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Based on groups of single factor experiments, the yield could reached to 88.8% with the conditions: sodamide: cedrol :dimethyl sulfate = 1.6:1:0.9, refluxed 2h in first step reaction, and reacted at room temperature 1h after instillation of dimethyl sulfate, followed refluxed 1h in the second steps.

通过多组单因素实验发现氨基钠:柏木脑:硫酸二甲酯的摩尔比为1.6:1:0.9,第一步反应条件控制在回流2h,第二步反应先室温(25℃)滴加硫酸二甲酯后反应1h,再回流反应1h,得率可达88.8%。

In retrospect, Motorola has taken solid steps to initiate innovation in the field of telecommunications so as to become the leader in cellular phone technology.

回首往事,摩托罗拉公司一步一个脚印地进行着电信领域中的技术革命,成为有目共睹的移动电话技术的领导者。

The cellulose nitrate containing secondary amine group was prepared by one-pot method in two steps: etherification and amination.

以硝化纤维素为原料,经一锅法醚化和胺化 2步反应合成了仲胺型硝化纤维素。

Every lecture has a plot: a central point with a series of steps that build up this point.

每堂课都有自己的结构:经过一系列的层次发展后,中心点就会凸显出来。

The preparation process includes the following steps: dissolving activator and RE oxide in the molar ratio of 0.01-0.02 in concentrated nitric acid and heating to dry, dissolving the obtain RE nitrate in deionized water to obtain solution of RE nitrate; dissolving soluble tungstate and surfactant in deionized water to obtain tungstate solution; mixing the RE nitrate solution and the tungstate solution through stirring to reaction for 25-60 min to obtain white precipitate; hydrothermal reaction of the precipitate in a reaction kettle at 100-260 deg.c for 24-72 hr; centrifugally separating, washing and drying to obtain the product.

浓硝酸的加入量保证稀土氧化物溶解就可以,过量的硝酸可以加热除去;将可溶性钨酸盐和表面活性剂溶解于去离子水中,得到钨酸盐溶液,表面活剂性的加入量为反应原料重量的0-30wt%;将稀土硝酸盐溶液加入到钨酸盐溶液中搅拌,发生沉淀反应,磁力搅拌时间为25-60分钟,得到白色沉淀;将含有沉淀物的溶液作为前驱物加入到反应釜中,发生水热反应,反应温度为100-260℃,反应时间为24~72小时;离心分离,洗涤,干燥,即得所需产物。

The synthesis method comprises the following steps: adding 2-( 5-(dimethylamino methyl- 2- furyl methyl sulpho ethylamine and 1- methylthio- 1- methylamino- 2- nitro ethylene with a molar ratio of 1.04: 1 into water, heating to 48- 52 Deg. C, reacting 4.5 hours with a vacuum degree of 0.02- 0.05 MPa, cooling, adding sodium-hydroxide of concentration of 10% to regulate the PH value to 11.0- 11.4, filtrating and cooling the filtrate to 0- 2 Deg. C, crystallizing for 12 hours, centrifugally filtrating, and rinsing filter cake with purity water to prepare wet ranitidine alkali; dissolving ranitidine alkali in alcohol and reacting with chlorhydric acid to prepare ranitidine hydrochloride.

合成方法包括:将摩尔比为1.04∶1的2-(5-(二甲氨基甲基-2-呋喃基甲基硫代乙胺与1-甲硫基-1-甲胺基-2-硝基乙烯加入水中,升温至48-52℃,于真空度0.02~0.05MPa反应4.5小时,反应完毕降温,用10%氢氧化钠溶液调pH=11.0-11.4,抽滤,滤液降温至0~2℃,结晶12小时,离心甩滤,用纯化水漂洗滤饼,得雷尼替丁碱湿品;将雷尼替丁碱溶于乙醇中与盐酸反应,制备得到盐酸雷尼替丁,产品符合欧洲药典标准。

You subject the resulting heart homogenate, which is dense and opaque, to a series of differential centrifugation steps.

你把得到的密集而不透明的牛心匀浆液用一系列的差速离心。

Cepheid's easy-to-use systems integrate a number of complicated and time-intensive steps, including sample preparation, DNA amplification and detection, which enable the analysis of complex biological samples in its proprietary test cartridges.

易用的系统整合了一系列复杂和耗时的步骤,包括样品制备、DNA扩增及检测,这样就可以在公司专有的监测盒中分析复杂的生物样品。

When the villagers were going through their cere monies to drive away pestilential influences, he put on his court robes and stood on the eastern steps.

乡里迎神驱鬼时,穿着朝服站在东面的台阶上。11。问人于他邦,再拜而送之。康子馈药,拜而受之。曰:"丘未达,不敢尝。"

Obviously all process steps are highly important in order to get a desired CG picture.

显然所有的过程步骤最重要的是得到一张想要的CG图像。

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推荐网络例句

It's not quite as simple as that.

并没有那么容易。

It debuted in 1992 in Japan and the United Kingdom, and 1993 in the United States.

它首次亮相于1992年在日本和英国,在美国1993年。

Nevertheless, moving free game confluence inchoately is driven is overflowed mostly adapt make game, game needs have the aid of to move the consequence that overflows successful work to win a player.

不过,早期的动漫游戏融合大多是从动漫改编成为游戏,游戏需借助动漫成功作品的影响力赢得玩家。