查询词典 aqueous

The invention relates to a continuous process for recovering caprolactam from aqueous caprolactam product, said aqueous caprolactam product comprising caprolactam, impurities, and water, said process comprising: adding alkali hydroxide to the aqueous caprolactam product, in an amount of not more than 100 mmol alkali hydroxide per kg of caprolactam; reacting at least part of the added alkali hydroxide to form alkali amino caproate, to obtain a caproate-enriched caprolactam product; and distilling the caproate-enriched caprolactam product at reduced pressure.

本发明涉及从含水己内酰胺产物中回收己内酰胺的连续方法，所述含水己内酰胺产物包括己内酰胺，杂质，和水，所述方法包括：以不超过100mmol碱金属氢氧化物/kg的己内酰胺的量将碱金属氢氧化物加入到含水己内酰胺产物中；让所添加的碱金属氢氧化物的至少一部分起反应，形成碱金属氨基己酸盐，以获得了富含己酸盐的己内酰胺产物；和减压蒸馏富含己酸盐的己内酰胺产物。

In this paper, the conventional isopiestic technique have been modified and extended to multicomponent unsaturated mixed solvent solutions, each containing two or three volatile solvents and two unsaturated solutes, and multicomponent saturated aqueous solutions, each containing two unsaturated solutes and one or two saturated solutes. Isopiestic measurements have been conducted systematically for the first time for two mixed solvent electrolyte solutions, two quaternary saturated aqueous solutions and three quinary saturated aqueous solutions and the experimental results have been compared with the ideal-like solution model.

本文将传统的等压技术，经过改进后，进一步应用于含有两种或三种挥发性溶剂和两种非饱和溶质的多元混合溶剂溶液以及含有一种或两种饱和溶质和两种非饱和溶质的多元饱和水溶液，首次系统地测定了两例混合溶剂电解质溶液、两例四元饱和水溶液和三例五元饱和水溶液的等压平衡，并将实验结果与类理想溶液模型进行了比较。

Suitable cleaning methods known in the art include rinsing in organic solvent, rinsing with aqueous detergent solution, mechanical abrasion such as sand-blasting, micro-etching with aqueous acids (eg HCl and H 2 SO 4 ) and aqueous oxidative cleaning with, for example, persulphate or perborate.

适当的清洗在艺术已知的方法包括在有机溶剂，与水清洗剂溶液冲洗，机械磨损，如喷砂，微蚀刻与水酸（如盐酸和H 2 SO 4计）和水的氧化清洗，例如，，过硫酸钾或过硼酸盐。

The phase diagrams of PEG/phosphate aqueous two-phase systems and the partition properties of BSA in the systems The PEG/phosphate aqueous two-phase system was regarded as the research object, the contents of phosphate and the polyethylene glycol in the system were measured by weighting and freeze-drying method respectively. Two diagrams were successfully drawn, and the characteristics such as binodal curves, tie lines and lever rule of the phase diagrams of the aqueous two-phase systems were described, as well as the achieved phase diagrams were qualitative analyzed with thermodynamics.

本论文以聚乙二醇／磷酸盐双水相系统相图和相分离过程及牛血清清蛋白在双水相系统中的分配特性为研究基础，从探讨超声波对双水相系统组成物质磷酸盐和PEG溶液的作用机理入手，建立了静态环境中双水相萃取过程的相分离数学模型，揭示了超声波对双水相系统组成和溶质分配效率影响的规律。

With the self-emulsifying aqueous polyurethane containing polymeric double bond in the lateral chain acted as macromolecular emulsor and reactant for acrylate monomer polymerization, controlling the reaction amount of polymeric double bond so that adjusting the chemical bond linkage degree between polyurethane and acrylate, core-shell type interpenetrating polymer network structural aqueous acrylate polyurethane hybrid dispersion was synthesized, which is now a new type molecular composite technology for aqueous polyurethane.

