查询词典 a column of water

Methods: from prepation of crude drug as start, study the technology of extract and defat with L9 (3~4) orthogonal test. With EtOH extraction and water sed, alkali washing, EtOAC extraction as main methods of eliminate dopant. Finally with alky AlzO3 chromatographic column, rich and gain anticancer active site. The maximum response was achieved at a 40 min extracting time with 10 times volume 90% EtOH added to the sample for the first time and 30 min for the second time. Adding 10 times water will produce precipitation; Place the precipitation into 6 times petroleum benzin to de-fat at 60℃.

云南红豆杉中抗癌活性物制备工艺研究方法：利用正交设计试验L9(3~4)确定原料药提取工艺为：10倍量90％乙醇提取两次，第一次40分钟，第二次30分钟；醇提液用10倍量水沉；沉淀加6倍量石油醚40℃脱脂；用1mol／L的NaOH溶液碱洗，除去酸性杂质；以碱性氧化铝柱，以环己烷／丙酮为洗脱溶剂，在环己烷-丙酮(6：4)段富集到所需活性部位，洗脱剂用量为3VB。

Attention to high titer cold agglutinin in infants with blood grouping and cross-matching the impact of high titer cold agglutinin with blood of the same type of sub-Suozhi mostly weak agglutination, agglutination disappeared after by the water bath to prove consistency of cross-matching of blood, it should be added do direct antiglobulin test or polybrene with micro-column method with blood or blood serum can be excluded may contain other irregular antibodies; subtypes with the same type of blood (including the weak antigens and antibodies with a weak blood) when irregularities for weak agglutination, but the 37℃ water bath does not disappear after the condensation to prove that cross-matching of blood mismatched for the blood transfusion taboo.

重视高效价冷凝集素对婴幼儿血型鉴定和交叉配血的影响，高效价冷凝集素所至同型配血不合多为弱凝集，经水浴后凝集消失，证明交叉配血相合，但应加做直接抗人球蛋白试验或凝聚胺配血或微柱法配血，可以排除血清中可能含有其他不规则抗体；亚型同型配血(包括弱抗原与弱抗体配血)不合时也为弱凝集，但37℃水浴后凝集不消失，证明交叉配血不相合，为输血禁忌。

Methods: Glipizide gliclazide glyburide glimepiride gliquidone repaglinide nateglinide pioglitazone rosiglitazone metformin phenformin and tolbutamide added in the blank ground samples were extracted with 80% methanol and were separated from an ACQUITY UPLC DBH C18 column with a gradient mobile phase of acetonitrile - 0.2 % formic acid water solution. A tandem quadrupole mass spectrometer equipped with electrospray ionization source was used in positive ion mode multiple reaction monitoring was performed to quantify above mentioned compounds.

被添加在中成药制剂及其包装物中的二甲双胍、苯乙双胍、罗格列酮、吡格列酮、格列吡嗫娶瑞格列奈、甲苯磺丁脲、格列齐特、格列苯脲、那格列奈、格列美脲、格列喹酮等西药成分用80%甲醇提取，以乙腈- 0.2%甲酸水溶液为流动相梯度洗脱，在ACQUITY UPLC DBH C18色谱柱上分离，串联四级杆质谱检测，MRM方式采集并定量。

The watermelons, the citrullus lamtus or the stems and leaves thereof are taken as raw materials, and the extracting process comprises the following steps: firstly, the raw materials are washed clean and broken to separate the watermelon peel from the watermelon pulp for respectively extracting juice; the two juices are mixed, and micro-filtration and ultra-filtration are carried out to remove insoluble substances and macromolecular substances; and then reverse osmosis and nano-filtration are carried out to obtain the filtrate; the pH value of the filtrate is regulated and then a macroporous strong acid cation exchange resin column is added; and then ammonia water is taken as an eluant for isocratic elution; the eluent obtained is decompressed, distilled, deaminized, discolored, condensed and crystallized to obtain a white crystalline product of the natural L-citrulline extracted from the watermelons.

本发明方法以西瓜、打瓜或者其茎叶为原料，其过程为：首先将原料清洗干净，破碎后将西瓜皮西瓜瓤分开，分别进行榨汁；所得汁液合并，经过微滤和超滤除去不容物和大分子物质；然后再经反渗透和纳滤过滤；透过液调节pH值后通入大孔型强酸性阳离子交换树脂柱；然后以氨水做洗脱剂进行等度洗脱；将洗脱液减压蒸馏脱氨，脱色，浓缩结晶，得到西瓜提取天然L-瓜氨酸白色结晶产品。

The high-performace liquid chromatographic method was developed for determination of Aloin and Isobarbaloin in rabbit blood. A HPLC system equipment, a Merk LiChrospher 100 RP-18e column with the mobile phase consisted of methanol-water (50:50) and UV detection wavelength at 359nm. The internal standard was 7-hydroxycoumarin and follow rate was 1.0ml/min.

