查询词典 molar quantities

The yield was about 32% by optimizing the scalar of catalyzer and the molar ratio of reactants.

在实验中，对催化剂的用量和反应物的投料比进行了优化，在最优条件下，目标产物收率为32％左右。

Results showed that reaction temperature has little effect on the molar ratio of catechol to hydroquinone and reactive period of catalyst.

试验结果表明，反应温度对反应产物中邻苯二酚/对苯二酚的比例和催化剂的活性周期的影响不明显，过氧化氢/苯酚摩尔比对邻苯二酚/对苯二酚的比例的影响较大，提高过氧化氢/苯酚摩尔比会降低邻苯二酚/对苯二酚的比例，缩短催化剂的活性周期。

In order to explore the relationship between structure and properties of hydroxyalkyl cellulose ether nitrate, molecular structures of nitrate ester of hydroxylethyl cellulose ether, nitrate ester of hydroxylpropyl cellulose and nitrate ester of cellulose glycerol ether with molar substitution of 1 were simulated by using Synthia module of Materials Studio, and their performances of nitrogen content, glass transition temperature and Young's modulus were predicted.

为探索羟烷基纤维素醚硝酸酯的结构与性能关系，借助Materials Studio软件中的Synthia模块模拟了摩尔取代度为1的羟乙基纤维素醚硝酸酯、羟丙基纤维素醚硝酸酯和二羟丙氧纤维素醚硝酸酯的结构，并预测了它们的含氮量、玻璃化转变温度和杨氏模量。

The invention discloses an InP quantum point preparing method, comprising the steps of:(1) mixing InCl3 with trioctylphosphine oxide, and preserving heat at 90-110DEG C to prepare a solution whose In content is 0.1-0.3mol/L;(2) raising temperature to 130-180DEG C, and charging argon gas;(3) injecting PSi(CH333 into InCl3-TOPO compound in the molar ratio of 1 to 1-1 to 2;(4) when the solution color turns into transparent red or orange, raising temperature to 260-270DEG C and preserving heat;(5) lowering temperature to 90-110DEG C and injecting dodecyl amine, decyl amine or mercaptan;(6) dissolving reacting mixture in nonpolar solvent to form transparent colloidal solution, then adding in polar solution until the colloidal solution is muddy, and centrifugally separating and obtaining deposits and supernatant; and (7) centrifugally separating the supernatant, where the above steps (1)-(5) are performed.

本发明公开了一种InP量子点的制备方法，其步骤为：①将InCl 3 与三辛基氧膦混合，在90～110℃保温制得In含量为0.1～0.3mol/L的溶液；②升温到130～180℃，通入氩气；③将PSi(CH 3 3 3 注射入InCl 3 -TOPO复合物中，其摩尔比为1∶1～1∶2；④待溶液颜色变为透明的红色或橙红色，将升温260～270℃保温；⑤降温到90～110℃，注入十二胺、癸胺或硫醇；⑥将反应混合物溶于非极性溶剂，形成透明的胶体溶液，然后加入极性溶剂，直至胶体溶液出现混浊状，然后离心分离获得沉积物和上层清液；⑦取上层清液进行离心分离。上述步骤①～⑤在保护气氛下进行。

The preparation process includes the following steps: dissolving activator and RE oxide in the molar ratio of 0.01-0.02 in concentrated nitric acid and heating to dry, dissolving the obtain RE nitrate in deionized water to obtain solution of RE nitrate; dissolving soluble tungstate and surfactant in deionized water to obtain tungstate solution; mixing the RE nitrate solution and the tungstate solution through stirring to reaction for 25-60 min to obtain white precipitate; hydrothermal reaction of the precipitate in a reaction kettle at 100-260 deg.c for 24-72 hr; centrifugally separating, washing and drying to obtain the product.

浓硝酸的加入量保证稀土氧化物溶解就可以，过量的硝酸可以加热除去；将可溶性钨酸盐和表面活性剂溶解于去离子水中，得到钨酸盐溶液，表面活剂性的加入量为反应原料重量的0-30wt％；将稀土硝酸盐溶液加入到钨酸盐溶液中搅拌，发生沉淀反应，磁力搅拌时间为25-60分钟，得到白色沉淀；将含有沉淀物的溶液作为前驱物加入到反应釜中，发生水热反应，反应温度为100-260℃，反应时间为24～72小时；离心分离，洗涤，干燥，即得所需产物。

The synthesis method comprises the following steps: adding 2-( 5-(dimethylamino methyl- 2- furyl methyl sulpho ethylamine and 1- methylthio- 1- methylamino- 2- nitro ethylene with a molar ratio of 1.04: 1 into water, heating to 48- 52 Deg. C, reacting 4.5 hours with a vacuum degree of 0.02- 0.05 MPa, cooling, adding sodium-hydroxide of concentration of 10% to regulate the PH value to 11.0- 11.4, filtrating and cooling the filtrate to 0- 2 Deg. C, crystallizing for 12 hours, centrifugally filtrating, and rinsing filter cake with purity water to prepare wet ranitidine alkali; dissolving ranitidine alkali in alcohol and reacting with chlorhydric acid to prepare ranitidine hydrochloride.

