查询词典 basic anhydride

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&O(来源：88AB57C论文网www.abclunwen.comne—pot Synthesis，由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4，4\'—二氨基二苯醚、3，4\'—二氨基二苯醚、2，2—双[4—(4—氨基苯氧基苯基]丙烷和2，2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

The process comprises the subsequent steps a through e: a reacting phthalic anhydride with fluorobenzene or a derivative thereof in appropriate reaction conditions; b over reducing the product obtained in step a at the ketone moiety; c reducing the product obtained in step b with sodium dihydro-bis (2- 15 methoxyethoxy) aluminate to the corresponding alcohol ; d chlorinat ing the alcohol obtained in step c ; e inserting CO into the product obtained in step d through an appropriate Pd-containing catalytic system.

该方法包括以下步骤a～e：a使邻苯二甲酸酐与氟苯或者其衍生物在适当的反应条件中反应；b完全还原步骤a中获得的产品的酮部分；c用二氢-二(2-甲氧基乙氧基)铝酸钠将步骤b中获得的产品还原成相应的醇；d对步骤c中获得的醇进行氯化；e通过适当的含Pd的催化剂体系，将CO插入到步骤d中获得的产品中。

The presence ofelectron donor(methoxy or methylenedioxy group) and electronacceptor anhydride group） moieties on phenyl fulgide derivativesleads to an intramolecular charge transfer upon exication that results ina solvatochromic effect.

可将苯基俘精酸酐视为由给电子基和得电子基两部分组成，分子内的电荷转移是造成正溶剂效应的主要原因。

The volume ratio of furaldehyde to acetic anhydride is 1∶2; the mole ratio of furaldehyde with anhydrous potassium carbonate is 1.00∶0.54. The best phase transfer catalyst is PEG1000, the mass ratio of PEG1000 with furaldehyde is 4.3%, the reaction time is 11 min, the reaction power of microwave is 260 W. The yield ofα-furanacrylicacid is up to 72.3% under these reaction conditions.

研究结果表明：在微波辐射功率为260 W、微波反应时间为11 min、以聚乙二醇1 000(PEG1000)为相转移催化剂，糠醛与乙酐的体积比为1∶2，糠醛与无水碳酸钾的量比为1.00∶0.55时，α-呋喃丙烯酸的产率为72.3%。

Then the fiber was transferred to a 4 mL vial which was filled with 100 μL of trifluoroacetic anhydride and stood 30 sec for headspace extraction. Afterward the fiber was transferred again to another blank 4 mL vial and stood 10 min for on-fiber derivatization before the analysis with GC/MS. The absorption-time profiles for both furoic acid and creatinine were examined.

有关尿中肌酸酐的量测，首先亦使用65μm PDMS/DVB纤维，在电磁搅拌转速1200rpm下以直接样本接触方式吸附60秒后，将已吸附肌酸酐的纤维挪至装有100μL无水三氟醋酸的4mL样本瓶中顶空吸附30 sec，再将纤维挪至另一个空白的样本瓶并静置10min（以利衍生物trifluoroacetamide的生成），最后再以气相层析质谱仪进行分析。

Diethyl glutarate was synthesized using glutaric anhydride and ethanol, which were separated from dicarboxylic acid, as raw material, heteropoly acid as catalyst.

以从二羧酸中分离出的戊二酸酐和乙醇为原料，用杂多酸为催化剂，合成了戊二酸二乙酯。

The diisoamyl glutarate in catalysis of silicotungsticacid was preparated by esterification of isoamyl alcohol and glutaric anhydride seperated from dicarboxylic acid.

用硅钨杂多酸为催化剂，以从二羧酸中分离出的戊二酸酐和异戊醇为原料合成了戊二酸二异戊酯。

Coupling ML-PLLA/GA and glutamic acid capped ML-PLLA-GC were prepared by modifying with Glutaric anhydride and L-Glutamic acid, respectively.

借助IR、~1HNMR、UV、DSC、TG等分析手段对材料进行了表征，并考察了戊二酸酐和L-谷氨酸对甘露糖醇-聚乳酸性能的影响，实验结果表明：以。

Tert-Butyldimethylsilyloxy) glutaric anhydride, as an important drug intermediate, is synthesized from citric acid by decarboxylation, reduction, hydroxyl protection, esterolysis, cyclization, with the total yield of 30.3%.

介绍了以柠檬酸为起始原料合成3-戊二酸酐的方法。该路线经脱羧反应、加氢还原、羟基保护、酯水解和再闭环，以总收率为30.3%得到目的产物。

The first and second generation of dendritic polyesters have been prepared by divergent synthetic ways using trimethylopropame as core and o-phthalic anhydride, glycidol as branched units.

以三羟甲基丙烷为核，邻苯二甲酸酐，环氧丙醇为支化结构单元，合成了第一及第二代树枝状聚酯。

There had been a moment during the breakfast meeting, though, after the backslapping and the small talk and when all of us were seated, with Vice President Cheney eating his eggs Benedict impassively and Karl Rove at the far end of the table discreetly checking his BlackBerry, that I witnessed a different side of the man.

那次早餐会期间，在表示过关心和寒暄以后，我们所有人坐了下来，我注意观察了一下，副总统切尼面无表情地吃着班尼迪克蛋（Eggs benedict，源自美国，以英式松饼、火腿、水煮蛋以及荷兰酱组合而成），卡尔。罗夫在餐桌的远端谨慎地经常查看他的黑莓手机，我目睹了他所不为人知的一面。

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