查询词典 basic anhydride

The kinetics on the hydrogenation of succinic anhydride to γbutyrolactone has been studied.

研究了琥珀酸酐加氢生成γ-丁内酯的反应动力学。

The effects of reaction conditions on the catalytic activity have been examined and a more than 95% yield of γ-butyrolactone obtained. Moreover, the above results are comparable with the catalytic activity of the same catalyst for hydrogenation of maleic anhydride.

结果表明，Cu/ZnO/Al2O3催化剂不但具有良好的顺酐加氢活性，而且在较温和的反应条件下对于1，4-丁二醇脱氢同样具有良好的催化活性，γ-丁内酯的收率可达95%以上。

The catalyst prepared by coprecipitation-impregnation has good catalytic performance of maleic anhydride hydrogenation to γ-butyrolactone.

共沉淀-浸渍法制备的20％CuO-20％SnO〓/Al〓O〓催化剂具有较好的顺酐加氢制γ-丁内酯活性，在280℃，顺酐转化率为94.4％，γ-丁内酯选择性为100.0％。

Over 5.4％CuO-10.8％NiO/TiO〓-Al〓O〓 catalyst, about 100％ selectivity to γ-butyrolactone at 100％ conversion of maleic anhydride was obtained at 200-270℃.

如使用5.4％CuO-10.8％NiO/TiO〓-Al〓O〓催化剂，在200-270℃，顺酐完全转化，γ-丁内酯选择性约为100％。

Through repairing the fixed bed calandria reactor during the molten salt leakage test in 2×104 t/a cis-butenedioic anhydride unit in Lanzhou Petroleum and Chemical Corporation,a pack of reasonable,practical and feasible technologic means was found to confirm the leakage points caused by molten salt and to repair it in reactor.

通过对兰州石油化工公司2×104t/a顺酐装置中的固定床列管式反应器熔盐渗漏的返修，摸索出一套实用、合理可行的熔盐渗漏漏点确认以及返修的工艺方法，可为类似反应器的制造提供一定的借鉴。

Compared with the Epoxy resorcinol-formaldehyde resin pretreatment system and Maleic anhydride pretreatment system developed by Xusigui, the 40% carbolated styrene-butadiene latex system can keep the composite"s properties and reduce the cost of pretreatment and simplify the pretreatment technology; especially to the HST 2073 latex system, the composite"s mechanics properties are improved greatly. Secondly, the composite"s comprehensive properties and interface performance are improved by reinforced with short fiber grafted with rubber in the surface. Thirdly, to simplify the production technology of composite, we add TKM-M and RF-90 as adhesive agent to the composite blended in an internal mixer, so as to the composite can be used to industry widely, then the effect of the amount adhesive agent on the composite"s properties and interface adhesive performance was studied, from the experiments the optimum amount of adhesive agent was deduced.

其中采用特软羧基丁苯胶乳预处理短纤维的方案，降低了预处理成本，相对许泗贵的低分子环氧和马来酸酐体系来说，预处理工艺大大简化了，而材料的力学性能保持良好，尤其是 HST 2073A 胶乳预处理体系，力学性能有较大幅度的提高；第二，通过对尼龙短纤维表面进行接枝橡胶分子链预处理，改善了复合材料的界面粘合性能，复合材料的综合性能也得到了相应的提高；第三，为了简化复合材料的生产工艺，使复合材料的应用得到工业化推广，我们选用TKM—M和RF—90长效增粘剂，直接加入短纤维橡胶复合材料中，采用密炼工艺，探讨了增粘剂的用量对复合材料界面粘合以及性能的影响，得出了增粘剂在复合材料中的最佳用量。

The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究，采用硫磺及乙酐复合催化剂，并且对氯化温度、氯化气氛、尾气回收等进行了过程优化，实现了乙酸氯化反应工艺条件的重大突破，使得氯乙酸的收率达到92.1%。

Kinetics of photo-chlorination of acetic acid to form monochloroacetic acid ;2. The mechanism for chlorinate acetic acid to monochloroacetic acid by using acetic anhydride or sulfur as catalysts respectively was studied.

通过对硫磺和乙酐催化氯化制备氯乙酸反应机理的分析研究，采用硫磺及乙酐复合催化剂，并且对氯化温度、氯化气氛、尾气回收等进行了过程优化，实现了乙酸氯化反应工艺条件的重大突破，使得氯乙酸的收率达到92。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2，6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐，然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基，而擅转乙酰，氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂，加氯。

Mono-cinnamyl maleate was prepared by esterification of maleic anhydride and cinnamyl alcohol of 1 mol:2 mol at 95 ℃ for 2～4 h.Then added isomeric catalyst and mono-cinnamyl fumarate was made by reacting at 90 ℃ for 4 h.After methanol (methanol:mono-cinnamyl fumarate = 6 mol:1 mol) was added,the mixture maintained at 90 ℃ for 4.0 h to synthesize CMF.

合成试验表明：以摩尔比为1：2的马来酸酐与肉桂醇在95 ℃醇解反应2～4 h后加入异构化催化剂，90 ℃转型反应4 h后，添加6倍摩尔质量的甲醇，在90 ℃恒温反应4 h，反丁烯二酸桂醇甲酯的合成产率较高。

There had been a moment during the breakfast meeting, though, after the backslapping and the small talk and when all of us were seated, with Vice President Cheney eating his eggs Benedict impassively and Karl Rove at the far end of the table discreetly checking his BlackBerry, that I witnessed a different side of the man.

那次早餐会期间，在表示过关心和寒暄以后，我们所有人坐了下来，我注意观察了一下，副总统切尼面无表情地吃着班尼迪克蛋（Eggs benedict，源自美国，以英式松饼、火腿、水煮蛋以及荷兰酱组合而成），卡尔。罗夫在餐桌的远端谨慎地经常查看他的黑莓手机，我目睹了他所不为人知的一面。

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