利用侧链含可聚双键的自乳化聚氨酯水分散体作为丙烯酸酯单体聚合反应的高分子乳化剂和反应物，通过控制聚氨酯水分散体侧链上参与共聚的双键数目，调节聚氨酯和丙烯酸酯的化学键合程度，制备得到核壳型互穿网络结构丙烯酸聚氨酯杂合水分散体是一种新颖的复合改性技术。

Through designing of composition and structure of the bioactive graded coating,innerstress and its distribution in the coating were analyzed and calculated, the resultsshowed that when composition distribution coefficient n was 1.5, a reasonable stressdistribution could be got, that was at the beginning of deposition the suspension containingrichly BG granules was used so that a rich BG granules layer, a good transitional layerbetween BG layer at the bottom and the coating could be obtained at the titanium alloy side,the bottom of the coating; the stress value near the interface and surface and its character,pressure stress or tensile stress, were decided by the character of its composition itself.Changing composition distribution coefficient n could only change the variation tendency ofstress in the coating, but did not change the stress distribution rule in the coating. Thethinner the coating is, the sharper stress variation in the coating is, which does not mean thatthicker coating is better because the thicker the coating is, the little the permitteddeformation of coating is, so the coating thickness should be thinner, for example, about50μm for bending applications, but for applications only bearing pure shear stress, such asroot of tooth implant, the coating can be thicker little, for instance, about 80～100μm. The study on electrification characteristic and electrophoresis deposition of HAand BG granules in aqueous and non-aqueous solution system found that EPD almost didn'toccur in aqueous solution system. However, because HA granules take position charges inabsolute alcohol, a homogeneous EPD be carried out on the cathode titanium alloy slice, but taking negative charge in absolute alcohol the BG granules not be deposited on the cathode. A guided HA crystallizing, 100～300nm, on surface of the BG granules be realized by metathetical reaction, which cover BG granules with HA microcrystals and make the covered BG granules taking position charges in absolute alcohol, sequentially realize the EPCD of the BG and HA granules on the cathode, so it is feasible to make a titanium alloy/BG/HA bioactive graded coating by making use of EPCD technology. The corrosion experiment of rich boron bioglass coating and plasma spray coating showed that split phase, rich boron and rich silicon phase, occurred during its preparation. In basic medium the corrosion behavior of 〓 BG coating showed uniformity corrosion, the corrosion mostly occurred at rich boron phase area, therefore batch formula design of BGshould avoid the occurring of split phase. The corrosion appearance of plasma spray coatingappeared a non-uniform corrosion, mostly occurred at the edge of the laminated HA moltendrops, and emerged an accelerated corrosion tendency, which will easyly lead to corrosioncrackles extending to the interface and the happening of osmotic interfacial corrosion, thatmay be one of the major reasons leading to the coating cracking-off in the later period. Thetesting results of thermal expansion coefficient of 〓 and 〓BG showed the thermalexpansion coefficient of 〓 BG matched with that of titanium alloy better, and 〓 BG couldsinter with titanium alloy into densification enamel layer at low temperature (720℃).

将Ti6Al4V合金在1000℃下进行真空热处理会降低其力学性能，且合金内的V元素会向表面富集，因此，钛合金真空热处理和表面涂层的烧结温度不能过高，即应低于其相转变点；通过对生物活性梯度涂层的组成和结构的设计，分析和计算了梯度涂层内的应力大小和分布，结果表明：对于本研究，当成分分布系数n=1.5时，可以获得较合理的涂层力学性能，即在沉积开始时，采用富含BG颗粒的悬浮液，以便在钛合金侧获得同底层BG有良好过渡的富BG涂层；梯度涂层界面和表面的应力大小、性质由材料组成本身的性质决定，改变成分分布系数，只能改变涂层内应力变化的趋势；涂层的厚薄不影响涂层内的应力分布规律，但涂层越薄，涂层内的应力变化越快，但这并不意味着涂层越厚越好，因为涂层越厚，涂层允许的变形越小，对于应用于弯曲受力部位的涂层而言，涂层应薄一点为好(50μm)；而对于仅纯受剪切应力的部位，如牙根种植体，涂层可适当加厚(80～100μm)；通过对HA和BG颗粒在水溶液体系和非水溶液体系中的带电特性和电泳沉积的研究发现，它们在水溶液体系中很难发生电沉积；在无水乙醇溶液中，HA颗粒带正电，可在阴极钛合金片上发生均匀的电泳沉积，而BG颗粒则带负电荷；利用复分解反应法，可以制得100～300nm的HA，通过诱导HA在BG颗粒表面结晶，可对BG颗粒进行表面包覆，获得了被HA包覆的BG颗粒，改变了BG颗粒表面的带电特性，使BG和HA颗粒在无水乙醇中均带上正电荷，从而实现了HA和BG颗粒在阴极上的共沉积。

