蒸馏物

The watermelons, the citrullus lamtus or the stems and leaves thereof are taken as raw materials, and the extracting process comprises the following steps: firstly, the raw materials are washed clean and broken to separate the watermelon peel from the watermelon pulp for respectively extracting juice; the two juices are mixed, and micro-filtration and ultra-filtration are carried out to remove insoluble substances and macromolecular substances; and then reverse osmosis and nano-filtration are carried out to obtain the filtrate; the pH value of the filtrate is regulated and then a macroporous strong acid cation exchange resin column is added; and then ammonia water is taken as an eluant for isocratic elution; the eluent obtained is decompressed, distilled, deaminized, discolored, condensed and crystallized to obtain a white crystalline product of the natural L-citrulline extracted from the watermelons.

本发明方法以西瓜、打瓜或者其茎叶为原料，其过程为：首先将原料清洗干净，破碎后将西瓜皮西瓜瓤分开，分别进行榨汁；所得汁液合并，经过微滤和超滤除去不容物和大分子物质；然后再经反渗透和纳滤过滤；透过液调节pH值后通入大孔型强酸性阳离子交换树脂柱；然后以氨水做洗脱剂进行等度洗脱；将洗脱液减压蒸馏脱氨，脱色，浓缩结晶，得到西瓜提取天然L-瓜氨酸白色结晶产品。

Finally, the effect of the complete recycling use of distilled effluent on ethanol fermentation was examined in order to save the cost for the treatment of waste distillage and promote cleansing production. Based on the data of 13 circulations, although the average fermentation time needed to be extended to 30~40 hours, over 12.5% ethanol was achieved, at the same time, residual reducing sugar and total sugar were maintained below 0.70% and 0.90%, which indicates that the negative effect of the completely recycling use of waste distillage was limited, and the waste distillage can be completely recycled within the fermentation system.

在此基础上，从减轻废糟液处理负荷，实现清洁生产的需要出发，进行了无种子罐条件下酒精蒸馏废液直接全循环使用的自絮凝颗粒酵母酒精连续发酵实验研究，十三次全循环运行得到的实验数据，与无废液循环的实验结果相比，虽然平均发酵时间略增至30h～40h，但发酵终点酒精浓度仍达到12.5％以上，残还原糖和残总糖分别在0.70％和0.90％以下，说明循环积累物对发酵的影响有限，废糟液直接全循环使用的工艺技术路线可行。

Objective To analyze the chemical components of the extracts of Kacmpferia galanga L from supercritical CO2 extraction, and to compare the extraction efficiency between supercritical CO2 extraction and traditional water distillation.

目的 研究沙姜超临界CO2萃取物的化学成分，并比较超临界CO2提取法和传统的水蒸气蒸馏提取法的提取效果。

In order to supply basic thermodynamic data for the separation design of acetyl acetone from the isomerization reaction of isopropenyl acetate,vapor-liquid equilibrium data of isopropenyl acetate-acetyl acetone system under 101.3 kPa was measured using Ellis equilibrium still.

为了给乙酸异丙烯酯异构化生产乙酰丙酮工艺的产物分离设计提供基础热力学数据，用埃利斯平衡蒸馏器测定了101.3 kPa下乙酸异丙烯酯-乙酰丙酮体系的汽液平衡数据，结果表明，该二元体系未形成共沸物，实验数据通过了Herrington面积法的热力学一致性检验。

In the technical scheme of the invention, reactant, ammonia and hydrogen peroxide are ordinally added into the reaction system of catalyst containing Ti-MWW-F molecular sieve and solvent, and after stiring, temperature raising and reaction are finished, an oxime product is produced by filtering, distillation, liquor filtering and separation.

本发明的技术方案是将反应物酮或醛、氨、过氧化氢依次加入到含Ti-MWW-F分子筛的催化剂和溶剂的反应体系中，搅拌，升温，反应结束后，经过滤，蒸馏滤液，分离得到产物肟。

Results Nine compounds from supercritical CO2 extraction were identified and the main constituents were pentadecane, ethyl pmethoxycinnamate and ethyl cinnamate. Twentyeight compounds from water distillation were identified and the main constituents were δ3carene, ethyl pmethoxycinnamate and ethyl cinnamate.

结果 沙姜超临界CO2萃取物中分离鉴定出9种化合物，主要成分为十五烷、肉桂酸乙酯、对甲氧基肉桂酸乙酯等；水蒸气蒸馏法中分离鉴定出28种化合物，主要成分为δ3蒈烯、肉桂酸乙酯和对甲氧基肉桂酸乙酯等。

Results Nine compounds from supercritical CO2 extraction were identified and the main constituents were pentadecane, ethyl p-methoxycinnamate and ethyl cinnamate. Twenty-eight compounds from water distillation were identified and the main constituents were δ-3-carene, ethyl p-methoxycinnamate and ethyl cinnamate.

结果 沙姜超临界CO2萃取物中分离鉴定出9种化合物，主要成分为十五烷、肉桂酸乙酯、对甲氧基肉桂酸乙酯等；水蒸气蒸馏法中分离鉴定出28种化合物，主要成分为δ-3-蒈烯、肉桂酸乙酯和对甲氧基肉桂酸乙酯等。

Syntheses and characterization of transition metal complexes of Schiff base derived from adamantaneamine and salicylaldehyde

收率90%。将光气通入熔融的对硝基苯甲酸，将光气化反应物进行减压蒸馏，也可以获得对硝基苯甲酰氯。

The effects of processing conditions, such as composition of wall material,dosage of emulsifier,wall material concentraion,the ratio of cinnaldehyde to wall material,inlet air temperature,inlet speed of mixture and air pressure of ejector were discussed.

实验结果表明，阿拉伯胶和麦芽糊精的最佳质量配比为 1∶1，蒸馏单甘酯的用量为 0 。4 g/dL ，固形物质量分数为 4 0 %，芯材与壁材的配比为 1mL∶10 g ，肉桂醛微胶囊化的最佳喷雾干燥条件为进风温度 2 2 5℃，进料流量 2 10mL/h ，喷射压力0 。18MPa 。

This causes the volatiles to be distilled from the coal to give a porous coke.

这一过程使挥发物从煤中蒸馏出来而产生多孔的焦炭。

Since historical times,England ,where the early inhabitants were Celts, has been conquered three times .

从有历史以来，英国，在此地早期居住的是凯尔特人，已经被征服了三次。

Bluetooth OBEX File Transfer Enables the sending and receiving of files on your phone via Bluetooth.

蓝牙OBEX文件移动允许经过蓝牙传送和接受文件。。。。