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The experimental results showed that when AcO-or other anion s were added to a solution consisting of 1,5-(di-benzaldehyde) dithiocarbohydrazone and Hg2+(at a ratio of 1∶2),a hypsochromic shift took place on the maximum ultraviolet absorption peak of the ligand.

设计合成了配体1,5-二双缩二氨基硫脲及其金属配合物,探讨了不同金属阳离子对1,5-二双缩二氨基硫脲紫外吸收光谱的影响,并将标题化合物应用于阴离子识别。

Marines are normally armed with C-14 Impaler gauss rifles that fire 8mm metal "spikes" at hypersonic speeds. Basic rounds are designed to provide maximum penetration against all armor types, but a number of specialized rounds exist.

机枪并通常装备的C-14穿刺高斯机枪能以超光速发射8MM的金属弹,基本这些金属弹的都是经过设计来最大程度上穿刺所有的护甲类型,但是也有一些其他特殊的子弹。

The main content include:(1) Considering the serious problem of metal structure of the gantry cranes and the technology actual status and trend of fault diagnose nowadays, this papers analyze seriousness of the existing fault and impendency of maintenance.

本论文的主要内容包括:(1)针对门座起重机金属结构故障十分突出的问题,综合分析了门座起重机金属结构故障存在的严重性及维修的紧迫性。

There were five kinds of NpCpTiCl〓, in which Np was pyrolyl , indolyl ; 7-azoindolyl , indazolyl , and benzimidazolyl respectively. All of them were prepared by the reactions of CpTiCl〓 with the anions of the relevant ligands, and characterized by elemental analysis, IR, or NMR.

此外,半茂体系的催化活性都随铝/钛比的增加呈上升而后衰减型,当Al/Ti比为500左右时活性达到最高,这个值远低于茂金属催化剂活性达最高时的Al/Ti比,即茂金属配合物比半茂配合物需要更多的MAO来活化,并稳定形成的活性中心。

On base of analysis to simulation result, it was point out the main cause making dissimilar metal"s bonding so difficult was metal"s inharmonic plastic deformation. The distribution and changement of stress and strain on interface and in workpieces were analyzed.Making use of experiment and simulation result, main factors that influence welding property of cold pressure welding were discussed.

通过对模拟结果的分析,说明了异种金属冷压焊较同种金属冷压焊困难的原因主要是界面处两种材料的径向和轴向的不协调塑性变形;直观地显示了冷压焊过程中工件内部及界面处的应力应变分布及变化情况。

Intercalation of metal complexes into the interlamellar space of clay is an excellent method for homogeneous catalyst heterogenization .

粘土的可膨胀的二维空间有助于将催化活性的金属络合物用阳离子交换法和配位体交换法插入到粘土层间,因而易于制得粘土层间金属络合物催化剂,这是匀相催化剂多相化的一种好方法。

The experimental results indicated that the longer the po uring intervallic time of the two kinds of molten metal and the higher the heigh t of the molten iron to pour into the tip of dipper teeth , the narrower its tran sitional zone will be, on the contrary, the wider its transitional zone will be.

用不同粘度的流体通过水力模拟的方法近似地描述了双金属斗齿过渡区的混合状态。试验结果表明:两种液体浇注的间隔时间越长,先浇入的铁液液面越高,过渡区越窄;反之,过渡区越宽。生产中为了保证过渡区双金属的结合质量,应控制较高的铁液液面高度及一定的双液间隔时间

Except for control group, rats in the other groups were intratracheally administered with bleomycin. Animals in pulmonary fibrosis model groups were sacrificed on day 3, 7, 14, 28 and 56. The sections of the right lung were stained by HE, Masson and sirius red. The left lung was weighed and its hydroxyproline content was assayed. The mRNAs of TGF-β1, MMP-9 and TIMP-1 in the lung homogenate were measured by semi-quantitative RT-PCR.

除N组外,其余各组采用气管内注入BLM致大鼠肺纤维化模型,分别于3、7、14、28、56d处死各组大鼠,右肺行苏木精-依红、Masson胶原及天狼猩红染色,测定左肺经脯氨酸的含量RT-PCR法半定量测定转化生长因子-1(TGF-β1)、基质金属蛋白酶-9(MMP-9)和基质金属蛋白酶组织抑制物-1(nMP-1)mRNA在肺内的表达。

A fungus CTB430-1 with resistance to copper and zinc was isolated from soil at a copper and Zinc Tailing of Linxiang in Yueyang city, Hunan province. The fungus was identified by analyzing the morphology and measuring the ITS sequence. The effects of pH, initial concentration, co-ions on the growth of CTB430-1 and bioaccumulation of Cu2+ and Zn2+ were studied. The protein and glutathione in the cells were determined by using the coomassie brilliant blue method and iodometric method, respectively.

摘 要:从湖南省岳阳市临湘铜锌尾砂坝土壤内分离、纯化得到1株抗铜和锌的菌株CTB430-1,分析该菌株形态和测定菌株ITS基因序列鉴定菌种,研究不同pH值、金属离子初始浓度和金属离子共存对菌体生长量和富集重金属的影响;分别采用考马斯亮兰法和碘量法测定菌体内可溶性蛋白和还原性谷胱甘肽含量。

Methods A wet hip joint's sample from corpse was scaned by CT and all images of every cross-section hip joint's layer was obtained, and an hip joint's model was contructed with Unigraphics NX 2.0 and Solid Works 2006 SP 0.0 software. The models were assembled when simulated total hip arthroplasty after total hip joint prosthetic and ischiofemoral ligament model had been constructured. Analysis was done on von Mises stress distribution and amount of total hip component when simulated seated leg-crossing manuver. The bone and metal components were meshed as rigid bodies, composed of three-dimensional, all-quadrilateral rigid body elements, and hip joint capsule ligament was fully three-dimensional, hexahedral continuum elements representations. Results The current form of this ischiofemoral ligament's reconstruction finite element model provided for multi-body contact, large displacement interfacial sliding, large deformation capsule ligament representation, and clearly reflected the real ischiofemoral ligansent's anatomy and biomechanical behavior. The maximum on Mises stresses at the joint interface was more than that fur an otherwise identical hardware-only construct.

选择成人尸体髋关节行CT成像得到髋关节每层横截面图像,提取边界坐标,利用有限元分析软件Unigraphics NX 2.0和Solid-Works 2006 SP0.0构建出髋关节三维有限元模型及人工髋关节假体,并模拟全髋置换术进行装配,将坐股韧带按其术中重建位置进行构建骨骼与金属模型采用三维十节点四面体实体单元进行网格划分,关节囊六面体连接单元划分,模拟坐位腿交叉动作载荷获取假体撞击过程的角活动度和相应的von Mises应力分布情况结果所构建的多体连接、大界面划移、大变形的坐股韧带重建有限元模型,客观反映坐股韧带真实解剖形态及生物力学行为,增加坐股韧带重建的模型其关节面的最大主应力值大于仅有金属的模型。

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If we can prove the independence of an axiomatic system, then we can guarantee the conciseness of this system, ie.

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