Raman spectrum of saturated aqueous solution of ammonium dimolybdate crystal was recorded, and compared with those of ammonium dimolybdate crystal , ammonium heptamolybdate crystal, saturated aqueous solution of ammonium heptamolybdate crystal and monomolybdate anion in aqueous solution respectively.

记录了常温下二钼酸铵晶体饱和水溶液的Raman光谱，并分别与二钼酸铵晶体、仲钼酸铵晶体、仲钼酸铵晶体饱和水溶液、水溶液状态下单钼酸根离子的Raman光谱进行了比较研究。

A set of apparatus for determining solid-liquid equilibrium data at atmospheric pressure has been established. The solubility of sebacic acid in water, 20% ethanol aqueous solution, 50% ethanol aqueous solution, 80% ethanol aqueous solution and ethanol were determined. Wilson equation, ideal thermodynamics equation and λh equation were applied to describe solid liquid equilibria data.

建立了一套常压固液平衡测定装置，测定了癸二酸在水、20％乙醇-水溶液、50％乙醇-水溶液、80％乙醇-水溶液、无水乙醇体系中的溶解度，并用Wilson方程、热力学简化方程和λh方程模型对实验数据进行关联。

Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.

本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基溴化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7／3、1／1和3／7时，前三个体系均形成水包油型分散，并有稳定的乳状液生成。

In order to research and evaluate the safety of food packaging of plasticizer Di-2-ethylhexyl phthalatein PVC film, the migration rate of DEHP from PVC film into water food simulants (distilled water, 65% aqueous ethanol, 20% aqueous ethanol, 4% aqueous acetic acid) was studied at 17, 30, 40, 50 and 60℃ by Gas Chromatography.

为了研究评判PVC膜中增塑剂邻苯二甲酸二异辛酯在食品包装中的安全性，采用气相色谱仪测试了几种水性溶剂（蒸馏水、65%乙醇、20%乙醇、4%乙酸）在不同温度（17℃、30℃、40℃、50℃、60℃）下对PVC膜中增塑剂DEHP的溶出率。

Cynanchum Lingtai apricot production in the average weight 65 grams, the brightly-colored fruit, juicy rich, sweet-sour taste, sweet from the nucleolus, when the late Qing Dynasty famous Shaanxi, Gansu provinces, the Qing imperial court Tongzhi tribute for years.

灵台生产的牛心杏平均单果重65克，果实色泽鲜艳，汁多味浓，甜酸适口，离核仁甜，清末时就驰名陕、甘两省，清同治年间曾为朝廷贡品。

Chenopodium album,Solanum nigrum, and Amaranthus retroflexus were very susceptible to the herbicides. Polygonum persicaria and Abutilon theophrasti were relatively less susceptible to the herbicides, and Lycopersicon esculentum was not susceptible to it. The relationship between reduction rates of weed biomass and PPM values of weed leaves 2,4, and 6 days after treatment was established.

供试的6种杂草对该混剂的敏感性存在显著差异：红心藜Chenopodium album、龙葵Solanum nigrum和反枝苋Amaranthus retroflexus对该混剂最敏感，ED90值分别为47.65、71.67和29.17g/hm2；春蓼Polygonum persicaria和苘麻Abutilon theophrasti敏感，ED90值分别为96.91、114.20g/hm2；而番茄不敏感。