并首先开发出在家兔体内血浆中二个指标成分之高效液相层析分析法，使用Merk LiChrospher 100 RP-18为层析管柱，移动相为甲醇与水（50：50），内部标准品为7-羟基香豆素，在检测波长359nm，流速1.0 ml/min下，分别定量血浆检品与进行确效性的评估。

Therelationship between the turbulent kinetic energy and its dissipation rate,whichis widely used to parameterize the dissipation rate in turbulence closure models,is found to hold well for both reversing and rotating flows,but with differentcoefficients.Microstructure profiling measurements at two comparative stations (a deepercentral basin and a local shelf break) in the stratified Yellow Sea are analyzed,with emphasis on tidal and internal-wave induced turbulence near the bottomand in the pyenocline.The water column has a distinct three-layer thermohaline structure,consisting of weakly stratified surface and bottom boundary layers anda narrow sharp pycnocline.Turbulence in the surface layer is controlled by thediurnal cycle of buoyancy flux and wind forcing at the sea surface.while thebottom stress induced by barotropic tidal eurrents dominates turbulence in thebottom boundary layer.The maximum level at which the tidally enhanced mixingcan affect generally depends on the magnitude of the tidal current,and it canbe up to 10-15 m in the Yellow Sea.This suggests that,in the deeper regionsof the shelf seas,turbulent dissipation and mixing are very weak at the levelsbetween the near-bottom tidally enhanced layer and the pycnocline.Therefore,these levels provide a significant bottle neck for the vertical exchanges.In theshallow regions,however,the tidally-induced turbulence can occupy the wholewater colum below the pycnocline.A quarter-diurnal periodicities of the turbulentdissipation rate and eddy diffusivity are found at different heights with evidenttime lag.In the relatively flat central basin,the pycnocline is essentially non-turbulent and internal-wave activity is very weak.Therefore,vertical fluxes acrossthe pycnocline decreased to molecular levels.In contrast,internal waves of variousperiods can be always found near the local shelf break.

对强层化季节黄海两对比性站位(分别位于中央海盆区与局地陆坡区)处层化、内波以及湍流混合特征的研究结果表明：1、强层化季节的陆架海水体一般呈现显著的三层热盐结构，在水体近乎混合均匀的上混合层与潮流底边界层之间为强跃层；2、近表层水体的湍流混合强度主要由海表浮力通量的日变化与海表风强迫控制，而在潮流底边界层内，潮混合是水体热量、物质、动量与能量垂直交换的主要机制；3、潮混合影响的深度由潮流大小决定，在黄海，一般可达10-15 m，因此，在水深较深的区域，在跃层与潮混合所至深度范围的上界之间存在湍流混合非常弱的区域，这显著抑制水体内物质的垂直通量，为物质垂直交换的瓶颈，而在水深较浅的区域，潮混合影响范围可至跃层底部，因此物质在跃层以下整个水体中混合非常均匀，当跃层内间歇性强混合发生时，可以产生显著的跨跃层物质输运；4、近底潮致强湍流耗散缓慢地向上传播，底上不同深度处垂直湍扩散系数也具有显著的位相差异，且二者均随时间呈现四分之一周日周期的变化；5、在地形较为平坦的中央海盆区，内波活动非常微弱，因此跃层内湍流混合非常弱，垂直扩散系数为分子扩散水平，跨跃层物质通量受到显著抑制，而在地形变化较为显著的局地陆坡区，内波活动非常活跃，除内潮的影响外，高频内波与内孤立波的影响也很显著，因此跃层内存在很强的间歇性强混合，内孤立波存在的区域，水体湍流混合显著增强。

The organic layer was evaporated and the residue was redissolved by mobile phase.The concentrations of propofol and lidocaine were assayed on a hypersil BDS C18 column with a mobile phase consisting of acetonitrile-methanol-water（10∶60∶30）（including 0.14%n-butyamine 0.1%acetic acid）at a flow rate of 1 mL*min-1 and detected at 220 nm during 1～7 min and at 273 nm during 7～16 min.

氮气吹干有机层，残留物用流动相重新溶解后，用Hypersil BDS C18柱分析，流动相为乙腈-甲醇-水(10∶60∶30)，内含正丁胺0.14%和冰醋酸0.1%，流速为1 mL*min-1，检测波长：1～7 min用220 nm，7～16 min用273 nm。

Methods The sample was separated with a C18 column (150mm×4.6mm, 5μm) at 30℃ with the mobile phase of methanol and water (74:26); A fluorescence detector was used (λex=230nm λem=460nm); The floss rate was 1mlmin^(-1) Results The retention time of aesculin was(3.620±0.05)min; A good linear relationship of aesculin in the plasma samples at the concentration between 0.1mgL^(-1) and 100mgL^(-1) was observed (r=0.997); The mean absolute recovery was 74.0%~82.6% and the lowest detective limit was 0.05ng; Both the intra-day and inter-day precisions were less than 9.0%.

以C18柱(150mm×4.6mm，5μm)分离；流动相为甲醇－水(76：24)；流速：1mlmin^(-1)；柱温：30℃；荧光检测器，激发波长230nm，发射波长460nm：结果秦皮甲素的保留时间为(3.620±0.05)min；血药浓度在0.1~100mgL^(-1)范围内线关系良好(r=0.997)；绝对回收率为74.0%-82.6%，日内、日间精密度均＜9.0%，最低检测限为0.05ng。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后，用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质，过滤，用次氯酸钠将样品溶液中的甜蜜素转化为N，N-二氯环己胺经正己烷萃取后，在phenomenex Gemini-C18柱上，以乙腈－水(7+3)或甲醇－水(8+2)为流动相进行分离，HPLC-UV检测器在314 nm测定，外标法定量。

The regenerating method invention thereof comprises the following steps: firstly, the treating tea after absorbing the heavy metal ions is washed by water to the neutral after HCL solution is used for eluting; and secondly, the NaOH solution of a certain proportion is used for flowing through the column, and then water is used for washing to the neutral.

其再生方法包括：(1)将已吸附了重金属离子的处理茶，用HCL溶液洗脱后用水洗至中性；(2)用NaOH溶液的比例过柱，再用水洗至中性。

Methods: Five patients with parkinsonism or dystonia were assigned to general anesthesia using an modified endotracheal tube.

本实验依照人体实验之相关规定进行，五位患有帕金森氏症或肌张力异常的病人接受神经立体定位手术。

If you can benefit from this book, it is our honour.

如果您能从本书获益，这将是我们的荣幸。