查询词典 optimum condition

Through the orthogonal experiment, the optimum condition for tagatose synthesization was determined to be 0.02 mol/L calcium chloride, 30 min, acetum neutralization.

通过正交设计实验优化反应条件，最终确定以0.02 mol/L的CaCl2为催化剂，反应时间30 min，用醋酸中和金属氢氧化物D-塔格糖复合物时，D-塔格糖的产率最高，可达到49.05%。

In order to explore the optimum condition of transition of Pb, the transfer behavior of Pb through the emulsion liquid membrane system of TBP-Span80-atoleine-kerosene was studied. The study analyzed the effect of Pb transport rate of membrane phase component, pH values in external aqueous phase, acidness in internal aqueous phase, rew and concentration of metal ions in external aqueous phase. In the case of the optimal technological conditions, the waste water of Pb, Cu and Ni was treated.

为了探求乳化液膜法迁移铅Pb(Ⅱ的最佳条件，采用磷酸三丁酯－Span80-液体石蜡－煤油乳化液膜体系研究了Pb的迁移行为，探讨了膜相组成、外水相pH、内水相酸度、乳水比、Pb起始浓度对Pb迁移率的影响，确定了最佳迁移条件，并在此条件下对含Pb、Cu和Ni废水进行了处理。

The processing technique of synthesis and purification of medium-chain triglycerides by alcoholysis, using camphor tree seed oil as material, was investigated by orthogonal analysis, and the optimum condition of the processing technique and performance parameter of product were obtained.

以樟树籽仁油为原料，通过正交实验法研究了用醇解法合成和纯化中碳链甘三酯的生产工艺，得到了中碳链甘三酯生产工艺的最佳条件及产品的物性参数。

In this paper, through a series of experiments, two series of quaternary-ammounium Gemini surfactants were synthesized, namely the pair alkylene double quaternary ammonium salt surfactant m-s-m·2Br and the pair the alkylene double quaternary ammonium salt surfactant -s-·2Br. We has carried on the attribute with the infrared spectrum to its structure, and to affected the factor which the synthesis pair the alkylene double quaternary ammonium salt surfactant responded to carry on the discussion. We has discovered the synthesis pair the ethylene double quaternary ammonium salt surfactant m-2-m·2Br optimum condition: The bromo alkane and a tetramethyl ethylene diamine mole of ratio is 3.0: 1.0, makes the solvent by the ethyl alcohol, 80℃ under responds for 48 hours in the backflow temperature; Synthesis pair alkylene double quaternary ammonium salt surfactant 12-S-12 ·2Br optimum condition: 12 tertiary amine and 1, 3- propylene dibromide (1, 4- two bromines butane) a mole of ratio is 2.2: 1.0, makes the solvent by the ethyl alcohol, responds for 48 hours in the constant temperature 80 ℃ under backflow.

本文通过一系列的实验，合成了两个系列的Gemini型表面活性剂，即双烷撑双季铵盐表面活性剂m-s-m·2Br和双烷撑双季铵盐表面活性剂-s-·2Br，用红外光谱对其结构进行了表征，并且对影响合成双烷撑双季铵盐表面活性剂反应的因素进行了讨论，找出了合成双乙撑双季铵盐表面活性剂m-2-m·2Br的最佳条件：溴代烷与四甲基乙二胺的摩尔比为3.0：1.0，以乙醇作溶剂，在回流温度80℃下反应48小时；合成双烷撑双季铵盐表面活性剂12-s-12·2Br的最佳条件：十二叔胺与1，3-二溴丙烷(1，4-二溴丁烷)摩尔比为2.2：1.0，以乙醇作溶剂，在恒温80℃下回流反应48小时。

The dependence of current efficiency on concentration of pyruvic acid, ammonia, and sal ammoniac.η value reached 90% at an optimum condition.

在优化的工艺条件下，电合成丙氨酸电流效率达到90%，比文献报导的64%提高了许多。

Filter paper and lindane can be degraded effectively by the complex microbial system during pH 7~9 which also was the optimum condition of cellulose degrading, and in the condition of pH 10, lindane was degraded 49.62%, much more than that of cellulose.

在纤维素降解最佳的pH值7～9范围内，也同样有利于林丹的降解，而在纤维素降解较少的pH值为10的条件下，林丹的降解率高达49.6％。

Filter paper and lindane can be degraded effectively by the complex microbial system during pH 7～9 which also was the optimum condition of cellulose degrading, and in the condition of pH 10, the degradation ratio of lindane reached 49.62%, much more than that of cellulose.

在纤维素降解最佳的pH值7～9范围内，也同样有利于林丹的降解，而在纤维素降解较少的pH值为10的条件下，林丹的降解率仍高达49.6%。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅，张金艳，梁英，沈勇(黑龙江八一农垦大学文理学院，黑龙江大庆 163319)摘要：以33%的氢氧化钠水溶液为缚酸剂，异丙醇胺、环戊酮和二氯乙酰氯为原料，采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷，采用正交实验法得到最佳反应条件：反应原料摩尔比为1∶1∶1.2，苯作溶剂，反应的温度为-15 ℃~-10 ℃，搅拌时间为3 h，产率达到50.0%。

The optimum reaction condition was as follows: catalyst dosage=4.3% of the amount of ethanediol,reaction time 50 min.1,4-dioxane yield of 84.82% was obtained under the optimum condition.

考察了催化剂用量、反应时间和反应温度等因素对收率的影响，得出最佳反应条件：催化剂用量为乙二醇质量的4.3%，反应时间50 min，收率可达84.82%。

The making condition for releasing cholesterol from the inclusion compound was found based on the single factor experiments. The experiments demonstrated that the releasing rate of cholesterol was reached to more than 97% in the optimum condition including pH value 9.5,regurgitant time hour,concentration of edible ethanol 96% and regurgitant temperature 80C.

利用单因素实验确定山包合物释放胆固醇的优化工艺条件：pH值为9.5，回流时间为1h，乙醇浓度为96％，回流温度为80℃，此时胆固醇的释放率达到97％以上。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。