查询词典 X-ray diffraction

In this paper, a turbostratic CN precursor was prepared by means of pyrolysis of melamine, then it was treated by high temperature and high pressure. The pyrolysis process of melamine, mechanism of hydrogen elimination and the effect of catalysts on pyrolysis of melamine were studied. The crystal structures, bonding states and chemical compositions of CN precursor obtained by pyrolyzing melamine are analyzed by X ray diffraction, burning spectrum, scanning elecron microscope and Fourier transform infrared Spectroscopy.

本文采用三聚氰胺热解法制备了乱层石墨结构的碳氮前驱物并进行了探索性的高温高压实验；研究了三聚氰胺热解的工艺、去氢机理以及催化剂对三聚氰胺热解过程的影响规律；借助 X 射线衍射、燃烧谱、透射电镜和红外光谱等手段，对获得的碳氮前驱物进行了成分、晶体结构、价键结构的分析。

The crystal structures of the two polymorphs are so similar that they can hardly be distinguished by usual polycrystalline X-ray diffraction methods.

后者是一种亚稳相。这两种多型体的结构非常相似，用通常的多晶衍射方法难以区分。

The structural changes in the fibres during drawing process were examined by wide-angle X-ray diffraction,polarising optical microscopy and density gradient column.

利用广角X-射线衍射试验、偏光显微镜观察等方法研究了拉伸过程中纤维结构的变化。

Solid complexes of rare earth picrates with the ligand 2,6-bis(benzimidazol-2-yl)pyridine have been synthesized and characterized by elemental analysis, IR and electronic spectra. The crystal and molecular structures of the complex [CeL22]·(CH3OH)3 have been determined by single crystal X-ray diffraction.

合成了稀土苦味酸盐与配体2，6-二(2-苯并咪唑基)吡啶的配合物，通过元素分析、红外光谱及电子光谱对配体及配合物进行了表征，并用X射线单晶衍射测定了配合物[CeL22]·(CH3OH)3的晶体结构。

We tried to prepare Li2S-SiS2 based thionitride glasses by the solid synthesize method, where Li3N was used as a nitrogen source. This paper reports the preparations, electrical, and electrochemical properties of Li2S-SiS2-Li3N glasses. Phase identification was carried out by X-ray diffraction .Ionic conductivity of the pelletized solid electrolytes was investigated through AC impedance.

本文以无机固体电解质为研究对象，利用固相合成方法制备了以Li2S-SiS2为基体掺杂Li3N的三元体系Li2S-SiS2-Li3N；通过XRD对样品进行了物相分析；采用交流阻抗技术测量了电解质样片的阻抗谱并计算了离子电导率和活化能；并利用循环伏安法估测了电解质样片的电化学稳定性；用固体电解质组装成模拟电池进行充放电测试。

By using the results from systemical petrography, X-ray powder diffraction, and EPMA analyses on the run products from experimental simulaion under constant temperature and pressure, we have explored the paragenesis for the pelites suffering metamorphic dehydration under high pressure condition, the process and mechanism for these metamorphic dehydration, and the relation between the components for garnets, one of the major phases in the paragenesis, and the experimental conditions including pressure, temperature, and chemical compositon in a system.

由恒温、恒压实验产物系统的岩相学、X射线粉晶衍射和电子探针分析，揭示了天然泥质岩发生高压变质脱水作用后的矿物相组合，确定了泥质岩高压变质脱水作用的过程和机理，以及主要矿物相石榴子石的组成与压力、温度和体系化学组成的关系。

This study presented the effect of multi-modification on microstructure and properties of high manganese steel by means of microstructure observation, X-ray diffraction line profile analysis and properties testing.

通过显微组织观察，X射线线形分析和性能测试，研究了多元变质处理对高锰钢微观结构和性能的影响。

X-ray diffraction. The microstructure and cross section microhardness of nitrided layers were observed and analyzed by optical microscope and microhardness tester.

在一定的工件表面温度下，粒子表面物理吸附的氮原子发生脱附，脱附下来的活性氮原子渗入基体的内部，形成渗氮层。

Zinc sulfide nanoparticles with different sizes were synthesized by a unique precipitate dissolution method using zinc alkyl xanthate and sodium sulfide as zinc and sulfur sources, respectively. The samples synthesized were characterized by low temperature nitrogen adsorption and desorption, Transmission Electron Microscope, powder X-ray Diffraction and Fourier Transform Infrared Spectroscopy techniques.

以烷基黄原酸锌和硫化钠分别为锌源和硫源，采用烷基黄原酸锌沉淀溶解法制备了粒度可调、粒径分布比较窄的面心硫化锌纳米粒子，利用比表面积测定、透射电镜、粉末X射线衍射、傅里叶转换红外光谱等方法对合成的硫化锌纳米粒子进行了表征。

Nanostructured ZnO films with grain size of 28～35 nm have been prepared on quartz glass substrates by pulse laser ablation of Zn target in oxygen atmosphere. The structural and optical properties of the films were studied. ZnO thin films with typical c-axis (002) orientation were successfully deposited at a range of 100～250 ℃. The results obtained by X-ray diffraction and photoluminescence measurements show that the strong UV emission centering is about 378～385 nm and deep-level emission centering about 518～558 nm in the room temperature PL spectra of the ZnO films.

利用脉冲激光沉积法在氧气氛中烧蚀锌靶制备了纳米晶氧化锌薄膜，衬底为石英玻璃，晶粒尺寸约为28～35 nm.X射线衍射结果和光致发光光谱的测量表明，当衬底温度在100～250 ℃范围内时，所获得的ZnO薄膜具有c轴的择优取向，所有样品的强紫外发射中心均在378～385 nm范围内，深能级发射中心约518～558 nm，衬底温度为200 ℃时，得到了单一的紫外光发射。

The role of the environment is very important.

的作用，环境是非常重要的。

At that time, the High Court of England and Wales Court of Queen's Bench president of William Murray, Lord Mansfield in June 22, 1772 ruling:"No matter then there is the inconvenience, but there must be a decision, I can not say that this case under the law in England are permitted or authorized; are so black should be released."

当时的英格兰及威尔士高等法院王座法庭院长William Murray， Lord Mansfield于1772年6月22日宣判：「无论有那麽不便，但总要有个决定，我不能说这件案在英格兰法律之下是准许或认可；所以黑人是应该被释放。