or an efficient catalyst with environmentally acceptable alternatives are an area of tremendous importance in modern organic synthesis. Basing the review about solid-phase synthesis with simple separation, the liquid phase organic synthesis supported by the solution polyethylene glycol and the chemical reactions in the medium of PEG, herein we are going to study the synthesis of 1-amidoalkyl-2 -naphthols in presence of the solution catalyst or the solid catalyst and the synthesis of thiourea in PEG-400 medium.

难溶性载体试剂参与下的固相合成使分离操作简单易行；可溶性聚乙二醇支载下的液相合成显示出液相反应的稳定高效性，同时兼顾大分子聚合物容易沉降分离的优点；无毒且稳定的小分子PEG作为反应介质，往往表现出醚和醇的双重性质和功能。

Main points of the thesis are as follows:(1) The main function models and information relations between these models in the CAPP system in the integrated CAD/CAM project are explained, a new process plan design method is mentioned based on analyses of process plan design. This method is based on the process plan prototype, and develops the prototype little by little until the perfect process plan is completed, the prospect of this method is discussed;(2) The feature abstracting rules and methods are studied, a feature coding system is developed based on GT, all the defined feature models are described by the mathematical methods;(3) The integrated method of CAD/CAPP based on features is mentioned, this method defines a feature exchanging model, and develops an interface software to exchange design data into technology data base, this technology data base includes the design and technology information of the parts;(4) The process plan reasoning method based on features is created, this method uses Mycin algorithm to solve the reasoning of the feature process plan. A process plan making system is developed. In this system part process plan is made by the semi-intelligent method, this method uses the feature reasoning, feature process chain searching and man-computer talking together;(5) The main structure of the HOPE system is introduced, a shaft drawing and its process plan made by this system are shown, the data process problem in process drawing making is also discussed;(6) A new method of describing process rule is introduced, this method uses IfThen rules and neural nets weight values together to describe process rules, the BP algorithm is adopted in this method;(7) The optimal machining sequence problem of the process steps on the same fixturing is discussed, optimal algorithms SA is applied to solve this problem, the result shows that this method is more efficient than the traditional method;(8) All jobs in the thesis are summarized. In order to carry out the research in the future, some rational proposals are given.

全文论述的内容主要有下列几个方面：(1)较为系统地阐述了CAD／CAM一体化工程项目中CAPP系统的主要功能模块及其信息流程，在分析工艺设计过程的基础上，提出了基于特征原型的渐进式工艺设计方法，并探讨了该方法的应用前景；(2)研究了零件特征提取的原则和方法，在成组技术的基础上，开发了一套基于特征的分类编码系统，并在提取零件特征的基础上，定义了零件特征的数据模型，开发了基于轴类零件特征的参数化设计系统；(3)研究了基于特征的CAD／CAPP集成的方法，通过定义零件特征数据模型的存储结构，开发了将设计数据转换到工艺数据库中的接口程序，为后续的CAPP系统提供必要的零件形状和工艺信息；(4)研究了基于特征的工艺推理方法，将Mycin算法应用到工艺决策中，开发了基于特征的工艺推理及工艺方案生成系统，在系统中综合运用特征推理、特征加工工艺链查询及人机对话相结合的半智能化方法确定零件加工工艺；(5)介绍了整个HOPE系统的总体结构，通过运行HOPE系统绘出了一轴类零件的零件图，并生成了该零件的加工工艺方案，初步探讨了基于特征的工序图生成技术中数据处理问题；(6)研究了工艺设计过程中知识如何有效表示的问题，提出了将显式的IF-THEN规则表示与隐式神经网络权值表示相结合的工艺知识表示方法，并利用BP算法进行了工艺知识表示的初步研究；(7)研究了工艺设计过程中同一安装下工步优化排序问题，利用神经网络中基于模拟退火的理论来解决该工步优化排序问题，实践证明该方法较传统的算法具有更高的效率；(8)总结了本文所进行的研究工作，为今后进一步开展工作提出了较为合理的建议。

By the algorithm, the surfaces are first divided into a series of mapping areas and synthesis areas using the constraints of the triangles' normal and texture attributes. Then the mapping areas are textured by harmonic mapping from the 2D mapping sample, by a patch-based synthesis method. Finally, the synthesis areas are textured by a triangle-based synthesis method.

首先以三角形法向量、切向矢量与纹理尺度为约束，将三角网格曲面分割为一系列映射区与合成区；然后用基于块的平面纹理合成方法生成大面积样图，用调和映射方法对映射区进行纹理映射；最后采用基于三角块的合成方法生成合成区纹理。

In this paper Ⅰ successfully applied these methods to fault diagnosis, and presenting some new innovative machinery fault diagnosis method; First Ⅰ present a new gear wornout fault diagnosis method, this method use the vibration signal's time-frequency attribute and instantaneous phase undulation to accurately detect gear's fault, and by comparing with the traditional frequency domain analysis method, this method reveals that many nonlinear and nonstationary characteristic exist in gear's vibration, this tell us that if we use frequency domain analysis method without pay attention to the signal's characteristic, we could get wrong diagnostic result; Then Ⅰ present a new bearing fault diagnosis method, this method use ATVFD and Hilbert transform to do envelop demodulation,Ⅰ analyze the envelop with time-frequency method and find out that this method is more accurate then traditional method.Ⅰ also explain that the modulation of the fault to the carrier wave may also be non-stationary and nonlinear; Finally Ⅰ present a cylinder pressure measurement method of diesel engine by means of vibration, cylinder pressure is an important parameter of diesel engine fault diagnosis, the pressure measuring is simplified a lot by this method,Ⅰ also use the ATVFD and time-frequency analysis to realize it.

