查询词典 methanol

The method on trans fatty acids analysis in food is very important. The effects of methylate sodium, potassium hydroxide, sulfuric acid and boron trifluoride in methanol and their different concentration and dosage on TFA analysis were studied. The chromatographic condition and the influence of time and temperature on the esterifation of TFA using boron trifluoride in methanol were optimized. A method for analyzing TFA were established by GC based on boron trifluoride in methanol and RT-2560(100m×0.25mm×0.2μm) capillary column.

研究了甲醇钠－甲醇、氢氧化钾－甲醇、浓硫酸－甲醇和三氟化硼－甲醇4种甲酯化试剂的浓度、用量及甲酯化时间和温度对反式脂肪酸检测的影响，优化了色谱条件，建立了以三氟化硼－甲醇法甲酯化，RT-2560(100m×0.25mm×0.2μm)毛细管柱为基础的反式脂肪酸气相色谱检测方法，C18：1-9 t， C18：1-11 t， C18：2-9 t， 12 t和C22：1-13 t 4种反式脂肪酸的最小检出浓度在0.774.08 mg/kg之间。4种反式脂肪酸不同添标浓度回收率为98.44%101.23%，重复测定的相对标准差在0.22%1.31%之间，有较好的准确度和重现性。

The main works include: 1. successfully observed the opalescence of critical methanol and the phase variation of PET degradation in methanol, studied the internal construction of PET in different stages of degradation, provided the conception of critical region and noncritical region of system in which PET and methanol participated.

主要内容如下： 1 实验观测了甲醇的临界乳光现象及PET在甲醇中降解的相态变化，同时研究了不同降解反应阶段PET内部结构特征，在本实验研究的范围内提出了PET在甲醇中的系统临界区域和非临界区域的概念。

M15 (methanol 15%, diesel 85%) and M30 (methanol 30%, diesel 70%) methanol/diesel fuel blends are tested in ZS1100 DI diesel engine. The study contents include load character, NO emission and smoke emission test. In addition, the solidifying point of the fuel blends is tested and the cost is estimated.

在ZS1100直喷式柴油机上，用自行配制的M15、M30甲醇－柴油混合燃料与纯柴油做了对比试验研究，进行了负荷特性、NO和碳烟的排放对比试验，还进行了混合燃料的浊点测试和成本估算。

The anode catalyst for direct methanol fuel cell is Pt-W-Sn/C, and it is prepared through dispersing carbon black in distilled water, adding H2PtCl6, tungstate and stannate, stirring to make the metal salt and H2PtCl6 adsorbed fully; dropping reductant to reduce and deposite until complete reaction; washing with distilled water, filtering and drying to obtain black C carried sanitary Pt-W-Sn catalyst. The catalyst has excellent methanol catalyzing activity and low cost, and its use can lower the cost of direct methanol fuel cell greatly and raise the performance/cost ratio of the cell.

一种直接甲醇燃料电池阳极催化剂是Pt-W-Sn/C；其制备方法是将碳黑分散在蒸馏水中，然后加入H2PtCl6、钨酸盐和锡盐，搅拌使得金属盐与H2PtCl6被充分吸附；逐滴加入还原剂使之还原沉积，待反应完全后，用蒸馏水洗涤，过滤，然后于干燥箱中干燥，便得到黑色的C负载Pt-W-Sn三元催化剂；该催化剂具有很好的甲醇催化活性，价格低廉，可以大大降低直接甲醇燃料电池的成本，提高电池的性能价格比和市场竞争能力。

Unroasted black sesame seeds were pressed and defatted with n-hexane, extracted with 80 % methanol, and separated by XAD-2 gel open column chromatography eluting with a serious of concentrations of aqueous methanol solutions (20 %, 40 % and 60 %). The 60 % methanol eluate, which contained higher content of ST compound, were collected and freeze-dried to obtain the ST extract powder.In animal experiment, we used vitamin E deficient rat model to increase oxidative stress.

试验材料为未经炒焙之泰国黑芝麻，将脱油后之芝麻粕先以80 %甲醇溶液进行萃取，经浓缩后再以XAD-2胶体进行管柱层析，以不同浓度之甲醇水溶液冲提后，收集ST含量较高之60 %甲醇水溶液区分层，行冷冻乾燥可得ST萃出物粉末。

Anthocyanidin extract in methanol showed 3 absorption peaks, at 270, 340 and 520 nm, in the UV-vis spectrum, with bathochromic and hypsochromic shift with methanol+AlCl3 and methanol+AlCl3+HCl, respectively; the ratio of the absorbance at 440 nm to that at 520 nm was 0.29. No fluorescence occurred under UV irradiance, and 5 absorption peaks occurred at 270 nm after HPLC. Five molecular ion peaks occurred on MS: 595, 381, 611, 587 and 571, respectively, and monosaccharides in the extract were identified as rhamuose and glucose on HPLC.

一品红花色素的甲醇溶液分别在270、340 和520 nm 处有 3 个吸收峰；在 440 nm 吸光度与可见光最大吸收波长 520 nm 吸光度的比值为0.29；花色素的甲醇溶液中加入AlCl3后发生红移，再加入HCl后发生蓝移；色素溶液在紫外光下无荧光；色素样品经液相色谱分离后在 270 nm检测有 5 个比较明显的吸收峰；质谱中得到 595、611、381、571 和 589 等对应的分子离子峰；花色素酸解液高效液相色谱图谱和鼠李糖、葡萄糖的出峰时间一致。

From the development of methane chloridate production, the early methane chloridate were mainly produced by methane chlorination, with the rapid development of methanol industry, the advantage of methanol hydrochlorinate become clearer and clearer and the methanol hydrochlorinate will take the place of methane chlorination in the world.

