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Six derivatives of 4-phenyl-3-phenoloxymethyl-5-mercapto-1,2,4-triazlyole were synthesized from phenoloxyacetyl hydrazide by two-steps reaction under microwave irradiation, then reacted with 2-chloroacetic acid to give six novel derivatives of 2-(3-phenoxymethyl-4-phenyl-[1,2,4]triazole-5-thio)-acetic acid.

在微波辐射条件下，芳氧乙酰肼经两步反应制得4-苯基－3-芳氧甲基－1，2，4-三唑－5-硫酮衍生物，再与氯乙酸反应得到6种尚未见文献报道的2-（3-芳氧甲基－4-苯基－1，2，4-三唑－5-硫基）乙酸衍生物。

The results indicated that the thermal stability of thepolymers is greatly associated with the structure of the modified groups.Moreover, the imide- derivatives have greater thermal stability than thecorresponding amide- derivatives. This can provide useful information on thepreparation and processing of this kind of polymers.

用PyGC-MS对酰胺型和酰亚胺型改性聚乙烯在加工条件下的热分解产物进行了定性和定量的测定，结果表明不同改性基团对聚合物热稳定性有很大影响，酰亚胺型改性聚乙烯的热稳定性大于酰胺型，这为该类聚合物的制备加工和应用提供了有用的信息。

In contrast,the imides derivatives of maleated polyethylene are stable for long periods of time at 160℃,and the decomposition of phenethylamine imide-,9-aminomethylphenanthrene imide-derivatives is initiated slowly at 255℃ and 280℃,respectively.

聚乙烯的化学改性已得到广泛应用，它能使PE获得新的物理化学或功能特性，如改进其表面粘合、亲水及吸湿、染色和印刷性质等，尤其在增加它与其它聚合物的相容性，制备共混材料时常常是必不可少的[1 ，2 ] 。

The bank supports a proposal to send standard derivatives contracts through an industrywide clearinghouse that can be monitored by regulators. J.P. Morgan, however, opposes a requirement that the trades should be moved onto an exchange, in part, because it would inhibit the use of customized derivatives that clients require.

政府提出，针对整个行业设置受监管机构监控的票据交换所，通过这类票据交换所发送标准的衍生产品合约，摩根大通对此表示支持，但反对将衍生品交易转到交易所进行的要求，部分原因在于这种做法将会限制客户要求的定制衍生产品的应用。

A catalyst composition for the polymerization of propylene comprising one or more Ziegler-Natta procatalyst compositions comprising one or more transition metal compounds and one or more esters of aromatic dicarboxylic acid internal electron donors; one or more aluminum containing cocatalysts; a selectivity control agent comprising at least one silicon containing compound containing at least one C1-10 alkoxy group bonded to a silicon atom, and one or more activity limiting agent compounds comprising one or more aliphatic or cycloaliphatic carboxylic acids; alkyl-, cycloalkyl- or alkyl-ester derivatives thereof; or inertly substituted derivatives of the foregoing.

一种用于丙烯聚合的催化剂组合物，所述催化剂组合物包括：一种或多种齐格勒-纳塔主催化剂组合物，该主催化剂组合物包括一种或多种过渡金属化合物和一种或多种芳族二羧酸酯内部电子给体；一种或多种包含铝的助催化剂；选择性控制剂，该选择性控制剂包括至少一种包含硅的化合物，该化合物包括至少一种与硅原子连接的C 1-10 烷氧基；和一种或多种活性限制剂化合物，该活性限制剂包括一种或多种脂族或脂环族的单或聚羧酸类、其烷基-、环烷基-或烷基-衍生物、或上述惰性取代的衍生物。

Limits, Continuity, Derivatives, and Integration of Single Variable, Integration Techniques, Applications of Derivatives and Integrals, Infinite Sequences and Series, Multivariable Function and Their Derivative, Multiple Integrals, Integration in Vector Fields.

课程内容：单变数函数之极限、连续、微分、积分，积分技巧，微分与积分的应用，无穷数列与级数，多变数函数之偏微分、可微性，多重积分，极值问题，向量场积分。

In this paper we will mainly study the gauge fixing Yang-Mills heat flow of a principal bundleFor a principle bundle with a compact seme-simple Lie group as its structure group over a compact Riemannian manifold without boundary, the evolutions of the curvature and its higher derivatives under the flow above will be derived, and the energy inequality and the Bochner type estimates will be obtained. Then, the monotonicity formula and the small action regularity theorem can be proved. We will give the locally uniform estimates for the higher derivatives of the curvature.

本论文主要讨论主丛上的规范固定Yang-Mills热流我们在紧致无边黎曼流形上的以半单紧致李群为结构群的主丛上，推导了在规范固定Yang-Mills热流下曲率及其高阶导数的演化方程，得到了该热流的能量不等式和Bochner估计，由此可推出单调性公式和小作用量正则性，以及曲率各阶导数的局部一致估计。

Although the derivatives have lower toxicity, the curative effects are often lower than that of nitrogen mustard. And the toxic-side effect of the derivatives, such as bone marrow inhibition, cross-resistance, and mutation are still serious.

然而不幸的是这一问题并未得以解决，新的氮芥衍生物的毒性虽然小于氮芥，但细胞毒作用常低于后者，并且发现新的衍生物仍有相当的毒副作用，如骨髓抑制，交抗，致突变作用等。

The results show that the atmosphere has a big influence on the thermal stability of C_(60).C_(60) begins to decompose at 423.5℃in the air,the deomposed peak temperature is 668.5℃,but very stable in the helium atmosphere,only sublimate,the crystal shape of C_(60) has a certain influence to its thermal stability.The synthesized nine kinds of nitro-fullerene derivatives all have good thermal stability and their decomposed peak temperatures all exceed 350℃.The thermal explosion temperature for 5 seconds delay of product 4 is 253℃.The category,number and position of nitryl group in nitro-fullerene derivatives all have influence on their thermal stability.

利用差热分析仪和DSC-TG综合热分析仪对C_(60)及其硝基衍生物的热稳定性进行了研究，结果表明，环境气氛对C_(60)热稳定性影响很大，C_(60)在空气中423.5℃开始分解，放热峰值温度为668.5℃，在氦气中很稳定，仅表现为升华，C_(60)的晶型对其热稳定性也有一定的影响；合成得到的九种硝基富勒烯衍生物都具有较好的热稳定性，分解峰值温度均高于350℃；产物4的5秒爆发点测试结果为253℃。

Syntheses of PPVs derivatives with alkoxyl as side-chain by the method of dehalogenating condensation reaction Those PPV derivatives, named poly (2-methoxy-5-alkoxyl) phenylene vinylene,containing alkoxyl on benzene ring, were placed on emphasis in this paper.

一。通过强碱诱导的去卤缩合法合成支链含不同烷氧基的PPV衍生物本文首先重点研究了支链中含不同链长烷氧取代基的PPV衍生物：聚(2-甲氧基-5-烷氧基)对苯乙炔。

Do not gum up the work by telling mother what we are going to do .

别告诉母亲我们要干的事，那会把事情搞糟的。

In recent years, application of the partial prestressed concrete beam s is developed.

近年来，随着部分预应力砼梁应用的推广，发现我国规范所采用的名义拉应力法的计算结果不稳定。