本文中将上述理论方法成功地应用到故障诊断中去，提出了几点创新性的诊断方法；提出了一种齿轮磨损故障诊断的新方法，该方法利用振动信号能量的时频域分布特征与瞬时相位波动特征可以进行精确的齿轮故障诊断，并通过与传统的频域诊断方法的比较，揭示出齿轮振动中存在的明显的非线性与非平稳特征，说明了不加选择地利用频域分析方法进行齿轮故障诊断很可能会得到错误的诊断结果；提出了一种轴承故障诊断的新方法，该方法利用ATVFD分解与Hilbert变换进行包络解调，并对解调得到的包络信号进行时频域分析，可以实现更加准确轴承故障诊断，说明了故障对载波信号的调制往往也是非平稳与非线性的；提出了一种利用振动信号进行柴油机汽缸内压力检测的新方法，柴油机汽缸压力的变化是柴油机故障诊断的重要参数，利用振动方法可大大简化汽缸压力的检测过程，该方法也是综合利用ATVFD分解与时频域分析方法实现的。

On the design of algorithms, a novel exact hierarchical delay analysis method for general circuits is proposed; based on the sensitization theorem for sequential circuits, an exact minimizing clocking method is proposed; based on Boolean process, a waveform simulation method considering interconnecting delay for logic circuit and a parallel waveform simulation method are proposed; a new method that transforms bit-level waveform polynomial to word-level polynomial model is proposed; a multiple valued synthesis algorithm based on multiple valued Boolean process and a wire-centered delay synthesis policy are proposed, in which timing planning, floorplanning, wire planning and optimal clock skew in early design are considered; a two-layers channel routing method for minimizing crosstalk under grid mode is proposed; based on the transition numbers theorems for waveform polynomial, a new method for generation of test with noise effects is proposed.

算法设计方面，提出了一种精确的通用电路层次化延时分析方法；基于时序电路的敏化定理提出时序电路最小时钟周期精确确定方法；提出基于Boolean过程论的考虑互连延迟的逻辑电路波形模拟方法，在分析了波形模拟适合并行化基础上，进一步提出一种并行波形模拟算法；提出一种将位级电路波形多项式描述转化成字级多项式描述的新方法；提出一种基于多值Boolean过程的多值电路综合算法以及一种将前期设计定时规划、前期设计的布局规划和线网结构化方法及低偏移的时钟分配等技术相结合的面向互连延时的综合策略；提出一种串绕最小化的网格模式下的双层通道布线方法；从波形多项式描述跳变数的定理出发提出了一种考虑噪声效应的测试生成新方法。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, acetochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、电化学法、乙醛酸钙法、尿素三氯乙醛合成法、尿酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, ace-tochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、化学法、醛酸钙法、素三氯乙醛合成法、酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

This train classifies "information carrier adhering to the build" as design elements, and probes into integrated design method of it and single building separately: method of definite position, method of definite form and method of combination; Then, this train probes into integrated design method of it and colonys building , that bases on the cognitive design method: method of rhythm controls,method of node outstanding, and that aims at the design method to protect: method of protect original, method of repairing and method of renewal.

本文的第四部分提出了一体化设计的思路，将建筑附着信息载体作为设计元素，探讨了它与建筑单体一体化设计的方法：定位法、定形法、混合法；以及它与建筑群体一体化设计时，基于认知的设计方法：节奏控制法、节点突出法，旨在保护的设计方法：存真法、修缮法、更新法。

It was observed after 24hrs of reaction that this lipase could compete very well with lipase from Candida antartica (93. 0％ for isoamyl butyrate synthesis and 95. 0％ for ethyl caproate synthesis) and lipase from Mucor miehei (75. 0％ for isoamyl butyrate synthesis and 93. 64％ for ethyl caproate synthesis).

反应24h后，来自Candida antartica脂肪酶合成丁酸异戊酯和己酸乙酯的转化率分别为93.0％和95.0％，来自Mucor miehei脂肪酶合成丁酸异戊酯和己酸乙酯的转化率分别为75.0％和93.64％。

There are three main synthesis routes:direct synthesis of imines;one-pot synthesis of imine with oxidation;one-pot synthesis of imine with reduction.

主要有三种合成路线：直接合成亚胺；一锅法氧化合成亚胺；一锅法还原合成亚胺。

Bob Eckert has been chairman and chief executive of Mattel for eight years.

美泰董事长兼首席执行官鲍勃·埃克尔特在任已8年。

The outlook for honors and disgraces carries on and surpasses the traditional outlook for honors and disgraces theoretically, and carries on and develops the theory of construction of socialist mora...

社会主义荣辱观的提出在理论上是对传统荣辱观的一次继承和超越，是对社会主义道德建设理论的继承和发展，在实践上有利于形成良好的社会风尚。