合成方法包括：将摩尔比为1.04∶1的2-(5-(二甲氨基甲基-2-呋喃基甲基硫代乙胺与1-甲硫基-1-甲胺基-2-硝基乙烯加入水中，升温至48-52℃，于真空度0.02～0.05MPa反应4.5小时，反应完毕降温，用10％氢氧化钠溶液调pH＝11.0-11.4，抽滤，滤液降温至0～2℃，结晶12小时，离心甩滤，用纯化水漂洗滤饼，得雷尼替丁碱湿品；将雷尼替丁碱溶于乙醇中与盐酸反应，制备得到盐酸雷尼替丁，产品符合欧洲药典标准。

The results indicate that improving temperature to reflux, using low polarity solvent as dispersion medium and proper molar ratio of tetrabutyl titanate to stearic acid can bring out good modification. The function of tetrabutyl titanate is to react with the surface hydroxyl groups and adsorbed H2O on the powder particles to produce new binding sites such as M—O—Ti—OC4H9and M—O—Ti—OH, which can easily react with the carboxylic acid. As temperature increases from room temperature to reflux temperature, the reactions between RCOO- and Ti change from coordinate bonds to covalent bonds, which makes the carbon chains of stearic acids more strongly bound with the powder particles surface.

研究结果表明，提高处理温度、适当增加复合改性剂中硬脂酸的量并选用极性弱的有机溶剂可达到比较理想的改性效果；钛酸四丁酯的作用是与粉体粒子表面的羟基以及吸附水反应产生偶联点，如M—O—Ti—OH，这些偶联点易于与羧酸反应；在低温时RCOO-与偶联点的Ti之间以配合物的形式发生作用，在回流温度下处理时，主要发生酯化反应，使硬脂酸更牢固地嫁接到粉体粒子表面，改性效果更好。

1 At a reaction temperature of 100 ℃ and a reaction time of 30 min to give 2,which was then subjected to condensation reaction with p-propoxy mandelic acid in the presence of phosphoric acid at a molar ratio of m(2)∶m( p-propoxy mandelic acid )∶m=1∶1∶1 at a reaction temperature of 60 ℃ for 3 h to yield 3,which was further oxidized by chloranil to give t.

对现有分散红356合成工艺进行了优化，以n∶n=1.2∶1投料，100℃反应30 min得缩合物2，再在等质量磷酸催化下与分批加入的等质量对丙氧基扁桃酸60℃缩合3 h得缩合物3，经温和氧化剂四氯苯醌氧化得标题化合物，总收率55%。

When the molar ratio of 2 chloroacetic acid∶ p chlorophenol is 1.25 and pH=5～7 at 104 ℃ reaction for 20 min in the 20% NaOH solation,the yield of PCPA can be reached 90%.

氯乙酸∶对氯苯酚为 1 2 5 ，质量分数为 0 2的氢氧化钠溶液中，pH值在 5～ 7之间，温度在 10 4℃左右为宜，反应时间为 2 0min ，PCPA收率为 90 3%。

I already enter the forth month today, growing up a little, i can eat one vitellus now, sometimes i also eat some molar biscurt, i want growing up chop-chop .

今天我已经进入了第四个月，我又长大了点，现在我可以吃一个蛋黄了。有时我还会吃些磨牙饼干，我要快快长大。

His female bullfighter Lydia gradually Health love, but she was in a vegetative state after the Bulls Zhuangcheng away from her, just because Lydia's ex-boyfriend showed more affectionate than he is like love.

他对女斗牛士莉迪亚渐生爱意，却在她被公牛撞成植物人后离她而去，仅仅因为莉迪亚的前男友表现出好似比他更深情的爱。

I know of none which are not easy to answer, but what I am trying to do now is only by a series of hints to throw some light on the narrow path of legal doctrine, and upon two pitfalls which, as it seems to me, lie perilously near to it.

我不认为有什么难以回答的问题，但我现在要做的仅仅是通过一系列线索，来给法律理论的狭窄路径以及在我看来离它近得危险的两个陷阱提供一些启示。