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The results revealed that the conversion was 92.4% when aniline concentration was 1 mol/L, feeding temperature was 25℃ and residence time was 11 s. With feeding temperature being the main factor, the effect of residence time decreases successively. The diazotization anomalies could be caused at aniline concentration above 1.5 mol/L. The proper feeding temperature which can lead to the highest conversion was 20~30℃.

试验结果表明,在苯胺浓度为1 mol/L,进料温度为25℃,停留时间为11 s时反应转化率达92.4%;苯胺浓度、进料温度、停留时间对反应影响程度各不相同,其中进料温度的影响最大,停留时间次之,苯胺浓度高于1.5mol/L后,对反应影响加剧,导致反应异常;从进料温度对反应的影响试验分析可得,反应转化率最高的进料温度在20~30℃之间。

Results: When the quantity of monochloroacetic acid was 0.3 mol, The preferable conditions were 0.42 mol dimethylamine, reaction temperature about 40℃, 2-hour reacton time and 50 ml dilute water.

结果 当氯乙酸投料量为0.3mol时的最佳反应条件为二甲胺0.42 mol,缩合温度40℃左右,缩合时间2h,稀释水量50ml。

The equilibrium association constant K of DNR with fish sperm DNA is 1.98×105 mol/L and that of DNR with denaturated DNA is 2.29×104 L/mol.

研究发现嵌入作用是柔红霉素和天然DNA之间的主要作用方式;并且柔红霉素和天然DNA之间的作用要强于和热变性单链DNA之间的作用。

The measured reaction enthalpy is 80 kJ/mol, the reaction volume is 10 mL/mol.

测得的反应热量与体积分别为80 kJ/mol和10 mL/mol。

Thus, 3 mol of Ethyl acetoacetate were treated with 2 mol of formaldehyde to yield 80% of I.

用2摩尔的甲醛处理3摩尔的乙酰乙酸乙酯可得到80%的I。

The optimum experimental conditions were as follows: the excitation and emission wavelengths of the complex were 332 nm and 618 nm, respectively, pH=7.5, the concentration of europium ion was 1.2×10^(-5) mol/L, the surfactant concentration of SDBS was 3.0×10^(-5) mol/L.

最佳测定条件为:最大激发和发射波长分别是332和618 nm;pH=7.5;Eu(上标 3+)浓度为1.2×10^(-5) mol/L,SDBS浓度为3.0×10^(-5) mol/L。

The results show that melting point and fusion enthalpy of the fresh nano-aluminium powders are 649.7 ℃ and 3.7 kJ/mol in Ar, respectively, which are 10.3 ℃ and 7.09 kJ/mol lower than those of coarse-grained Al.

研究结果表明:在Ar气流中,新纳米铝粉的熔点为649.7 ℃,熔化焓为3.7 kJ/mol,分别比粗晶铝的熔点(660 ℃)和熔化焓(10.79 kJ/mol)低10.3 ℃和7.09 kJ/mol;在N2气流中,从20 ℃升温到800 ℃时,新纳米铝粉增重约为33%,熔点为648.8 ℃。

The experimental results indicate that oleic acid has inhibitory effect on the precipitation, and the inhibitory effect is more obvious with increasing addition of oleic acid. Specially, oleic acid of 1×10^(-5) mol/L would facilitate the agglomeration of gibbsite, oleic acid of 1×10^(-4) mol/L would inhibit the agglomeration of gibbsite.

结果表明:油酸对铝酸钠溶液的种分过程产生比较明显的抑制作用,油酸的添加量越大,抑制作用越明显;添加1×10^(-5) mol/L油酸时可促进附聚,添加1×10^(-4) mol/L油酸时抑制附聚。

Methods:YCP was coupled to bovine serum albumin to construct three neoglycoprotein s which are different in their degrees of substitution(DSs;≈3,≈6,or ≈10 mol of BSA carrier/mol of YCP hapten,respectively),and their immunogenicities were evaluated in mice following subcutaneous immunization,respectively.

将YCP与牛血清白蛋白共价偶联,获得取代度分别约为3、6和10的3种拟糖蛋白,经皮下分别接种ICR小鼠,测定免疫血清中多糖YCP的特异性抗体IgM和总IgG水平,以及半抗原和载体蛋白的特异性IgG亚型。

A method was developed to determine the activation energy and material parameters in the hyperbolic sine constitutive equation.The activation energies determined are 570 kJ/mol and 548 kJ/mol for steel T122 in saturation stress and peak stress,respectively.The values of critical strain for dynamic recrystalli...

采用应变硬化速率—应力曲线图较精确地获得了饱和流变应力和峰值应力;用回归法确定了双曲线本构方程中的变形激活能及材料常数,确定了T122钢在饱和应力和峰值应力条件下的变形激活能分别为570和548 kJ/mol;采用力学方法直接从流变曲线确定了T122钢发生动态再结晶的临界应变量,并回归出临界应变量与Zener—Hollomon参数的关系式。

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