查询词典 calcining

The thermal stability and specific surface area of the samples are improved by using mesitylene and phosphoric acid .Calcining temperature can affect the pore size and morphology of the samples.

经500℃焙绍5h 后，用磷酸处理的样品仍未出现晶相转变的迹象，表明经均三甲苯和磷酸处理后，样品的热稳定性和比表面积均有一定程度地提高。

The crystal structure was perovskite-like type, as evidenced by the results of X-ray diffraction and scanning electron micrography. The distribution of K4Nb6O17 powder with particle size of less than 10 m, which would become larger as the calcining temperature grew.

通过XRD和SEM对样品进行表征，发现该法合成的K_4Nb_6O_(17)均具有钙钛矿结构，样品的颗粒大小分布不均，但大多小于10μm，且合成的温度越高，颗粒粒径越大。

Based on the first heat treatment, the second ball milling and calcining favor the osculation and mass transfer of the reactants in the second solid state reaction, and compared with one-step method, the density of resultant LiFePO4/C is ameliorated.

在一次热处理的基础上，二次球磨和烧结有利于第二次固相反应过程中反应物质的接触和传质，较一步固相法提高了生成的LiFePO4的振实密度。

Taking phosphogypsum from factory as the raw material,the possibility of transformation into plaster of paris is studied by the experiments of chemical analysis,calcining technology,check test.

以磷酸厂废渣——磷石膏为原料，通过化学成分分析、磷石膏炒制、对比研究等实验，探讨了转化为建筑石膏的可能性。

With the co-precipitation, using cross experiment, constitute of catalyst (include 2 equations), proportionment of precipitator, aged time, calcine temperature, had been discussed-how to influence the activity of catalyst. The activity will be primed if prepareing the catalyst with CuO:ZnO:CeO_2=6:9:10, using NaOH as precipitator, aged time 3h, calcining the calatyst at 450℃.

在共沉淀法中利用正交试验对催化剂中各种物质的配比量、沉淀剂类型、陈化时间和焙烧温度这4种因素进行了4水平分析，结果显示制备催化剂时使用的金属盐Cu(NO_3)_2、Zn(NO_3)_2和Ce(NO_3)_3的物质的量之比符合n_1∶n_2∶n_3=6∶9∶10、并且NaOH溶液作沉淀剂、3h陈化后在450℃焙烧，制得的催化剂催化效果最好，在130℃时CO转化率即达到99％以上。

More sinterable yttria powders can be synthesized by calcining the hydroxide precursor with platelet-shaped structure.

添加适量的（NH4）2SO4能够减轻Y2O3粉体的团聚，沉淀的同时控制pH值在9以下，所得到的粉体具有更好的烧结性能。

Fine particles with diameter about 10nm to 200nm are obtained through hydrolysis and calcining of the complex alkoxide.

结合热分析、红外光谱、X射线衍射技术等研究了钙钛矿结构钛酸铅微粉的形成机理。

Different from conventional fabrication of cathode powder, non-chelating polymer polvinyl alcohol serves to sterically entrap the metal cationa in a manner thewey which facilitates the formation of an atomistically homogeneous precursor material. And, calcining the solid precursor material to form a mixed metal oxide material, that is perovskite structured powder La0.5Sr0.2Co0.5Fe0.5O3.

该方法与传统方法不同，采用非螯合聚合物－聚乙烯醇(PVA， Polvinyl alcohol)作为阳离子的载体，形成含有La(上标 3+)，Sr(上标 2+)，Co(上标2+)，Fe(上标 3+) 4种金属阳离子和非螯合聚合物的均匀溶胶，干燥生成固体凝胶状前驱体。

The structural and photocatalytic properties of TiO〓 as well as surface acidity were greatly improved by sulfation. SO〓〓/TiO〓 solid superacid with Hammett constant Ho less than -12.14 was prepared by treating the TiO〓 with 1.0mol. L〓 sulfuric acid solution and then calcining at 450℃ for 3h. When compared to unmodified TiO〓, the SO〓〓/TiO〓 superacid catalyst exhibited higher anatase content, smaller crystal size, higher specific surface area, centralized pore size distribution, and the blue-shifted band edge of uv-vis adsorption spectra. Furthermore, the SO〓〓/TiO〓 superacid also showed excellent reaction activity and stability for CH〓Br photocatalytic decomposition even under the moist reaction conditions. The apparent quantum efficiency of SO〓〓/TiO〓 was 10 times of that of TiO〓 catalyst for the photocatalytic degradation of bromomethane. Therefore, the SO〓〓/TiO〓 superacid catalyst is promising for practical application in environmental remediation.It was found that both L and B acid sites exist on SO〓〓/TiO〓 photocatalyst while only L acid sites on TiO〓 photocatalyst. On the basis of experimental results, the synergistic model of superacidic centers was proposed for SO〓〓/TiO〓 photocatalyst to explain the photocatalytic behavior and the mechanism of superacidifing effects, assuming that the adjacent L and B acid sites induced by SO〓〓 comprise cooperatively the superacidic center on superacid photocatalyst. The group cooperation of the superacidic center could strengthen the surface acidity, increase surface acid sites and the adsorbtion of O〓, promote separation of photogenerated electron-hole pair, enhance the interfacial transfer of charges and reversibility of water adsorption. Consequently the excellent photocatalytic activity, reaction stability and resistibility to humidity of SO〓〓/TiO〓 superacid photocatalyst may attributed to the group cooperated effect of the superacidic center on the photocatalyst.

研究结果表明：SO〓〓与TiO〓表面的结合为螯合式双配位结构；TiO〓光催化剂表面经H〓SO〓浸渍处理后，提高了表面酸性，改善了催化剂结构和光催化性能，当H〓SO〓浸渍浓度为1.0mol.L〓、烧结温度为450℃时，可制得SO〓〓/TiO〓超强酸催化剂(H〓＜-12.14)，其结构和光催化活性得到明显改善，与TiO〓相比，SO〓〓/TiO〓光催化剂的锐钛矿含量高、晶粒小、BET比表面积大、孔径分布集中、光谱吸收边蓝移，具有优异的光催化氧化活性、稳定性及抗湿性能，光催化降解溴代甲烷的表观量子效率比TiO〓催化剂提高了一个数量级，是一种有实际应用前景的高效光催化剂；由此提出了SO〓〓/TiO〓超强酸催化剂表面集团协同作用的超强酸中心模型，认为在SO〓〓/TiO〓超强酸催化剂表面，由SO〓〓诱导的相邻L酸中心和B酸中心组成了集团协同作用的超强酸中心，其集团协同作用显著地增强了催化剂表面酸性、增大了表面酸量及O〓吸附量、促进了光生电子和空穴的分离及界面电荷转移，具有可逆吸附水的性能，是SO〓〓/TiO〓超强酸催化剂具有优异的光催化氧化活性、很好的活性稳定性及抗湿性能的重要原因。

As one of the major equipments utilized in calcining active calcareousness, rotary kiln is applied broadly in China and it has the advantage of posing extensive material shape, good measuring adaptability and good mixture characteristic in inner kiln.

回转窑作为煅烧活性石灰的主要设备之一在我国有着广泛的用途，它具有广泛的物料形状、尺寸适应性和良好的窑内混合等优点。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。