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This paper mainly introduces experimental methods and basic principle about gelled acid reaction kinetics. Through the reaction kinetics experiment of straight acid and gelled acid, the reaction parameters of acid - rock reaction and kinetic equation in different conditions were achieved.

介绍了胶凝反应动力学的试验方法及基本原理,进行了普通和胶凝与灰岩的反应动力学试验,得到不同条件下的岩反应动力学参数及反应动力学方程,对优化碳盐岩油藏压设计有一定的指导作用。

Acidifier supplementation I could improve significantly average daily gain,feed conversion ratio,apparent digestibility. Acidifier supplementation II could reduce diarrhea rate. And the reason needed to be research further.

化剂产品Ⅰ提高羔羊的增重速度、饲料转化效率和饲料主要营养物质表观消化率的作用效果均优于化剂产品Ⅱ,但化剂产品Ⅱ降低腹泻率的效果优于化剂产品Ⅰ,这可能与不同产品中的种类、组成不同有关,其机理尚有待进一步研究。

We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯基]-金合欢-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

The levels of all identified metabolites are notably higher at day 11 and day 14. At day 21, the amounts of Asn and His were decreased, but Val, lactate, Ala, malate, succinate, GABA, choline,β-glucose, fructose, allantoid, Phe and formate were all increased. Enteric bacteria must overcome the acid environments in host organs to colonize the host.

结果表明:根瘤菌处理5d后苹果含量显著增加,7d时丙氨浓度降低而异亮氨、苹果、琥珀、GABA、胆碱、磷胆碱、β-葡萄糖、延胡索、组氨、苯丙氨、色氨含量显著增加。11d和14d的差别极为显著,所有已鉴定代谢物的含量都大大增高。

Principal cmponent analysis was used for 34 aroma components,and the relsult showed that the 34 aroma components could be represented asssumably by butanoic acid methylester, butanoic acid ethylester, propylalcohol, butylalcohol, 2,3-butanediol, decanoic acid ethylester, ethyl 4-hydroxybutanoate, eugenol, palmitic acid ethylester, 9-Octadeceroic acid ethylester.

对定量的34种香气物质进行主成分分析,结果表明:由丁甲酯,丁乙酯,丙醇,丁醇,2,3-丁二醇,癸乙酯,4-羟基丁乙酯,丁子香酚,棕榈乙酯,油乙酯基本可以代表本试验所定量出的34种香气物质呈现出的香气物质所构成的风味特征。

The results showed that new-type solid ferric potassium alum was a good catalyst for the synthesis of ethyl decanoate and the optimum conditions were as follows: molar ratio of acid to alcohol was 1∶2, the use level of catalyst was 0.6 g/0.05 mol capric acid, water-taking reagent benzene was...

结果表明,新型固体铁钾矾是合成癸乙酯的良好催化剂,在醇物质的量比为1∶2,催化剂用量为0.6g(0.05mol癸),带水剂苯为15mL,反应时间为2.5h的条件下,癸乙酯的酯化率可达98%。

In the present paper,the solid state synthesis and luminescent properties of RE activated tungstates are introduced.

本文从单钨盐、混合碱土金属钨盐、氟钨盐、同多钨盐、杂多钨盐等方面综述了掺杂稀土离子钨盐的固相合成及发光特性研究进展。

The luminescent propetties of RE activated tungstates are dealt with in respect to mixed alkali earth metal tungstates,fluorotungstates,isopolytungstates,heteropoly tungstates.

本文从单钨盐、混合二价金属钨盐、卤钨盐、同多钨盐、杂多钨盐等方面综述了掺杂稀土离子钨盐的发光特性研究情况。

Effects of microwave power, reaction time, reaction temperature, solvent etc. on reaction were studied by a single factor tests. The results show that maleic acid is more active than fumaric acid; the introduction of methyl group on the double bond can weak the reactivity of the Michael addition reaction; the ester base is more propitious to complete the Michael addition reaction than the nitrile base.

为研究微波下迈克尔反应的规律,本文采用单模聚焦微波有机合成仪,通过对顺丁烯二、反丁烯二和氨水合成DL-天冬氨、顺式3-甲基丁烯二和氨水合成3-甲基天冬氨、丙烯甲酯和氨水合成β-丙氨、丙烯腈和氨水合成β-氨基丙腈等五个反应对迈克尔加成反应进行了研究。

As one of the most important osmoregulation actor, firstly,Proline plays a keyrole in the osmotic potential adjustment in plant cells. Secondly, Proline can preventNaCl from damaging the structure of biomacromolecule in cells. Thirdly, the highdissolubility and non-rejection capability of Proline can enlarge the solution volumnof the cell, so the concentration of salt will be diminished in cytoplasm and the saltstress will be relieved. Forthly, the accumulation of Proline could prevent thedehydrolysis from sap cavity in cytoplasm. Fifthly, the synthesis of plant chlorophyllwill be diminished under the salt stress, but the Proline can provide request ofchlorophyll synthesis.

脯氨作为渗透调节剂对植物体细胞渗透势的变化起重要作用:一,在盐胁迫下,脯氨在植物体内是一种重要的渗透调节剂,它是一些高等植物和绿藻抗盐和抗旱的主要渗透剂之一;二,脯氨可以保护细胞中的生物大分子的结构,使之不被NaCl破坏,并能维持其完整的水合范围;三,脯氨的高度溶解性以及其对植物各种酶活性不抑制性,可以扩大细胞的溶解容积,从而降低细胞质液中盐的浓度,减轻盐的胁迫作用;四,细胞质中积累的大量脯氨可以防止液泡对细胞质的脱水作用;五,在盐胁迫下,植物叶绿素的合成受到抑制,叶绿素的合成需要脯氨

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