甲醇氢氯化法包括甲醇氢氯化反应生成一氯甲烷和一氯甲烷氯化生成多氯甲烷两步。按国外先进水平，该法甲醇总收率可达97.7％，氯总收率可达98.6％。从世界甲烷氯化物生产的发展来看，早期的甲烷氯化物生产是以甲烷热氯化法为主。

MTT assays indicated that the methanol extract from Hericium erinaceus and Lentinus striguellus have stronger cytotoxity against HeLa cells than other extracts.The methanol extracts from Agrocybe sp had the bioactivity of antibacteria and anti-candida.The methanol extracts from Phellinus vanini and Fistulina hepatica had the bioactivity of inhibition on elastase.

MTT测定表明大部分食药用真菌的甲醇提取物具有不同程度的细胞毒活性，猴头菌与巴西革耳甲醇提取物的作用较强；鳞伞甲醇提取物的抗细菌和抗真菌活性较强；牛舌菌和杨黄菌的甲醇提取物具有抑制弹性蛋白酶活性的作用。

The fungicidal activity of methanol extract was higher than that of ethylacetate extract. The bioassay showed that the methanol extracts of strain As fermentation products had certain degree fungicidical activity against Botrytis cinerea, Alternaria longipes, Glomerella cingulata, Curvulavia lunata, Gibberella zeae, Valsa malt under the concentration of 4000μg/mL, the inhibiting ratio against pathogen growth was ranging from 62.9%~85.1%; The results of the inhibition of spore germination indicated that the fermentation products exhibited obvious inhibition rate against Alternaria longipes, the EC50 values was 62.5328μg/mL; The bioassay showed that the methanol extracts of strain As fermentation products had certain degree fungicidical activity against Bacillus cereus , Bacillus subtilis.

其中甲醇提取物的抑菌活性较乙酸乙酯好，在4000μg/mL浓度下对番茄灰霉病菌、烟草赤星病菌、苹果炭疽病菌、玉米弯孢叫斑病菌、小麦赤霉病菌、苹果腐烂病菌6种植物病原真菌均有抑制作用，抑制率在62.9%~85.1%；抑制孢子萌发试验表明：菌丝体甲醇提取物对烟草赤星病菌的毒力较好，其EC50仅为62.5328μg/mL；抑制细菌活性表明菌丝体甲醇提取物对蜡状芽孢杆菌和枯草芽孢杆菌有一定的抑制作用，而对大肠杆菌无明显的抑制作用。

The results showed that (1) The grain size of nanometer YiO_2 was40～80nm.The wavelength corresponding to the maximum absorbency values were observedin the 200～320nm range.The crystal structure of carbon doped TiO_2 photocatalyst is primarilyanatase(22.43% rutile), and the content of carbon is about 4.6%.(2) The relative humidityvaring from 8% to 80%, the photocatalytic degradation degree of benzene increased withincreasing relative humidity; and to toluene, degradation rate was hanced by relative humidityup to 60%, and more or less inhibited above 60%.(3) Scheme and results of orthogonal testswere used by evaluating the photocatalytic performance of the gas phase methanol, acetoneand 1-heptane.The results revealed that their degradation degree reached 84.5%, 93.39% and93.45%, respectively.(4) The 254nm UV lamp showed higher photocatalytic degradation rate.For methanol, acetone and 1-heptane, it was found that photocatalytic degradation reactionoccurs with the light strength of daylight lamp.(5) Under the the same conditions, 15%degradation degree has been obtained for benzene, whilst about 10% degradation degree wasattained by Degussa P25; During the initial phases, the toluene revealed higher photocatalyticactivity, comparing with Degussa P25, the degradation degree of methanol, acetone and1-heptane were slightly lower.

结果表明：(1)CVD法制备的纳米TiO_2光催化剂，颗粒球形度好、粒径在40～80nm之间；最大吸光度值所对应的波长为200～320nm；含碳量约为4.6％；晶型组成主要为锐钛矿型，金红石的含量约为22.43％；(2)在相对湿度为8％～80％范围内，苯的光催化降解率随着相对湿度的增大而增大；甲苯在相对湿度为60％时达到最好降解效果，当相对湿度增大到80％时光催化效果降低；(3)将正交实验设计及实验方案应用于气相甲醇、丙酮和正庚烷光催化降解研究，实验结果表明：三者最高降解率分别为84.5％、93.39％和93.45％；(4)有254nm紫外灯参与的光催化实验可以大大提高有机气体的光催化降解率；在日光灯的照射下，掺碳纳米TiO_2对气相甲醇、丙酮和正庚烷具有一定的光催化氧化能力；(5)较P25粉，在相同的光催化操作条件下：气相苯的平均降解率达15％，高于P25粉10％的降解率；气相甲苯在初始阶段具有较高的反应速率；气相甲醇、丙酮和正庚烷的降解率略低于P25粉。

Objective To investigate the effects of interleukin-1 β converting enzyme gene on the biologic characteristics of ovarian cancer cells.

目的 探讨白细胞介素-1 β转换酶的表达，对卵巢癌细胞生物学特性的影响。

Campylobacter: This illness is the most commonly identified cause of diarrheal illness in the world.

弯曲：这种病是最常见的原因查明腹泻病，在世界上。