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Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

The Km and Vmax were 7.35 mg/ml and 0.206 nmol/min-mg for ChoA, and 30.42 mg/ml and 0.376xmol/min-mg for ChoB, respectively. A 270bp DNA fragment, the partial chitosanase gene from Penicillium sp.

酶A的米氏常数K_m及最大反应速度V_分别为7.35 mg／ml、0.206 μmol／min·mg，酶B的米氏常数K_m及最大反应速度V_分别是30.42 mg／ml、0.376μmol／min·mg。

The results indicated, catalytic activity was very high, the average rate of O 2 uptake was 4.25×10 -2 mmol/min after 10 min, the yield of cyclopentanone was up to 83%.

实验结果表明，该催化体系对环戊烯的羰基化显示出较高的催化活性，反应 1 0 min，反应的平均吸氧速率为 4.2 5× 1 0 -2 mmol/min，环戊酮的收率可达 83%。

The CPF/ZnO nanomaterial, obtained by treating the precursor PF/ZnO at 460 ℃ for 40 min, could fully decolorize and degrade dye MB in 10 min under the natural light compared with 10% degradation of MB on ZnO only under the same reaction condition. The decolorizing efficiency will be still above 80% after 3 cycles.

如在460 ℃下处理40 min所得的纳米复合材料，在自然光条件下，10 min即可使MB溶液完全脱色，而在相同条件下，纯纳米ZnO仅能使MB的脱色率为10%左右；该催化材料重复使用3次仍可使MB溶液的脱色率保持在80%以上。

Results demonstrate that the Cu(superscript 2+) can be concentrated effectively under the following condition: exchange column internal diameter 0.8 cm and 15 cm high, the dosage of spiral algae 2 g and pH value 6, the flow rate of the dry food leach solution 10 mL/min, elute with 0.6 mol/L HCl at a flow-rate of 6 mL/min.

结果表明，在交换柱内径为0.8 cm、柱高为15 cm、螺旋藻用量为2 g、pH值6的条件下，干制品浸出液流速为10 mL/min时，用0.6 mol/L HCl以6 mL/min的速度洗脱，可对Cu(上标 2+)进行高效富集。

Methods 58 cases patients needing endocardiac orthoptic surgery were enrolled in this study, they are divided into control group and SFI group randomly. Injecting of SFI 1ml/kg by intravenous before CPB was performed in group SFI, tidal volume, Pmax , Pmean and calculating Crs and RI during 10 min , 30 min , 60 min after the trachea intubating, in the beginning of CPB and during 10min, 60min, 120min after CPB were recorded.

选择临床心内直视手术病人58例，随机分为对照组和SFI组，SFI组于CPB前予SFI 1ml/kg静注，记录气管插管后10、30、60 min，CPB手术开始时，CPB停止后10、60、120min时的潮气量、气道峰值压、平均气道压并肺顺应性和呼吸指数。

Methods Forty-five patients with hysteromyoma undergone hysteromyomectomy were randomly assigned to three groups (n=15,each group): group Ⅰ, control group without pre-emptive analgesia; group Ⅱ, the patients were administrated with 0.2 mg·kg-1 ketamine intravenously 30 min before operation; group Ⅲ, 30 mg ketamine was administrated into epidural analgesia 30 min before operation.

45例子宫肌瘤患者均于硬膜外麻醉行全子宫切除术，随机分为3组，即Ⅰ组：对照组，术前不施行超前镇痛；Ⅱ组：切皮前30 min静脉注入氯胺酮0.2 mg·kg-1；Ⅲ组：切皮前30 min将氯胺酮30 mg加入实验剂量(2%利多卡因4或5 mL)中注入硬膜外腔。3组术后均连接Graseby9300镇痛泵行患者自控硬腺外镇痛，镇痛药物为0.2%罗哌卡因加50 mg·L-1吗啡。

Results: Diacetyl monoxime solution of acetic acid and to without acetic acid DMA color liquid, transparent tube and the Brown tube of absorbance determination, 30 min to put average drop of 6.80%, 1.30% and 1.44%, 0.98%; 60 min put average drop 19.8%, 1.92% and

结果：二乙酰一肟乙酸溶液与无乙酸的DMA显色液，其透明管与遮光管测定的吸光度，放置30 min平均下降了6.80%、1.30%与1.44%、0.98%；放置60 min平均下降了19.8%、1.92%与2.49%、1.60%。

The underlying diseases included chronic glomerulonephritis(in 71 patients),nephrosclerosis(in 30),diabetic nephropathy(in 5),polycystic kidney disease(in 3),and miscellaneous or unknown disorders(in 9).The severity of renal insufficiency was classified under two groups according to the base-line creatinine clearance:32 patients had mild insufficiency (Ccr 46～60 ml/min),and 86 had moderate insufficiency (Ccr 30～45 ml/min).

先依次选用倍他乐克、双氢克尿噻、心痛定控制病人血压，待血压及肾功能稳定后，根据Ccr将病人分为轻度CRF组(Ccr 46～60ml/min)和中度CRF组(Ccr 30～45ml/min)，每组病人再随机分为治疗组（抑平舒2.5～5.0 mg/qd n=80）和对照组（n=38），所有高血压病人继用上述降压药维持正常血压，随访期6个月。

1 After comparison of sum fusion and optimal fusion, sum fusion was selected as the fusion scheme for local test statistics. For the distributed CFAR detection based on the above three local statistics and sum fusion: CA-R-SUM and OS-R-SUM, CA-S- SUM and OS-S-SUM, Max-OS and Min-OS, Max-CA and Min-CA, their analytic expressions of detection performance were derived for and in nonhomogenous background.

2.1 通过求和融合与最优融合的性能对比，确定了以求和融合做为对局部检测统计量的融合方案；推导出了基于上述三种新的局部检测统计量和求和融合的分布式 CFAR 检测方案： CA-R-SUM 和 OS-R-SUM 、 CA-S-SUM 和 OS-S-SUM 以及 Max-OS 和 Min-OS 、 Max-CA 和 Min-CA 在、条件下在非均匀杂波背景中检测性能的解析表达式。

Chrysanthemum of 10 thousand birthday is lax to edaphic requirement, with the arenaceous qualitative loam with fecund, good drainage had better.

万寿菊对土壤要求不严，以肥沃。排水良好的砂质壤土为好。

He unstepped the mast and furled the sail and tied it.

他拔下桅杆，把帆卷起，系住。