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The optimum conditions of reaction of each reaction:(1) The synthesis condition of PS with monocarboxylic acid terminated is that the mole ratio reatant of FeCl2·4H2O/chloroactic acid was 2.0, the reaction temperature 110℃, the reaction time

各步的最佳聚合反应条件:(1)mPEG与丁二酸酐反应最佳条件:溶剂为甲苯

Can induce the reaction of cleavage H atom from methyl on the ring of deactivated toluenes,such as nitrotoluene. The carbanions caused by base are the very important reaction intermediums, which determined the reaction rate and reaction effect.

该反应体系中,NaOH的加入对此催化反应起着相当关键的作用,研究表明强碱也能像温度一样促进苯环卜甲基的摘氢速度,使底物形成相应的硝基苯甲基阴离子,稳定的硝基苯甲基阴离子是氧化反应进行的重要中间体。

The rhythmic hydrogenation reaction of piperylene C5 petroleum resin produced by Fushun Zhengchuan chemical plant was carried out by using the laboratory made catalysts that load of palladium is 1.0%, load of other metals is 1.0%. The best hydroprocessing conditions are:reaction temperature is 270 ℃, reaction pressure is 3.0 MPa, reaction time is 4 h.

采用含钯质量分数1.0%,其他金属质量分数1.0%的自制催化剂对抚顺市正川化工厂生产间戊二烯C5石油树脂,在高压釜中进行间歇加氢,最佳工艺条件为:反应温度270℃,反应压力3.0MPa,反应时间4h。

The main objective of this research project is to modify the Methyl-Acetylene/propadiene selective hydrogenation reaction system of the No.3 Naphtha Cracker in CPC. The original gas phase reaction system was redesigned to a liquid phase reaction so that higher propylene selectivity was achieved and lower rates of propane and green oil were produced. To recover effectively the higher production of valuable propylene from the reaction system, the following fractionator was also redesigned.

本研究之目的在於修改中油公司三轻工场老旧的甲基乙炔/丙二烯选择性氢化气相反应系统,使成为液相反应系统,藉由液相反应的优异性,提高由MAPD氢化得到丙烯之选择率,同时降低丙烷及绿油产率,以增加丙烯产率,另亦修改丙烯精馏系统,以提升蒸馏塔提纯之效率。

The 352 valid samples were analyzed by SPSS. The results showed there was no distinct corresponding relationship between the product attributes and reaction time. The different key attributes from questionnaire importance rating and the shortest reaction time standards were used to regressively analyze the results of customers' overall rating (such as overall satisfaction,objective quality, recommend intention).The results indicated that the coefficiency of regression of the special attributes chosen from reaction time to overall rating was distinct, while the coefficiency of the special attributes chosen from importance rating to overall rating was not. The main conclusions are: 1. Regarded attributes can be obtained by the reaction time of brand performance rating.

本实验的有效样本为352个,通过SPSS软件进行分析统计,数据统计结果显示,在品牌表现评价反应时与其重要性问卷评定结果的相关系数的检验中,并未发现品牌表现评价反应时与品牌属性重要性评定结果之间的显著相关;将由问卷重要性评价最高标准所得到的关键属性与通过品牌表现评价反应时最短的标准所选取的关键属性的品牌表现分别对消费者的总体评价结果(如&总体满意度&、&主观质量&、&推荐意向&)进行回归分析,发现通过品牌表现评价反应时方法选取的特殊关键属性(与问卷重要性评定法选取不一致的关键属性)的品牌表现对总体评价结果的回归系数显著,而重要性评定问卷法选取的特殊关键属性(与品牌表现评价反应时法选取的不一致的关键属性)的品牌表现对总体评价结果回归系数不显著。

A new fullerene derivative containing energy-producing groups was prepared, and the reaction conditions affecting the yield were studied by the kroenecker method. The optimal reaction conditions with a 53.5% yield (based on consumed C60) are: 1:3:6 of molar ratio of C60 , o–nitrobenzaldehyde and sarcosine , 55℃ of reaction temperature, 12 h of reaction time, 40mL of toluene solvent.

利用N-甲基甘氨酸、邻-硝基苯甲醛和C60反应,合成分离出了含有硝基的新型富勒烯吡咯烷衍生物,通过正交试验对其工艺条件进行了研究,探讨了反应物剂量比、温度、时间和溶剂体积对产物产率的影响,得到了合成产物的最佳工艺条件:反应物剂量比为1:3:6、温度为55℃、反应时间为12h、溶剂甲苯体积为40mL,此时产物产率可达到53.5%(以消耗的C60计)。

The photo decomposition reaction of lead styphnate is a simple thermal decomposition reaction, in which light energy rise will increase the rate of decomposition reaction of lead styphnate and the decomposition reaction has clear stages at higher light energy.

激光束能量增大能明显地提高斯蒂醋酸铅的分解反应速率,而且在较高的光能量下,分解反应出现明显的阶段性。

The optimal reaction conditions were as follows:chloroform was used as the reaction solvent,3,5-propionyl acid 0.02 mol,sulphoxide diloride 0.054 mol,the reaction temperature 50℃ and the reaction time 5 h. Under these conditions,the yield of product was 98.9%.

对酰氯合成条件进行了研究,得出优惠反应条件为:以氯仿作溶剂、β-(3,5-二叔丁基-4-羟基苯基)丙酸0.02 mol、二氯亚砜0.054 mol、反应温度50℃、反应时间5 h,优惠条件下产品的收率为98.9%。

The phosphorus oxychloride or phosphorus tribromide N, N-dimethylformamide mix and react to form the Vilsmeier reagent used in the reaction. The newly prepared Vilsmeier reagent is added into the reaction bottle provided with the return condenser and the blender; a reaction raw material N, N-dimethylformamide solution expressed in the reaction formula is added into the system; the temperature is risen; the corresponding multi substituting pyridine-2 (1 H)-ketone compound can be made after the column chromatography of the silica gel; the production rate is between 60 and 95 percent according to different reactions.

由三氯氧磷或三溴化磷N,N-二甲基甲酰胺混合获得反应中所用Vilsmeier试剂;将新配制的Vilsmeier试剂加入装有回流冷凝管、搅拌器的反应瓶中,向体系中加入反应通式中表示的一种反应原料的N,N-二甲基甲酰胺溶液,升温,经硅胶柱层析分离得相应的多取代吡啶-2(1H)-酮类化合物,产率视不同反应在60~95%之间。

Moreover, the kinetics of the esterifieation reaction using ammonium molybdate as catalyst was studied. The result showed that the reaction was chemical reaction controlling. The rate equations were established, and the reaction models gave satisfactory result.

对钼酸铵为催化剂时2,6-NDCA甲酯化反应动力学进行了研究,结果表明,该反应属化学反应控制,根据实验结果,建立了反应的宏观动力学方程式,动力学模型有较好的拟合效果。

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从有历史以来,英国,在此地早期居住的是凯尔特人,已经被征服了三次。

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